Specific Process Knowledge/Lithography/UVLithography: Difference between revisions

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'''Feedback to this page''': '''[mailto:labadviser@nanolab.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.nanolab.dtu.dk/index.php/Specific_Process_Knowledge/Lithography/UVLithography click here]'''
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[[Image:UVLithography.jpg|320x320px|right|frame|]]
'''Feedback to this page''': '''[mailto:labadviser@nanolab.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.nanolab.dtu.dk/index.php?title=Specific_Process_Knowledge/Lithography/UVLithography click here]'''


UV Lithography uses ultraviolet light to transfer a pattern from a mask to a wafer coated with photoresist. The photoresist film is spin coated on the wafers and the pattern is transferred to the wafer by using a mask aligner. DTU Nanolab houses a number of automatic or semi-automatic coaters and mask aligners.
[[Category: Equipment|Lithography]]
[[Category: Lithography]]
 
[[Image:UVLithography.jpg|320x320px|right|]]
 
__TOC__
 
UV Lithography uses ultraviolet light to transfer a pattern from a photo-mask or a design file to a wafer coated with photoresist. The photoresist film is spin coated onto the wafers, the design is transferred to the resist by using an aligner, and subsequently the resist pattern is developed. DTU Nanolab houses a number of automatic or manual coaters, mask or maskless aligners, as well as automatic or semi-automatic developers.


= Getting started =
= Getting started =
Line 12: Line 19:


'''Before you plan your UV processing and request for training on any equipment in UV lithography, please go through the following steps.''' Include the information in the training request.
'''Before you plan your UV processing and request for training on any equipment in UV lithography, please go through the following steps.''' Include the information in the training request.
Also, please remember that the [https://labadviser.nanolab.dtu.dk//index.php?title=Specific_Process_Knowledge/Lithography#Lithography_Tool_Package_Training Lithography TPT] is mandatory before training in any lithography equipment.


If you are new to photolithography, you can visit <u>[https://en.wikipedia.org/wiki/Photolithography this]</u> wikipedia webpage about photolithography before you start.
If you are new to photolithography, you can visit <u>[https://en.wikipedia.org/wiki/Photolithography this]</u> wikipedia webpage about photolithography before you start.
<br> <br>
<br> <br>


* '''Prepare a process flow''' which describes all steps in your UV lithography process. You can find docx-templates <u>[[Specific_Process_Knowledge/Lithography/UVLithography#Resist_Overview|in this table]]</u>.
'''Pre-cleanroom work:'''
 
#'''Complete the [https://labadviser.nanolab.dtu.dk//index.php?title=Specific_Process_Knowledge/Lithography#Lithography_Tool_Package_Training Lithography TPT].
* '''Substrate pretreatment''': In many processes it is recommended to <u>[[Specific_Process_Knowledge/Lithography/Pretreatment|pretreat or prime]]</u> your wafer before spin-coating. In some <u>[[Specific_Process_Knowledge/Lithography/Coaters|spin-coaters]]</u>, these pretreatment processes are included in the spin coating of resist.
#'''Prepare a process flow:''' The process flow describes all steps in your UV lithography process. You can find docx-templates <u>[[Specific_Process_Knowledge/Lithography/Resist/UVresist#UV_resist_comparison_table|in this table]]</u>.
 
#'''Design device''': Design your device and layout. A detailed instruction on how to design a layout (or mask) can be found <u>[[Specific_Process_Knowledge/Pattern_Design|here]]</u>.
* '''Spin Coater''': Do you wish to use a manual spin coater or a robot spin coater? See a list of spin coaters <u>[[Specific_Process_Knowledge/Lithography/Coaters|here]]</u>.
#'''Mask''': If you wish to use a mask aligner, order a photomask for your UV process. Instructions on how to order a photomask can be found <u>[[Specific_Process_Knowledge/Pattern_Design#Mask_Ordering_and_Fabrication|here]]</u>.
 
