Specific Process Knowledge/Lithography/UVLithography: Difference between revisions

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'''Feedback to this page''': '''[mailto:labadviser@danchip.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.danchip.dtu.dk/index.php/Specific_Process_Knowledge/Lithography/UVLithography click here]'''
{{cc-nanolab}}


[[Image:UVLithography.jpg|320x320px|right|frame|]]
'''Feedback to this page''': '''[mailto:labadviser@nanolab.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.nanolab.dtu.dk/index.php?title=Specific_Process_Knowledge/Lithography/UVLithography click here]'''


UV Lithography uses ultraviolet light to transfer a pattern from a mask to a wafer coated with photoresist.  The photoresist film is spin coated on the wafers and the pattern is transferred to the wafer by using a mask aligner. DTU Danchip houses a number of automatic or semi-automatic coaters and mask aligners.
[[Category: Equipment|Lithography]]
[[Category: Lithography]]


[[Image:UVLithography.jpg|320x320px|right|]]


=Mask Design=
__TOC__


In order to realize your device you will need a way to draw the patterns that define the structures in the different layers on the wafer.
UV Lithography uses ultraviolet light to transfer a pattern from a photo-mask or a design file to a wafer coated with photoresist. The photoresist film is spin coated onto the wafers, the design is transferred to the resist by using an aligner, and subsequently the resist pattern is developed. DTU Nanolab houses a number of automatic or manual coaters, mask or maskless aligners, as well as automatic or semi-automatic developers.
This is done in a drawing tool for mask layout. The output is a file you send to a mask house, which in return supplies you with a number of photolithographic masks. Each mask is a glass plate with a chromium pattern that mimics a layer in your layout.  


Please read more details here: [[/Mask Design|Mask Design]]
= Getting started =


[[File:UVLPic1.png|450px|right]]


= Resist Overview =
[[File:UVLPic2.png|160px|right]]


{|border="1" cellspacing="1" cellpadding="3" style="text-align:left;" width="90%"
'''Before you plan your UV processing and request for training on any equipment in UV lithography, please go through the following steps.''' Include the information in the training request.
|-


|-
Also, please remember that the [https://labadviser.nanolab.dtu.dk//index.php?title=Specific_Process_Knowledge/Lithography#Lithography_Tool_Package_Training Lithography TPT] is mandatory before training in any lithography equipment.
|-style="background:silver; color:black"
|'''Resist'''
|'''Polarity'''
|'''Manufacturer'''
|'''Comments'''
|'''Technical reports'''
|'''[[Specific_Process_Knowledge/Lithography/Coaters|Spin Coating]]'''
|'''[[Specific_Process_Knowledge/Lithography/UVExposure|Exposure dose]]'''
|'''[[Specific_Process_Knowledge/Lithography/Development|Developer]]'''
|'''Rinse'''
|'''Remover'''
|'''Process flows (in docx-format)'''


|-
If you are new to photolithography, you can visit <u>[https://en.wikipedia.org/wiki/Photolithography this]</u> wikipedia webpage about photolithography before you start.
<br> <br>


|-
'''Pre-cleanroom work:'''
|-style="background:WhiteSmoke; color:black"
#'''Complete the [https://labadviser.nanolab.dtu.dk//index.php?title=Specific_Process_Knowledge/Lithography#Lithography_Tool_Package_Training Lithography TPT].
|'''AZ 5214E'''
#'''Prepare a process flow:''' The process flow describes all steps in your UV lithography process. You can find docx-templates <u>[[Specific_Process_Knowledge/Lithography/Resist/UVresist#UV_resist_comparison_table|in this table]]</u>.
|Positive but can be reversed
#'''Design device''': Design your device and layout. A detailed instruction on how to design a layout (or mask) can be found <u>[[Specific_Process_Knowledge/Pattern_Design|here]]</u>.
|[http://www.azem.com/en/Products/Litho-technology/Photoresists.aspx AZ Electronic Materials]
#'''Mask''': If you wish to use a mask aligner, order a photomask for your UV process. Instructions on how to order a photomask can be found <u>[[Specific_Process_Knowledge/Pattern_Design#Mask_Ordering_and_Fabrication|here]]</u>.
|Can be used for both positive and reverse processes with resist thickness between 1 to 4um.
|[[media:AZ5214E.pdf‎|AZ5214E.pdf‎]]
|[[Specific_Process_Knowledge/Lithography/Coaters#SSE Spinner|SSE]], [[Specific_Process_Knowledge/Lithography/Coaters#KS Spinner|KS Spinner]], [[Specific_Process_Knowledge/Lithography/Coaters#III-V Spinner|III-V Spinner]]
|'''Positive process:'''


