Specific Process Knowledge/Lithography/Strip
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Strip Comparison Table
| Equipment | Plasma Asher 3: Descum | Plasma Asher 4 | Plasma Asher 5 | Resist strip | Lift-off | |
|---|---|---|---|---|---|---|
| Purpose |
Resist descum |
Clean wafers only: |
All purposes |
Resist strip - no metal lift off! |
Lift-off | |
| Method |
Plasma ashing |
Plasma ashing |
Plasma ashing |
Solvent and ultra sound |
Solvent and ultra sound | |
| Process parameters | Process gasses |
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| Max. process power |
100 W (100%) |
1000 W |
1000 W |
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| Solvent |
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| Substrates | Batch size |
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| Allowed materials |
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Plasma Ashing process parameters
| Photoresist stripping | Descum after lithography | Surface treatment of plastic, ceramic and metal | Ashing of organic material | |
|---|---|---|---|---|
| Process pressure | 1.3 mbar | 1.3 mbar | 0.5-1.5 mbar | 0.5-1.5 mbar |
| Process gases |
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O2, CF4, N2 or their mixtures | O2 |
| Process power | 1000 W | 200 W | 150-1000 W | 1000 W or less for heat- sensitive materials |
| Process time | 5-90 minutes | 1-30 minutes | seconds to minutes | Between 0.5 and 20 hours, depending on the material |
| Batch size | 1-25 | 1-25 | 1 wafer at a time | 1 wafer at a time, use a container, e.g Petri dish |
Process gas ratio for plasma asher 4 & 5
The ashing rate is related to the gas mix, usually expressed as percentage of nitrogen of the total amount of gas. Process development tests found that a gas mix of 50% nitrogen gives the highest ashing rate for both processing single substrates and when processing a full boat with 25 substrates.
Please note that the ashing rate for a full boat is approximately ten times slower, than the processing time for a single substrate.
| Test setup | Single substrate | Full boat |
|---|---|---|
| Test results | Highest ashing rate at 30-80% Nitrogen | Highest ashing rate at 50-70% Nitrogen |
| Wafers | 1 | 25 |
| Wafer size | 100 mm | 100 mm |
| Boat position | Center of chamber | Center of chamber |
| Test wafer position | Center of boat | Center of boat |
| Total gas flow rate | 500 | 200 |
| Gas mix ratio | Tested parameter | Tested parameter |
| Chamber pressure | 1.25 mbar | 1.3 mbar |
| Power | 1000 W | 1000 W |
| Test processing time | 2 minutes | 10 minutes |
| Test average temperature | 43°C | 47°C |
Process chamber pressure for plasma asher 4 & 5
The ashing rate is related to the chamber pressure during processing. Process development tests found that 1.3 mbar gives the highest ashing rate for both processing single substrates and when processing a full boat with 25 substrates.
Please note that the ashing rate for a full boat is approximately ten times slower, than the processing time for a single substrate.
| Test setup | Single substrate | Full boat |
|---|---|---|
| Test results | Highest ashing rate at 1.3 mbar | Highest ashing rate at 1.4 mbar |
| Wafers | 1 | 25 |
| Wafer size | 100 mm | 100 mm |
| Boat position | Center of chamber | Center of chamber |
| Test wafer position | Center of boat | Center of boat |
| Total gas flow rate | 150 | 200 |
| Gas mix ratio | 30% N2 | 30% N2 |
| Chamber pressure | Tested parameter | Tested parameter |
| Power | 1000 W | 1000 W |
| Test processing time | 2 minutes | 10 minutes |
| Test average temperature | 43°C | 55°C |
Process gas flow rate for plasma asher 4 & 5
The ashing rate is related to the total gas flow rate during processing. Process development tests found that 200 sccm gives the highest ashing rate for both processing single substrates and when processing a full boat with 25 substrates.
Please note that the ashing rate for a full boat is approximately ten times slower, than the processing time for a single substrate.
Single substrate:
Test using a single 100 mm wafer in the center of the process chamber shows that 200 sccm gives the highest ashing rate.
Total gas flow rate: tested parameter
Gas mix ratio: 30% nitrogen
Chamber pressure: 1.3 mbar
Power: 1000 W
Processing time: 2 minutes
Temperature (average): 43°C
Full boat:
Test using a boat of 25 100 mm wafers in the center of the process chamber shows that 200 sccm gives the highest ashing rate.