* '''Resist Type''': Choose the type of resist you wish to use: a list of UV lithography resist types available at DTU Nanolab can be found <u>[[Specific_Process_Knowledge/Lithography/UVLithography#Resist_Overview|on this page]]</u>.
** Positive tone resist: Resist exposed to UV light will be dissolved in the developer. The mask openings are an exact copy of the resist pattern which is to remain on the wafer.
** Negative tone resist: Resist exposed to UV light will become polymerized and difficult to dissolve. The mask openings are an inverse copy of the resist pattern which is to remain on the wafer.
 
* '''Thickness of resist''': In general, it is recommended to work at or below an aspect ratio of ~1, i.e. where the width of the pattern is larger than the thickness of the resist. Furthermore, when you decide for the resist thickness, consider which transfer you need:
** For <u>[[Specific_Process_Knowledge/Lithography/LiftOff|lift-off]]</u> processes, we recommend resist thickness at least 5 times larger than the thickness of the metal to be lifted.
** For dry etch or wet etch processes, investigate the resist etch rate of your process as this might limit the minimum thickness of your resist.
 
*'''Exposure''': Choose which aligner you wish to use, and consider the exposure dose.
** You can find a list of mask aligners <u>[[Specific_Process_Knowledge/Lithography/UVExposure|here]]</u>.
** You can find information on dose <u>[[Specific_Process_Knowledge/Lithography/UVExposure_Dose|here]]</u>.
 
* '''Mask''': Design and order a photomask for your UV process. A detailed instruction on how to design and order a photomask can be found <u>[[Specific_Process_Knowledge/Pattern_Design|here]]</u>.


* '''Development''': Choose which equipment you wish to use to develop your photoresist from <u>[[Specific_Process_Knowledge/Lithography/Development|this list]]</u>. Remember the development process influences the <u>[[Specific_Process_Knowledge/Lithography/UVExposure_Dose|exposure dose]]</u>.
'''Cleanroom work:'''
 
#'''Substrate pretreatment''': In many processes it is recommended to <u>[[Specific_Process_Knowledge/Lithography/Pretreatment|pretreat or prime]]</u> your wafer before spin-coating. In some <u>[[Specific_Process_Knowledge/Lithography/Coaters|spin-coaters]]</u>, these pretreatment processes are included in the spin coating of resist.
* '''Specify whether you wish to strip or lift-off your resist''': <u>[[Specific_Process_Knowledge/Lithography/Strip|strip]]</u> and <u>[[Specific_Process_Knowledge/Lithography/LiftOff|lift-off]]</u>.
#'''Resist Type''': Choose the type of resist you wish to use: a list of UV lithography resist types available at DTU Nanolab can be found <u>[[Specific_Process_Knowledge/Lithography/Resist#UV_Resist|on this page]]</u>.
#*Positive tone resist: Resist exposed to UV light will be dissolved in the developer. For mask aligners, the mask openings are an exact copy of the resist pattern which is to remain on the wafer.
#*Negative tone resist: Resist exposed to UV light will become polymerized and difficult to dissolve. For mask aligners, the mask openings are an ''inverse'' copy of the resist pattern which is to remain on the wafer.
#'''Thickness of resist''': In general, it is recommended to work at, or below, an aspect ratio of ~1, i.e. where the feature sizes of the pattern, is larger than the thickness of the resist. Furthermore, when you decide on the resist thickness, consider which transfer you need:
#*For <u>[[Specific_Process_Knowledge/Lithography/LiftOff|lift-off]]</u> processes, we recommend resist thickness at least 5 times larger than the thickness of the metal to be lifted.
#*For dry etch or wet etch processes, investigate the resist etch rate of your process, as this might limit the ''minimum'' thickness of your resist.
#'''Spin Coater''': Do you wish to use a manual spin coater or an automatic spin coater? See a list of spin coaters <u>[[Specific_Process_Knowledge/Lithography/Coaters|here]]</u>.
#'''Exposure''': Choose which aligner you wish to use, and consider the exposure dose.
#*You can find a list of mask aligners and maskless aligners <u>[[Specific_Process_Knowledge/Lithography/UVExposure|here]]</u>.
#*You can find information on dose <u>[[Specific_Process_Knowledge/Lithography/Resist#UV_Resist|here]]</u>.
#'''Development''': Choose which equipment you wish to use to develop your photoresist from <u>[[Specific_Process_Knowledge/Lithography/Development|this list]]</u>. Remember the development process influences the <u>[[Specific_Process_Knowledge/Lithography/Resist#UV_Resist|exposure dose]]</u>.
#'''Specify whether you wish to strip or lift-off your resist''': <u>[[Specific_Process_Knowledge/Lithography/Strip|strip]]</u> and <u>[[Specific_Process_Knowledge/Lithography/LiftOff|lift-off]]</u>.


