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Specific Process Knowledge/Lithography/Strip

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Strip Comparison Table

Equipment Plasma Asher 3: Descum Plasma Asher 4 Plasma Asher 5 Resist strip Lift-off
Purpose

Resist descum

Clean wafers only:
No metal
No metal oxides
No III-V materials

All purposes

Resist strip - no metal lift off!

Lift-off

Method

Plasma ashing

Plasma ashing

Plasma ashing

Solvent and ultra sound

Solvent and ultra sound

Process parameters Process gasses
  • O2 (flow unknown)
  • O2 (0-500 sccm)
  • N2 (0-500 sccm)
  • O2 (0-500 sccm)
  • N2 (0-500 sccm)
  • CF4 (0-200 sccm)
  • NA
  • NA
Max. process power

100 W (100%)

1000 W

1000 W

  • NA
  • NA
Solvent
  • NA
  • NA
  • NA
  • NMP (Remover 1165)
  • Rinse in IPA
  • NMP (Remover 1165)
  • Rinse in IPA
Substrates Batch size
  • 1 small sample
  • 1 50 mm wafer
  • 1 100 mm wafer
  • 1 small sample
  • 1 50 mm wafer
  • 1-25 100 mm wafers
  • 1-25 150 mm wafers
  • 1-25 200 mm wafers
  • 1 small sample
  • 1 50 mm wafer
  • 1-25 100 mm wafers
  • 1-25 150 mm wafers
  • 1-25 200 mm wafers
  • 1 - 25 100 mm wafers
  • 1 - 25 150 mm wafers
  • 1 - 25 100 mm wafers
  • 1 - 25 150 mm wafers
Allowed materials
  • Silicon, glass, and polymer substrates
  • Film or pattern of all but Type IV
  • No metals
  • No metal oxides
  • No III-V materials
  • Silicon, glass, and polymer substrates
  • Film or pattern of photoresist/polymer
  • Silicon, III-V, and glass substrates
  • Film or pattern of all but Type IV
  • No metals
  • No metal oxides
  • Silicon, glass, and polymer substrates
  • Film or pattern of photoresist/polymer
  • Silicon and glass substrates
  • Film or pattern of all but Type IV


Plasma Ashing process parameters

Photoresist stripping Descum after lithography Surface treatment of plastic, ceramic and metal Ashing of organic material
Process pressure 1.3 mbar 1.3 mbar 0.5-1.5 mbar 0.5-1.5 mbar
Process gases
  • O2 (100 sccm)
  • N2 (100 sccm)
  • O2 (100 sccm)
  • N2 (100 sccm)
O2, CF4, N2 or their mixtures O2
Process power 1000 W 200 W 150-1000 W 1000 W or less for heat- sensitive materials
Process time 5-90 minutes 1-30 minutes seconds to minutes Between 0.5 and 20 hours, depending on the material
Batch size 1-25 1-25 1 wafer at a time 1 wafer at a time, use a container, e.g Petri dish



Process gas ratio for plasma asher 4 & 5

 
Ashing rate as function of gas mix ratio when processing a single 100 mm wafer and when processing a full boat with 25 wafers.

The ashing rate is related to the gas mix, usually expressed as percentage of nitrogen of the total amount of gas. Process development tests found that a gas mix of 50% nitrogen gives the highest ashing rate for both processing single substrates and when processing a full boat with 25 substrates.

Please note that the ashing rate for a full boat is approximately ten times slower, than the processing time for a single substrate.

Test setup Single substrate Full boat
Test results Highest ashing rate at 30-80% Nitrogen Highest ashing rate at 50-70% Nitrogen
Wafers 1 25
Wafer size 100 mm 100 mm
Boat position Center of chamber Center of chamber
Test wafer position Center of boat Center of boat
Total gas flow rate 500 200
Gas mix ratio Tested parameter Tested parameter
Chamber pressure 1.25 mbar 1.3 mbar
Power 1000 W 1000 W
Test processing time 2 minutes 10 minutes
Test average temperature 43°C 47°C


Process chamber pressure for plasma asher 4 & 5

 
Ashing rate as function of chamber pressure when processing a single substrate and when processing a full boat with 25 substrates.

The ashing rate is related to the chamber pressure during processing. Process development tests found that 1.3 mbar gives the highest ashing rate for both processing single substrates and when processing a full boat with 25 substrates.

Please note that the ashing rate for a full boat is approximately ten times slower, than the processing time for a single substrate.

Test setup Single substrate Full boat
Test results Highest ashing rate at 1.3 mbar Highest ashing rate at 1.4 mbar
Wafers 1 25
Wafer size 100 mm 100 mm
Boat position Center of chamber Center of chamber
Test wafer position Center of boat Center of boat
Total gas flow rate 150 200
Gas mix ratio 30% N2 30% N2
Chamber pressure Tested parameter Tested parameter
Power 1000 W 1000 W
Test processing time 2 minutes 10 minutes
Test average temperature 43°C 55°C


Process gas flow rate for plasma asher 4 & 5

 
Ashing rate as function of total gas flow when processing a single substrate and when processing a full boat with 25 wafers.

The ashing rate is related to the total gas flow rate during processing. Process development tests found that 200 sccm gives the highest ashing rate for both processing single substrates and when processing a full boat with 25 substrates.

Please note that the ashing rate for a full boat is approximately ten times slower, than the processing time for a single substrate.

Single substrate:
Test using a single 100 mm wafer in the center of the process chamber shows that 200 sccm gives the highest ashing rate.