Total gas flow rate: tested parameter
Gas mix ratio: 30% nitrogen
Chamber pressure: 1.3 mbar
Power: 1000 W
Processing time: 10 minutes
Temperature (average): 43°C
Process power for plasma asher 4 & 5
The ashing rate is related to the power used during processing. Higher power increases ashing rate.
Single substrate:
Test using a single 100 mm wafer in the center of the process chamber shows that a power of 1000 W gives the highest ashing rate.
Total gas flow rate: 200 sccm
Gas mix ratio: 30% nitrogen
Chamber pressure: 1.3 mbar
Power: tested parameter
Processing time: 2 minutes
Temperature (average): 43°C
Process temperature for plasma asher 4 & 5
The ashing rate is related to the temperature during processing. Higher temperature increases ashing rate.
Single substrate:
Test using a single 100 mm wafer in the center of the process chamber shows that increasing processing temperature gives increasing ashing rate.
Total gas flow rate: 200 sccm
Gas mix ratio: 30% nitrogen
Chamber pressure: 1.3 mbar
Power: 1000 W
Processing time: 2 minutes
Temperature (average): tested parameter
Plasma Asher 1
Plasma asher 1 was decommissioned 2024-12-02.
Plasma Asher 2
Plasma asher 2 was decommissioned 2024-12-02.
Plasma Asher 3: Descum
The Plasma Asher 3: Descum is dedicated for resist descum, i.e. removal of remains resist traces after development. It has a small chamber, so you can only load a single 100 mm substrate, or a few smaller pieces.
In this machine, only Oxygen and Nitrogen are used for processing.
Typical process parameters:
Process: Photoresist descumming
Pressure: 0.2-0.8 mbar
Gas: 45 sccm O2
Power: 100%
Time: 1 -10 minutes (depending on photoresist type and thickness)
Other materials have not been tested.
The user manual, user APV, and contact information can be found in LabManager - requires login
Process Information
Detailed information about descum processing on Plasma asher 3: Descum can be found here.
Plasma Asher 4
The Plasma Asher 4 can be used for the following processes:
- Photoresist stripping
- Descumming
- Surface cleaning
- Removal of organic passivation layers and masks
Plasma asher 4 has the following material restrictions:
- No metals allowed
- No metal oxides allowed
- No III-V materials allowed
The user manual, risk assessment, and contact information can be found in LabManager - requires login
Process Information
Typical stripping parameters
- Resist: 1.5 µm AZ 5214E
- Substrate: 100 mm Si
- O2: 100 sccm
- N2: 100 sccm
- Pressure (DSC): 1.3 mbar
- Power: 1000 W
- Time (single wafer): 20 minutes
- Time (full boat): 90 minutes
The user manual, user APV, and contact information can be found in LabManager - requires login
Process Information
Plasma Asher 5
The Plasma Asher 5 can be used for the following processes:
- Photoresist stripping
- Descumming
- Surface cleaning
- Removal of organic passivation layers and masks
Furthermore plasma processing using CF4 in plasma asher 5 can be used for:
- Etching of glass and ceramic
- Etching of SiO2, Si3N4, Si
- Removal of polyimide layers
Typical stripping parameters
- Resist: 1.5 µm AZ 5214E
- Substrate: 100 mm Si
- O2: 100 sccm
- N2: 100 sccm
- Pressure (DSC): 1.3 mbar
- Power: 1000 W
- Time (single wafer): 20 minutes
- Time (full boat): 90 minutes
Plasma asher 5 can be used for almost every material, but if you have any doubt if your materials are compatible/allowed in plasma asher 5, feel free to ask the lithography group at Nanolab.
The user manual, risk assessment, and contact information can be found in LabManager - requires login
Process Information
Resist Strip
This resist strip is only for wafers without metal and SU-8.
There are one Remover 1165 bath for stripping and one IPA bath for rinsing.
Here are the main rules for resist strip use:
- Place the wafers in a wafer holder and put them in the first bath for 10 min, this time is depending how much resist you have on the surface.
- After the strip rinse your wafers in the IPA bath for 2-3 min.
- Rinse your wafers for 4-5 min. in running water after stripping.
The user manual and contact information can be found in LabManager: Resist Strip - requires login
Overview of wet bench 06 and 07
| Resist Strip | Lift-off | |
|---|---|---|
| General description | Wet stripping of resist | Lift-off process |
| Chemical solution | NMP Remover 1165 | NMP Remover 1165 |
| Process temperature | Up to 65°C | Up to 65°C |
| Batch size |
1 - 25 wafers |
1 - 25 wafers |
| Size of substrate |
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| Allowed materials |
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All metals except Type IV (Pb, Te) |