<br clear=all />
<br clear=all />
= Resist Overview =
{|border="1" cellspacing="1" cellpadding="3" style="text-align:left;" width="90%"
|-
|-
|-style="background:silver; color:black"
|'''Resist'''
|width=100|'''Polarity'''
|'''Spectral sensitivity'''
|'''Manufacturer'''
|width=200|'''Comments'''
|width=100|'''Technical reports'''
|'''[[Specific_Process_Knowledge/Lithography/Coaters|Spin Coating]]'''
|'''[[Specific_Process_Knowledge/Lithography/UVExposure|Exposure]]'''
|'''[[Specific_Process_Knowledge/Lithography/Development|Developer]]'''
|'''Rinse'''
|width=100|'''Remover'''
|'''Process flows (in docx-format)'''
|-
|-
|-style="background:WhiteSmoke; color:black"
|'''[[Specific_Process_Knowledge/Lithography/5214E|AZ 5214E]]'''
|Positive but the image can be reversed
|310 - 420 nm
|[https://www.merckgroup.com/en/brands/pm/az-products.html Merck KGaA]
Supplied by [https://www.microchemicals.com/ MicroChemicals GmbH]
|Can be used for both positive and image reversed (negative) processes with resist thickness between 1 and 4 µm.
|[[media:AZ5214E.pdf‎|AZ5214E.pdf‎]]
[https://www.microchemicals.com/micro/tds_az_5214e_photoresist.pdf Photoresist AZ® 5214 E (TDS)]
|Automatic spin coater ([[Specific_Process_Knowledge/Lithography/Coaters#Spin_Coater:_Gamma_UV|Gamma UV]] or [[Specific_Process_Knowledge/Lithography/Coaters#Spin_Coater:_Gamma_E-beam_and_UV|Gamma e-beam & UV]])
Manual spin coater ([[Specific_Process_Knowledge/Lithography/Coaters#Manual_Spin_Coaters|LabSpin]] or [[Specific_Process_Knowledge/Lithography/Coaters#Spin_Coater:_RCD8|RCD8]])
|Mask aligner ([[Specific_Process_Knowledge/Lithography/UVExposure#KS_Aligner|KS]] or [[Specific_Process_Knowledge/Lithography/UVExposure#Aligner:_MA6_-_2|MA6 - 2]])
Maskless aligner ([[Specific_Process_Knowledge/Lithography/UVExposure#Aligner:_Maskless_01|01]], [[Specific_Process_Knowledge/Lithography/UVExposure#Aligner:_Maskless_02|02]] or [[Specific_Process_Knowledge/Lithography/UVExposure#Aligner:_Maskless_03|03]])
|[[Specific_Process_Knowledge/Lithography/Development#Developer-6inch|AZ 351B developer]]
or
[[Specific_Process_Knowledge/Lithography/Development#Developer_TMAH_UV-lithography|AZ 726 MIF developer]]
|DI water
|Acetone
|
[[media:‎Process_Flow_AZ5214E_pos_vers2.docx‎ |Process_Flow_AZ5214_pos.docx‎]]
[[media:Process_Flow_AZ5214E_rev_vers2.docx‎ |Process_Flow_AZ5214_rev.docx‎]]
|-
|-style="background:LightGrey; color:black"
|'''[[Specific_Process_Knowledge/Lithography/4562|AZ 4562]]'''
|Positive
|310 - 440 nm
|[https://www.merckgroup.com/en/brands/pm/az-products.html Merck KGaA]