23-33 mJ/cm<sup>2</sup> per µm resist for i-line.
'''Cleanroom work:'''
#'''Substrate pretreatment''': In many processes it is recommended to <u>[[Specific_Process_Knowledge/Lithography/Pretreatment|pretreat or prime]]</u> your wafer before spin-coating. In some <u>[[Specific_Process_Knowledge/Lithography/Coaters|spin-coaters]]</u>, these pretreatment processes are included in the spin coating of resist.
#'''Resist Type''': Choose the type of resist you wish to use: a list of UV lithography resist types available at DTU Nanolab can be found <u>[[Specific_Process_Knowledge/Lithography/Resist#UV_Resist|on this page]]</u>.
#*Positive tone resist: Resist exposed to UV light will be dissolved in the developer. For mask aligners, the mask openings are an exact copy of the resist pattern which is to remain on the wafer.
#*Negative tone resist: Resist exposed to UV light will become polymerized and difficult to dissolve. For mask aligners, the mask openings are an ''inverse'' copy of the resist pattern which is to remain on the wafer.
#'''Thickness of resist''': In general, it is recommended to work at, or below, an aspect ratio of ~1, i.e. where the feature sizes of the pattern, is larger than the thickness of the resist. Furthermore, when you decide on the resist thickness, consider which transfer you need:
#*For <u>[[Specific_Process_Knowledge/Lithography/LiftOff|lift-off]]</u> processes, we recommend resist thickness at least 5 times larger than the thickness of the metal to be lifted.
#*For dry etch or wet etch processes, investigate the resist etch rate of your process, as this might limit the ''minimum'' thickness of your resist.
#'''Spin Coater''': Do you wish to use a manual spin coater or an automatic spin coater? See a list of spin coaters <u>[[Specific_Process_Knowledge/Lithography/Coaters|here]]</u>.
#'''Exposure''': Choose which aligner you wish to use, and consider the exposure dose.
#*You can find a list of mask aligners and maskless aligners <u>[[Specific_Process_Knowledge/Lithography/UVExposure|here]]</u>.
#*You can find information on dose <u>[[Specific_Process_Knowledge/Lithography/Resist#UV_Resist|here]]</u>.
#'''Development''': Choose which equipment you wish to use to develop your photoresist from <u>[[Specific_Process_Knowledge/Lithography/Development|this list]]</u>. Remember the development process influences the <u>[[Specific_Process_Knowledge/Lithography/Resist#UV_Resist|exposure dose]]</u>.
#'''Specify whether you wish to strip or lift-off your resist''': <u>[[Specific_Process_Knowledge/Lithography/Strip|strip]]</u> and <u>[[Specific_Process_Knowledge/Lithography/LiftOff|lift-off]]</u>.


½ dose for broadband exposure.
<br clear=all />
 
'''Reverse process:'''
 
10.5 mJ/cm<sup>2</sup> per µm resist for i-line, followed by 210 mJ/cm<sup>2</sup> flood exposure after reversal bake.
 
