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Specific Process Knowledge/Lithography/Strip

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Strip Comparison Table

Equipment Plasma Asher 3: Descum Plasma Asher 4 Plasma Asher 5 Resist strip Lift-off
Purpose

Resist descum

Clean wafers only, no metal

All purposes

Resist strip, no metal lift off

Lift-off

Method

Plasma ashing

Plasma ashing

Plasma ashing

Solvent and ultra sound

Solvent and ultra sound

Process parameters Process gasses
  • O2 (flow unknown)
  • O2 (0-500 sccm)
  • N2 (0-500 sccm)
  • O2 (0-500 sccm)
  • N2 (0-500 sccm)
  • CF4 (0-200 sccm)
  • NA
  • NA
Max. process power

100 W (100%)

1000 W

1000 W

  • NA
  • NA
Solvent
  • NA
  • NA
  • NA
  • NMP (Remover 1165)
  • Rinse in IPA
  • NMP (Remover 1165)
  • Rinse in IPA
Substrates Batch size
  • 1 small sample
  • 1 50 mm wafer
  • 1 100 mm wafer
  • 1 small sample
  • 1 50 mm wafer
  • 1-25 100 mm wafers
  • 1-25 150 mm wafers
  • 1-25 200 mm wafers
  • 1 small sample
  • 1 50 mm wafer
  • 1-25 100 mm wafers
  • 1-25 150 mm wafers
  • 1-25 200 mm wafers
  • 1 - 25 100 mm wafers
  • 1 - 25 150 mm wafers
  • 1 - 25 100 mm wafers
  • 1 - 25 150 mm wafers
Allowed materials
  • Silicon, glass, and polymer substrates
  • Film or pattern of all but Type IV
  • No metals allowed - including metal oxides
  • No III-V materials
  • Silicon, glass, and polymer substrates
  • Film or pattern of photoresist/polymer
  • Silicon, III-V, and glass substrates
  • Film or pattern of all but Type IV
  • No metals allowed - including metal oxides
  • Silicon, glass, and polymer substrates
  • Film or pattern of photoresist/polymer
  • Silicon and glass substrates
  • Film or pattern of all but Type IV


Plasma Ashing

Photoresist stripping Descum after lithography Surface treatment of plastic, ceramic and metal Ashing of organic material
Process pressure 0.5-1.5 mbar 0.5-1.5 mbar 0.5-1.5 mbar 0.5-1.5 mbar
Process gases
  • O2 (140 sccm)
  • N2 (60 sccm)
  • O2 (70-210 sccm)
  • N2 (0-70 sccm)
O2, CF4, N2 or their mixtures O2
Process power 1000 W 150-1000 W 150-1000 W 1000 W or less for heat- sensitive materials
Process time 5-90 minutes 1-10 minutes seconds to minutes Between 0.5 and 20 hours, depending on the material
Batch size 1-25 1-25 1 wafer at a time 1 wafer at a time, use a container, e.g Petri dish



Process gas ratio for plasma asher 4 & 5

 
Ashing rate as function of gas mix ratio when processing a single 100 mm wafer and when processing a full boat with 25 wafers.

The ashing rate is related to the gas mix, usually expressed as percentage of nitrogen of the total amount of gas.

Testing found that a gas mix of 50% nitrogen gives the highest ashing rate for both processing single substrates and when processing a full boat with 25 substrates.

Single substrate:
Test using a single 100 mm wafer in the center of the process chamber shows that 30-80% nitrogen gives the highest ashing rate.

Total gas flow rate: 500 sccm
Gas mix ratio: tested parameter
Chamber pressure: 1.25 mbar
Power: 1000 W
Processing time: 2 minutes
Temperature (average): 43°C

Full boat:
Test using a boat of 25 100 mm wafers in the center of the process chamber shows that 50-70% nitrogen gives the highest ashing rate.

Total gas flow rate: 200 sccm
Gas mix ratio: tested parameter
Chamber pressure: 1.3 mbar
Power: 1000 W
Processing time: 5 minutes
Temperature (average): 43°C

Process chamber pressure for plasma asher 4 & 5

 
Ashing rate as function of chamber pressure.

The ashing rate is related to the chamber pressure during processing.

Test using a single 100 mm wafer in the center of the process chamber shows that a chamber pressure of 1.3 mbar gives the highest ashing rate.

Test parameters:
Total gas flow rate: 150 sccm
Gas mix ratio: 30% nitrogen
DSC: tested parameter
Chamber pressure: tested parameter
Power: 1000 W
Processing time: 2 minutes
Temperature (average): 43°C

Process gas flow rate for plasma asher 4 & 5

 
Ashing rate as function of total gas flow when processing a single 100 mm wafer.

The ashing rate is related to the total gas flow rate during processing.

Test using a single 100 mm wafer in the center of the process chamber shows that a total flow rate of 200 sccm gives the highest ashing rate.

Test parameters:
Total gas flow rate: tested parameter
Gas mix ratio: 30% nitrogen
DSC: 1.3 mbar
Chamber pressure: 1.3 mbar
Power: 1000 W
Processing time: 2 minutes
Temperature (average): 43°C

 
Ashing rate as function of total gas flow when processing a full boat of 25 100 mm wafers.

Test using a boat of 25 100 mm wafers in the center of the process chamber shows that a total flow rate of 200 sccm gives the highest ashing rate.