Supplied by [https://www.microchemicals.com/ MicroChemicals GmbH]
|For process with resist thickness between 6 and 25 µm.
|[[media:AZ4500.pdf‎|AZ4500.pdf‎]]
[https://www.microchemicals.com/micro/tds_az_4500_series.pdf Photoresist AZ® 4562 (TDS)]
|Automatic spin coater ([[Specific_Process_Knowledge/Lithography/Coaters#Spin_Coater:_Gamma_E-beam_and_UV|Gamma e-beam & UV]])
Manual spin coater ([[Specific_Process_Knowledge/Lithography/Coaters#Manual_Spin_Coaters|LabSpin]] or [[Specific_Process_Knowledge/Lithography/Coaters#Spin_Coater:_RCD8|RCD8]])
|Mask aligner ([[Specific_Process_Knowledge/Lithography/UVExposure#KS_Aligner|KS]] or [[Specific_Process_Knowledge/Lithography/UVExposure#Aligner:_MA6_-_2|MA6 - 2]])
Maskless aligner ([[Specific_Process_Knowledge/Lithography/UVExposure#Aligner:_Maskless_01|01]] or [[Specific_Process_Knowledge/Lithography/UVExposure#Aligner:_Maskless_03|03]])
|[[Specific_Process_Knowledge/Lithography/Development#Developer-6inch|AZ 351B developer]]
or
[[Specific_Process_Knowledge/Lithography/Development#Developer_TMAH_UV-lithography|AZ 726 MIF developer]]
|DI water
|Acetone
|[[media:Process_Flow_thick_AZ4562_vers2.docx‎|Process_Flow_thick_AZ4562.docx‎]]
|-
|-style="background:WhiteSmoke; color:black"
|'''[[Specific_Process_Knowledge/Lithography/MiR|AZ MiR 701]]'''
|Positive
|310 - 445 nm
|[https://www.merckgroup.com/en/brands/pm/az-products.html Merck KGaA]
Supplied by [https://www.microchemicals.com/ MicroChemicals GmbH]
|High selectivity for dry etch.
Resist thickness 1.5 - 4 µm.
|[[media:AZ_MiR_701.pdf‎|AZ_MiR_701.pdf‎]]
[https://www.microchemicals.com/micro/tds_az_mir701_photoresist.pdf Photoresist AZ® MIR 701 (TDS)]
|Automatic spin coater ([[Specific_Process_Knowledge/Lithography/Coaters#Spin_Coater:_Gamma_UV|Gamma UV]] or [[Specific_Process_Knowledge/Lithography/Coaters#Spin_Coater:_Gamma_E-beam_and_UV|Gamma e-beam & UV]])
Manual spin coater ([[Specific_Process_Knowledge/Lithography/Coaters#Manual_Spin_Coaters|LabSpin]] or [[Specific_Process_Knowledge/Lithography/Coaters#Spin_Coater:_RCD8|RCD8]])
|Mask aligner ([[Specific_Process_Knowledge/Lithography/UVExposure#KS_Aligner|KS]] or [[Specific_Process_Knowledge/Lithography/UVExposure#Aligner:_MA6_-_2|MA6 - 2]])
Maskless aligner ([[Specific_Process_Knowledge/Lithography/UVExposure#Aligner:_Maskless_01|01]], [[Specific_Process_Knowledge/Lithography/UVExposure#Aligner:_Maskless_02|02]] or [[Specific_Process_Knowledge/Lithography/UVExposure#Aligner:_Maskless_03|03]])
|[[Specific_Process_Knowledge/Lithography/Development#Developer_TMAH_UV-lithography|AZ 726 MIF developer]]
|DI water
|Remover 1165