½ dose for broadband exposure.
|AZ 351B developer
|DI water
|Acetone
|
[[media:‎Process_Flow_AZ5214E_pos_vers2.docx‎ |Process_Flow_AZ5214_pos.docx‎]]
[[media:Process_Flow_AZ5214E_rev_vers2.docx‎ |Process_Flow_AZ5214_rev.docx‎]]
 
|-
|-style="background:LightGrey; color:black"
|'''AZ 4562'''
|Positive
|[http://www.azem.com/en/Products/Litho-technology/Photoresists.aspx AZ Electronic Materials]
|For process with resist thickness between 6 and 25um.
|[[media:AZ4500.pdf‎|AZ4500.pdf‎]]
|[[Specific_Process_Knowledge/Lithography/Coaters#SSE Spinner|SSE]], [[Specific_Process_Knowledge/Lithography/Coaters#KS Spinner|KS Spinner]]
|28 mJ/cm<sup>2</sup> per µm resist for i-line, probably increasing with increasing thickness.
 
Multiple exposure recommended.
 
½ dose for broadband exposure.
|AZ 351B developer
|DI water
|Acetone
|[[media:Process_Flow_thick_AZ4562_vers2.docx‎|Process_Flow_thick_AZ4562.docx‎]]
 
|-
|-style="background:WhiteSmoke; color:black"
|'''AZ MiR 701'''
|Positive
|[http://www.azem.com/en/Products/Litho-technology/Photoresists.aspx AZ Electronic Materials]
|High selectivity for dry etch.
|[[media:AZ_MiR_701.pdf‎|AZ_MiR_701.pdf‎]]
|[[Specific_Process_Knowledge/Lithography/Coaters#Spin Track 1 + 2|Spin Track 1 + 2]]
|Preliminary results:
 
105 mJ/cm<sup>2</sup> per µm resist for i-line.
 
1/5 dose for broadband exposure.
|AZ 726 MIF developer
|DI water
|Remover 1165
|[[media:Process_Flow_AZ_MiR701.docx‎|Process_Flow_AZ_MiR701.docx‎]]
 
|-
|-style="background:LightGrey; color:black"
|'''AZ nLOF 2020'''
|Negative
|[http://www.azem.com/en/Products/Litho-technology/Photoresists.aspx AZ Electronic Materials]
|
|[[media:AZ_nLOF_2020.pdf‎|AZ_nLOF_2020.pdf‎]]
|[[Specific_Process_Knowledge/Lithography/Coaters#Spin Track 1 + 2|Spin Track 1 + 2]]
|<30 mJ/cm<sup>2</sup> per µm resist for i-line, decreasing with increasing thickness.
 
Same dose for broadband exposure.
|AZ 726 MIF developer
|DI water
|Remover 1165
|[[media:Process_Flow_AZ_nLOF_2020.docx‎|Process_Flow_AZ_nLOF_2020.docx‎]]
 
|-
|-style="background:WhiteSmoke; color:black"
|'''SU-8'''
|Negative
|[http://microchem.com/Prod-SU82000.htm Microchem]
|
|[[media:SU-8_DataSheet_2005.pdf‎|SU-8_DataSheet_2005.pdf‎]], [[media:SU-8_DataSheet_2075.pdf‎|SU-8_DataSheet_2075.pdf‎]]
|[[Specific_Process_Knowledge/Lithography/Coaters#KS Spinner|KS Spinner]]
|Thickness and process dependent.
 
Refer to process datasheet and literature.
|mr-Dev 600 developer (PGMEA)
|IPA
|Plasma ashing can remove crosslinked SU8.
|[[media:Process_Flow_SU8_70um.docx‎|Process_Flow_SU8_70um.docx‎]]
 
|}
 
<br clear="all" />
 
=UV Lithography Equipment=
 
{| style="color: black;" width="100%"
| colspan="2" |
|-
| style="width: 50%"|


=Process information=


===[[Specific Process Knowledge/Lithography/Resist#UV_Resist|UV Resist]]===
===[[Specific Process Knowledge/Lithography/Pretreatment|Pretreatment]]===
===[[Specific Process Knowledge/Lithography/Pretreatment|Pretreatment]]===
*[[Specific Process Knowledge/Lithography/Pretreatment#HMDS|HMDS]]
===[[Specific Process Knowledge/Lithography/Coaters|Coating]]===
*[[Specific Process Knowledge/Lithography/Pretreatment#Buffered HF-Clean|BHF]]
*[[Specific Process Knowledge/Lithography/Pretreatment#Oven_250C|Oven 250C]]
 