Total gas flow rate: tested parameter
Gas mix ratio: 30% nitrogen
Chamber pressure: 1.3 mbar
Power: 1000 W
Processing time: 2 minutes
Temperature (average): 43°C

Full boat:
Test using a boat of 25 100 mm wafers in the center of the process chamber shows that 200 sccm gives the highest ashing rate.

Total gas flow rate: tested parameter
Gas mix ratio: 30% nitrogen
Chamber pressure: 1.3 mbar
Power: 1000 W
Processing time: 10 minutes
Temperature (average): 43°C

Process power for plasma asher 4 & 5

 
Ashing rate as function of microwave power.

The ashing rate is related to the power used during processing. Higher power increases ashing rate.

Single substrate:
Test using a single 100 mm wafer in the center of the process chamber shows that a power of 1000 W gives the highest ashing rate.

Total gas flow rate: 200 sccm
Gas mix ratio: 30% nitrogen
Chamber pressure: 1.3 mbar
Power: tested parameter
Processing time: 2 minutes
Temperature (average): 43°C

Process temperature for plasma asher 4 & 5

 
Ashing rate as function of temperature.

The ashing rate is related to the temperature during processing. Higher temperature increases ashing rate.

Single substrate:
Test using a single 100 mm wafer in the center of the process chamber shows that increasing processing temperature gives increasing ashing rate.

Total gas flow rate: 200 sccm
Gas mix ratio: 30% nitrogen
Chamber pressure: 1.3 mbar
Power: 1000 W
Processing time: 2 minutes
Temperature (average): tested parameter

Plasma Asher 1

Plasma asher 1 was decommissioned 2024-12-02.

Information about decommissioned tool can be found here.

Plasma Asher 2

Plasma asher 2 was decommissioned 2024-12-02.

Information about decommissioned tool can be found here.

Plasma Asher 3: Descum

 
Plasma Asher 3: Descum is placed A-5

The Plasma Asher 3: Descum is dedicated for resist descum, i.e. removal of remains resist traces after development. It has a small chamber, so you can only load a single 100 mm substrate, or a few smaller pieces.

In this machine, only Oxygen and Nitrogen are used for processing.

Typical process parameters:
Process: Photoresist descumming
Pressure: 0.2-0.8 mbar
Gas: 45 sccm O2
Power: 100%
Time: 1 -10 minutes (depending on photoresist type and thickness)

Other materials have not been tested.

The user manual, user APV, and contact information can be found in LabManager - requires login

Process Information

Detailed information about descum processing on Plasma asher 3: Descum can be found here.



Plasma Asher 4

 
Plasma asher 4 in cleanroom E-5.

The Plasma Asher 4 can be used for the following processes:

  • Photoresist stripping
  • Descumming
  • Surface cleaning
  • Removal of organic passivation layers and masks


Plasma asher 4 has the following material restrictions:

  • No metals allowed
  • No metal oxides allowed
  • No III-V materials allowed

The user manual, risk assessment, and contact information can be found in LabManager - requires login

Process Information


Typical stripping parameters

  • Resist: 1.5 µm AZ 5214E
  • Substrate: 100 mm Si
  • O2: 100 sccm
  • N2: 100 sccm
  • Pressure (DSC): 1.3 mbar
  • Power: 1000 W
  • Time (single wafer): 20 minutes
  • Time (full boat): 90 minutes


The user manual, user APV, and contact information can be found in LabManager - requires login

Process Information


Plasma Asher 5

 
Plasma asher 5 in cleanroom E-5.

The Plasma Asher 5 can be used for the following processes:

  • Photoresist stripping
  • Descumming
  • Surface cleaning
  • Removal of organic passivation layers and masks


Furthermore plasma processing using CF4 in plasma asher 5 can be used for:

  • Etching of glass and ceramic
  • Etching of SiO2, Si3N4, Si
  • Removal of polyimide layers


Typical stripping parameters

  • Resist: 1.5 µm AZ 5214E
  • Substrate: 100 mm Si
  • O2: 100 sccm
  • N2: 100 sccm
  • Pressure (DSC): 1.3 mbar
  • Power: 1000 W
  • Time (single wafer): 20 minutes
  • Time (full boat): 90 minutes


Plasma asher 5 can be used for almost every material, but if you have any doubt if your materials are compatible/allowed in plasma asher 5, feel free to ask the lithography group at Nanolab.

The user manual, risk assessment, and contact information can be found in LabManager - requires login

Process Information


Resist Strip

 
Resist strip bench in D-3

This resist strip is only for wafers without metal and SU-8.

There are one Remover 1165 bath for stripping and one IPA bath for rinsing.

Here are the main rules for resist strip use:

  • Place the wafers in a wafer holder and put them in the first bath for 10 min, this time is depending how much resist you have on the surface.
  • After the strip rinse your wafers in the IPA bath for 2-3 min.
  • Rinse your wafers for 4-5 min. in running water after stripping.


The user manual and contact information can be found in LabManager: Resist Strip - requires login


Overview of wet bench 06 and 07

Resist Strip Lift-off
General description Wet stripping of resist Lift-off process
Chemical solution NMP Remover 1165 NMP Remover 1165
Process temperature Up to 65°C Up to 65°C
Batch size

1 - 25 wafers

1 - 25 wafers

Size of substrate
  • 100 mm wafers
  • 150 mm wafers
  • 100 mm wafers
  • 150 mm wafers
Allowed materials
  • Silicon
  • Silicon Oxide
  • Silicon Nitride
  • Silicon Oxynitride

All metals except Type IV (Pb, Te)