|[[media:Process_Flow_AZ_MiR701.docx‎|Process_Flow_AZ_MiR701.docx‎]]
|-
|-style="background:LightGrey; color:black"
|'''[[Specific_Process_Knowledge/Lithography/nLOF|AZ nLOF 2020]]'''
|Negative
|310 - 380 nm
|[https://www.merckgroup.com/en/brands/pm/az-products.html Merck KGaA]
Supplied by [https://www.microchemicals.com/ MicroChemicals GmbH]
|Negative sidewalls for lift-off.
Resist thickness 1.5 - 4 µm.
|[[media:AZ_nLOF_2020.pdf‎|AZ_nLOF_2020.pdf‎]]
[https://www.microchemicals.com/micro/tds_az_nlof2000_series.pdf Photoresist AZ®nLOF 2020 (TDS)]
|Automatic spin coater ([[Specific_Process_Knowledge/Lithography/Coaters#Spin_Coater:_Gamma_UV|Gamma UV]])
Manual spin coater ([[Specific_Process_Knowledge/Lithography/Coaters#Manual_Spin_Coaters|LabSpin]] or [[Specific_Process_Knowledge/Lithography/Coaters#Spin_Coater:_RCD8|RCD8]])
|Mask aligner ([[Specific_Process_Knowledge/Lithography/UVExposure#KS_Aligner|KS]] or [[Specific_Process_Knowledge/Lithography/UVExposure#Aligner:_MA6_-_2|MA6 - 2]])
Maskless aligner ([[Specific_Process_Knowledge/Lithography/UVExposure#Aligner:_Maskless_01|01]] or [[Specific_Process_Knowledge/Lithography/UVExposure#Aligner:_Maskless_02|02]])
|[[Specific_Process_Knowledge/Lithography/Development#Developer_TMAH_UV-lithography|AZ 726 MIF developer]]
|DI water
|Remover 1165
|[[media:Process_Flow_AZ_nLOF_2020.docx‎|Process_Flow_AZ_nLOF_2020.docx‎]]
|-
|-style="background:WhiteSmoke; color:black"
|'''[[Specific Process Knowledge/Lithography/SU-8|SU-8]]'''
|Negative
|350 - 400 nm
|[https://kayakuam.com/products/su-8-2000/ Kayaku Advanced Materials, Inc.]
Supplied by [http://www.microresist.com/products/ micro resist technology GmbH]
|High aspect ratio.
Resist thickness 1 µm to several 100 µm.
|[[media:SU-8_DataSheet_2005.pdf‎|SU-8_DataSheet_2005.pdf‎]], [[media:SU-8_DataSheet_2075.pdf‎|SU-8_DataSheet_2075.pdf‎]]
|Manual spin coater ([[Specific_Process_Knowledge/Lithography/Coaters#Manual_Spin_Coaters|LabSpin]] or [[Specific_Process_Knowledge/Lithography/Coaters#Spin_Coater:_RCD8|RCD8]])
|Mask aligner ([[Specific_Process_Knowledge/Lithography/UVExposure#KS_Aligner|KS]] or [[Specific_Process_Knowledge/Lithography/UVExposure#Aligner:_MA6_-_2|MA6 - 2]])
Maskless aligner ([[Specific_Process_Knowledge/Lithography/UVExposure#Aligner:_Maskless_01|01]] or [[Specific_Process_Knowledge/Lithography/UVExposure#Aligner:_Maskless_02|02]])
|[[Specific_Process_Knowledge/Lithography/Development#SU8-Developer|mr-Dev 600 developer (PGMEA)]]
|IPA
|Plasma ashing can remove crosslinked SU-8
|[[media:Process_Flow_SU8_70um.docx‎|Process_Flow_SU8_70um.docx‎]]
|}
<br clear="all" />