===[[Specific Process Knowledge/Lithography/Coaters|Coaters]]===
*[[Specific Process Knowledge/Lithography/Coaters#SSE Spinner|SSE Spinner]]
*[[Specific Process Knowledge/Lithography/Coaters#Spin Track 1 + 2|Spin Track 1 + 2]]
*[[Specific Process Knowledge/Lithography/Coaters#KS Spinner|KS Spinner]]
*[[Specific Process Knowledge/Lithography/Coaters#Manual Spinner (Polymers)|Manual Spinner (Polymers)]]
*[[Specific Process Knowledge/Lithography/Coaters#Manual Spinner 1 (Laurell)|Manual Spinner 1 (Laurell)]]
*[[Specific Process Knowledge/Lithography/Coaters#Spin coater: Manual Labspin|Spin coater: Manual Labspin]]
*[[Specific_Process_Knowledge/Lithography/Coaters/SprayCoater|Spray Coater]]
 
===[[Specific Process Knowledge/Lithography/UVExposure|UV Exposure]]===
*[[Specific Process Knowledge/Lithography/UVExposure#KS Aligner|KS Aligner]]
*[[Specific Process Knowledge/Lithography/UVExposure#Aligner-6inch|Aligner-6inch]]
*[[Specific Process Knowledge/Lithography/UVExposure#III-V Aligner|III-V Aligner]]
*[[Specific Process Knowledge/Lithography/UVExposure#Inclined UV Lamp|Inclined UV Lamp]]
| style="width: 50%"|
 
===[[Specific Process Knowledge/Lithography/Baking|Baking]]===
===[[Specific Process Knowledge/Lithography/Baking|Baking]]===
*[[Specific Process Knowledge/Lithography/Baking#Hotplates|Hotplates]]
===[[Specific Process Knowledge/Lithography/UVExposure|UV Exposure Tools]]===
*[[Specific Process Knowledge/Lithography/Baking#Ovens|Ovens]]
 
===[[Specific Process Knowledge/Lithography/Development|Development]]===
===[[Specific Process Knowledge/Lithography/Development|Development]]===
*[[Specific Process Knowledge/Lithography/Development#Developer-1 and Developer-2|Developer-1 and Developer-2]]
===[[Specific Process Knowledge/Lithography/Descum|Descum]]===
*[[Specific Process Knowledge/Lithography/Development#Developer-6inch|Developer-6inch]]
*[[Specific Process Knowledge/Lithography/Development#SU8-Developer|SU8-Developer]]
*[[Specific Process Knowledge/Lithography/Development#Developer-TMAH|Developer-TMAH]]
 
===[[Specific Process Knowledge/Lithography/Strip|Strip]]===
*[[Specific Process Knowledge/Lithography/Strip#Plasma Asher 1|Plasma Asher 1]]
*[[Specific Process Knowledge/Lithography/Strip#Plasma Asher 2|Plasma Asher 2]]
*[[Specific Process Knowledge/Lithography/Strip#III-V Plasma Asher|III-V Plasma Asher]]
*[[Specific Process Knowledge/Lithography/Strip#Rough Acetone Strip|Rough Acetone Strip]]
*[[Specific Process Knowledge/Lithography/Strip#Fine Acetone Strip|Fine Acetone Strip]]
 