Test parameters:
Total gas flow rate: tested parameter
Gas mix ratio: 30% nitrogen
DSC: 1.3 mbar
Chamber pressure: 1.3 mbar
Power: 1000 W
Processing time: 5 minutes
Temperature (average): 43°C

Process power for plasma asher 4 & 5

 
Ashing rate as function of microwave power.

The ashing rate is related to the power used during processing. Higher power gives higher ashing rate.

Test using a single 100 mm wafer in the center of the process chamber shows that a power of 1000 W gives the highest ashing rate.

Test parameters:
Total gas flow rate: 200 sccm
Gas mix ratio: 30% nitrogen
DSC: 1.3 mbar
Chamber pressure: 1.3 mbar
Power: tested parameter
Processing time: 2 minutes
Temperature (average): 43°C

Process temperature for plasma asher 4 & 5

 
Ashing rate as function of temperature.

The ashing rate is related to the temperature during processing. Higher temperature gives higher ashing rate.

Test using a single 100 mm wafer in the center of the process chamber shows that increasing processing temperature gives increasing ashing rate.

Test parameters:
Total gas flow rate: 200 sccm
Gas mix ratio: 30% nitrogen
DSC: 1.3 mbar
Chamber pressure: 1.3 mbar
Power: 1000 W
Processing time: 2 minutes
Temperature (average): tested parameter

Plasma Asher 1

Plasma asher 1 was decommissioned 2024-12-02.

Information about decommissioned tool can be found here.

Plasma Asher 2

Plasma asher 2 was decommissioned 2024-12-02.

Information about decommissioned tool can be found here.

Plasma Asher 3: Descum

 
Plasma Asher 3: Descum is placed A-5

The Plasma Asher 3: Descum dedicated for resist descum i.e. removal of remains resist traces after development. It has a small chamber, so you can only load a single 100 mm substrate or a few smaller pieces.

In this machine, only O2 and N2 gases are used for processes.

Typical process parameters when operating the equipment:
Process: Photoresist descum
Pressure: 0.2-0.8 mbar
Gas: O2
Power: 50-100%
Time:1 -10 minutes (depending on photoresist type and thickness)

The other materials have not been tested yet.

The user manual, user APV, and contact information can be found in LabManager - requires login

Process Information

Detailed information about descum processing on Plasma asher 3: Descum can be found here.



Plasma Asher 4

 
Plasma asher 4 in cleanroom E-5.

The Plasma Asher 4 can be used for the following processes:

  • Photoresist stripping
  • Descumming
  • Surface cleaning
  • Removal of organic passivation layers and masks


Plasma asher 4 has the following material restrictions:

  • No metals allowed
  • No metal oxides allowed
  • No III-V materials allowed

The user manual, risk assessment, and contact information can be found in LabManager - requires login

Process Information


Typical stripping parameters

  • Resist: 1.5 µm AZ 5214E
  • Substrate: 100 mm Si
  • O2: 140 sccm
  • N2: 60 sccm
  • Pressure (DSC): 1.3 mbar
  • Power: 1000 W
  • Time (single wafer): 20 minutes
  • Time (full boat): 90 minutes


The user manual, user APV, and contact information can be found in LabManager - requires login

Process Information


Plasma Asher 5

 
Plasma asher 5 in cleanroom E-5.

The Plasma Asher 5 can be used for the following processes:

  • Photoresist stripping
  • Descumming
  • Surface cleaning
  • Removal of organic passivation layers and masks


Furthermore plasma processing using CF4 in plasma asher 5 can be used for:

  • Etching of glass and ceramic
  • Etching of SiO2, Si3N4, Si
  • Removal of polyimide layers


Typical stripping parameters

  • Resist: 1.5 µm AZ 5214E
  • Substrate: 100 mm Si
  • O2: 140 sccm
  • N2: 60 sccm
  • Pressure (DSC): 1.3 mbar
  • Power: 1000 W
  • Time (single wafer): 20 minutes
  • Time (full boat): 90 minutes


Plasma asher 5 can be used for almost every material, but if you have any doubt if your materials are compatible/allowed in plasma asher 5, feel free to ask the lithography group at Nanolab.

The user manual, risk assessment, and contact information can be found in LabManager - requires login

Process Information


Resist Strip

 
Resist strip bench in D-3

This resist strip is only for wafers without metal and SU-8.

There are one Remover 1165 bath for stripping and one IPA bath for rinsing.

Here are the main rules for resist strip use:

  • Place the wafers in a wafer holder and put them in the first bath for 10 min, this time is depending how much resist you have on the surface.
  • After the strip rinse your wafers in the IPA bath for 2-3 min.
  • Rinse your wafers for 4-5 min. in running water after stripping.


The user manual and contact information can be found in LabManager: Resist Strip - requires login


Overview of wet bench 06 and 07

Resist Strip Lift-off
General description Wet stripping of resist Lift-off process
Chemical solution NMP Remover 1165 NMP Remover 1165
Process temperature Up to 65°C Up to 65°C
Batch size

1 - 25 wafers

1 - 25 wafers

Size of substrate
  • 100 mm wafers
  • 150 mm wafers
  • 100 mm wafers
  • 150 mm wafers
Allowed materials
  • Silicon
  • Silicon Oxide
  • Silicon Nitride
  • Silicon Oxynitride

All metals except Type IV (Pb, Te)