=Process information=
=Process information=


===Information from our suppliers===
===[[Specific Process Knowledge/Lithography/Resist#UV_Resist|UV Resist]]===
 
[https://www.microchemicals.com/downloads/application_notes.html Application notes] from MicroChemicals GmbH, e.g. [https://www.microchemicals.com/technical_information/lithography_trouble_shooting.pdf Lithography Trouble-Shooter]
 
===[[Specific Process Knowledge/Lithography/Pretreatment|Pretreatment]]===
===[[Specific Process Knowledge/Lithography/Pretreatment|Pretreatment]]===
===[[Specific Process Knowledge/Lithography/Coaters|Coaters]]===
===[[Specific Process Knowledge/Lithography/Coaters|Coating]]===
===[[Specific Process Knowledge/Lithography/UVExposure|UV Exposure]]===
===[[Specific_Process_Knowledge/Lithography/UVExposure_Dose|Information on UV Exposure Dose]]===
===[[Specific Process Knowledge/Lithography/Baking|Baking]]===
===[[Specific Process Knowledge/Lithography/Baking|Baking]]===
===[[Specific Process Knowledge/Lithography/UVExposure|UV Exposure Tools]]===
===[[Specific Process Knowledge/Lithography/Development|Development]]===
===[[Specific Process Knowledge/Lithography/Development|Development]]===
===[[Specific Process Knowledge/Lithography/Descum|Descum]]===
===[[Specific Process Knowledge/Lithography/Descum|Descum]]===
===[[Specific Process Knowledge/Lithography/LiftOff|Lift-off]]===
===[[Specific Process Knowledge/Lithography/Strip|Stripping Resist]]===
===[[Specific Process Knowledge/Lithography/Strip|Stripping Resist]]===
===[[Specific Process Knowledge/Lithography/LiftOff|Lift-off]]===
 
==Information from our suppliers==
 
[https://www.microchemicals.com/downloads/application_notes.html Application notes] from MicroChemicals GmbH, e.g. [https://www.microchemicals.com/technical_information/lithography_trouble_shooting.pdf Lithography Trouble-Shooter]

Latest revision as of 13:56, 18 September 2024

The contents on this page, including all images and pictures, was created by DTU Nanolab staff unless otherwise stated.

Feedback to this page: click here

UV Lithography uses ultraviolet light to transfer a pattern from a photo-mask or a design file to a wafer coated with photoresist. The photoresist film is spin coated onto the wafers, the design is transferred to the resist by using an aligner, and subsequently the resist pattern is developed. DTU Nanolab houses a number of automatic or manual coaters, mask or maskless aligners, as well as automatic or semi-automatic developers.

Getting started

Before you plan your UV processing and request for training on any equipment in UV lithography, please go through the following steps. Include the information in the training request.

Also, please remember that the Lithography TPT is mandatory before training in any lithography equipment.

If you are new to photolithography, you can visit this wikipedia webpage about photolithography before you start.

Pre-cleanroom work:

  1. Complete the Lithography TPT.
  2. Prepare a process flow: The process flow describes all steps in your UV lithography process. You can find docx-templates in this table.
  3. Design device: Design your device and layout. A detailed instruction on how to design a layout (or mask) can be found here.
  4. Mask: If you wish to use a mask aligner, order a photomask for your UV process. Instructions on how to order a photomask can be found here.

Cleanroom work:

  1. Substrate pretreatment: In many processes it is recommended to pretreat or prime your wafer before spin-coating. In some spin-coaters, these pretreatment processes are included in the spin coating of resist.
  2. Resist Type: Choose the type of resist you wish to use: a list of UV lithography resist types available at DTU Nanolab can be found on this page.
    • Positive tone resist: Resist exposed to UV light will be dissolved in the developer. For mask aligners, the mask openings are an exact copy of the resist pattern which is to remain on the wafer.
    • Negative tone resist: Resist exposed to UV light will become polymerized and difficult to dissolve. For mask aligners, the mask openings are an inverse copy of the resist pattern which is to remain on the wafer.
  3. Thickness of resist: In general, it is recommended to work at, or below, an aspect ratio of ~1, i.e. where the feature sizes of the pattern, is larger than the thickness of the resist. Furthermore, when you decide on the resist thickness, consider which transfer you need:
    • For lift-off processes, we recommend resist thickness at least 5 times larger than the thickness of the metal to be lifted.
    • For dry etch or wet etch processes, investigate the resist etch rate of your process, as this might limit the minimum thickness of your resist.
  4. Spin Coater: Do you wish to use a manual spin coater or an automatic spin coater? See a list of spin coaters here.
  5. Exposure: Choose which aligner you wish to use, and consider the exposure dose.
    • You can find a list of mask aligners and maskless aligners here.
    • You can find information on dose here.
  6. Development: Choose which equipment you wish to use to develop your photoresist from this list. Remember the development process influences the exposure dose.
  7. Specify whether you wish to strip or lift-off your resist: strip and lift-off.


Process information

UV Resist

Pretreatment

Coating

Baking

UV Exposure Tools

Development

Descum

Lift-off

Stripping Resist

Information from our suppliers

Application notes from MicroChemicals GmbH, e.g. Lithography Trouble-Shooter