===[[Specific Process Knowledge/Lithography/LiftOff|Lift-off]]===
===[[Specific Process Knowledge/Lithography/LiftOff|Lift-off]]===
*[[Specific Process Knowledge/Lithography/LiftOff#Lift-off wet bench|Lift-off wet bench]]
===[[Specific Process Knowledge/Lithography/Strip|Stripping Resist]]===
*[[Specific Process Knowledge/Lithography/LiftOff#Lift-off (4", 6")|Lift-off (4", 6")]]


===[[Specific Process Knowledge/Lithography/WaferCleaning|Wafer Cleaning]]===
==Information from our suppliers==


|}
[https://www.microchemicals.com/downloads/application_notes.html Application notes] from MicroChemicals GmbH, e.g. [https://www.microchemicals.com/technical_information/lithography_trouble_shooting.pdf Lithography Trouble-Shooter]

Latest revision as of 13:56, 18 September 2024

The contents on this page, including all images and pictures, was created by DTU Nanolab staff unless otherwise stated.

Feedback to this page: click here

UV Lithography uses ultraviolet light to transfer a pattern from a photo-mask or a design file to a wafer coated with photoresist. The photoresist film is spin coated onto the wafers, the design is transferred to the resist by using an aligner, and subsequently the resist pattern is developed. DTU Nanolab houses a number of automatic or manual coaters, mask or maskless aligners, as well as automatic or semi-automatic developers.

Getting started

Before you plan your UV processing and request for training on any equipment in UV lithography, please go through the following steps. Include the information in the training request.

Also, please remember that the Lithography TPT is mandatory before training in any lithography equipment.

If you are new to photolithography, you can visit this wikipedia webpage about photolithography before you start.

Pre-cleanroom work:

  1. Complete the Lithography TPT.
  2. Prepare a process flow: The process flow describes all steps in your UV lithography process. You can find docx-templates in this table.
  3. Design device: Design your device and layout. A detailed instruction on how to design a layout (or mask) can be found here.
  4. Mask: If you wish to use a mask aligner, order a photomask for your UV process. Instructions on how to order a photomask can be found here.

Cleanroom work:

  1. Substrate pretreatment: In many processes it is recommended to pretreat or prime your wafer before spin-coating. In some spin-coaters, these pretreatment processes are included in the spin coating of resist.
  2. Resist Type: Choose the type of resist you wish to use: a list of UV lithography resist types available at DTU Nanolab can be found on this page.
    • Positive tone resist: Resist exposed to UV light will be dissolved in the developer. For mask aligners, the mask openings are an exact copy of the resist pattern which is to remain on the wafer.
    • Negative tone resist: Resist exposed to UV light will become polymerized and difficult to dissolve. For mask aligners, the mask openings are an inverse copy of the resist pattern which is to remain on the wafer.
  3. Thickness of resist: In general, it is recommended to work at, or below, an aspect ratio of ~1, i.e. where the feature sizes of the pattern, is larger than the thickness of the resist. Furthermore, when you decide on the resist thickness, consider which transfer you need:
    • For lift-off processes, we recommend resist thickness at least 5 times larger than the thickness of the metal to be lifted.
    • For dry etch or wet etch processes, investigate the resist etch rate of your process, as this might limit the minimum thickness of your resist.
  4. Spin Coater: Do you wish to use a manual spin coater or an automatic spin coater? See a list of spin coaters here.
  5. Exposure: Choose which aligner you wish to use, and consider the exposure dose.
    • You can find a list of mask aligners and maskless aligners here.
    • You can find information on dose here.
  6. Development: Choose which equipment you wish to use to develop your photoresist from this list. Remember the development process influences the exposure dose.
  7. Specify whether you wish to strip or lift-off your resist: strip and lift-off.


Process information

UV Resist

Pretreatment

Coating

Baking

UV Exposure Tools

Development

Descum

Lift-off

Stripping Resist

Information from our suppliers

Application notes from MicroChemicals GmbH, e.g. Lithography Trouble-Shooter