Specific Process Knowledge/Lithography/Strip

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Strip Comparison Table

Equipment		Plasma asher	Plasma Asher 2	III-V Plasma Asher	Resist strip	Lift-off
Purpose		All purposes	Clean wafers only, no metal	III-V materials only	Resist strip, no metal lift off	Lift-off
Method		Plasma ashing	Plasma ashing	Plasma ashing	Solvent and ultra sound	Solvent and ultra sound
Process parameters	Process gasses	O2 (0 - 400 sccm) N2 CF4	O2 (0 - 400 sccm) N2	O2 (flow unknown)	NA	NA
	Max. process power	1000 W	1000 W	100% (power unknown)	NA	NA
	Solvent	NA	NA	NA	NMP (Remover 1165) Rinse in IPA	NMP (Remover 1165) Rinse in IPA
Substrates	Batch size	1 small sample 1 50 mm wafer 1 - 30 100 mm wafers 1 - 25 150 mm wafers	1 small sample 1 50 mm wafer 1 - 30 100 mm wafers 1 - 25 150 mm wafers	1 small sample 1 50 mm wafer 1 100 mm wafer	1 - 25 100 mm wafers 1 - 25 150 mm wafers	1 - 25 100 mm wafers 1 - 25 150 mm wafers
	Allowed materials	Silicon, glass, and polymer substrates Film or pattern of all but Type IV	No metal! Silicon, glass, and polymer substrates Film or pattern of photoresist/polymer	Silicon, III-V, and glass substrates Film or pattern of all but Type IV	No metal! Silicon, glass, and polymer substrates Film or pattern of photoresist/polymer	Silicon and glass substrates Film or pattern of all but Type IV

Plasma ashing

	Photoresist stripping	Descum after lithography	Surface treatment of plastic, ceramic and metal	Ashing of organic material
Process pressure	0.8- 1.2mbar	0.5- 1.0mbar	0.5- 1.0mbar	0.8-1.5mbar
Process gases	O2 (400 sccm) N2 (0-70 sccm)	O2 (70-210 sccm) N2 (0-70 sccm)	O2, CF4, N2 or their mixtures	O2
Process power	600-1000W	150-300W	150-300W	1000W or less for heat- sensitive materials
Process time	5-60 minutes	1-5 minutes	a few seconds to a few minutes	Between 0.5 and 20 hours, depending on the material
Batch size	1-30	1-10	1 wafer at a time	1 wafer at a time, use a container, e.g Petri dish

A typical process time for stripping of 1.5 µm AZ5214e resist is 15-25 min and for stripping of 9.5 µm AZ4562 resist is 20-35 min with the process parameters: 210 ml O$_{2}$/min or mixture of 210 ml O$_{2}$/min and 70 ml N$_{2}$/min, power 1000 W.

A Descum process in manual mode: O2: 70 sccm, N2: 70 sccm, power: 150 W, time: 10 min. Be sure to wait for cooling if the machine has been used at 1000W right before. At a load at 2 Fused silica wafers resist removed 0.01-01,5 um

Plasma asher

The Plasma Asher 1 is placed in C-1

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The Plasma Asher 1 (TePla 300 auto load model) can be used for the following process:

• Photoresist stripping
• Descumming
• Surface cleaning after storage
• Surface cleaning after processes using oil pump or diffusion pump vacuum
• Surface cleaning as part of photolithography after wet developing of lacquer structures prior to wet or plasma etching
• Stripping of photoresist layers after etching, including after being exposed to high temperatures as after implantation, ion etching, sputter etching, RIE
• Removal of organic passivation layers and masks
• Etching of glass and ceramic
• Etching of SiO$_{2}$, Si$_{3}$N$_{4}$, Si
• Removal of polyimide layers

The machine can be used for almost every materials, but if you have any doubt about your materials are compatible with the plasma process it is better to ask photolithography group at Nanolab.

The user manual, user APV, and contact information can be found in LabManager

Process Information

• SiO2 etch using Plasma Asher 1
• Descum

Plasma Asher 2

Plasma asher for removing AZ resist on 6" wafers: positioned in E-5

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The Plasma Asher 2 is the same as Plasma Asher 1 but has another loading system which is more convenient for batch loading of 6inch substrates.

In this machine, only O2 and N2 gases are used for processes (in PlasmaAsher1, CF4 is used as well).

The typical process parameters when operating the equipment:

• Photeresist stripping

Pressure: 0.8 - 1.0 mbar

Gas: O2

Power: 600 - 1000 watts

Time: 5 -30 min., depending on photoresist type and thickness

A typical process time for stripping of 1.5 um AZ5214e resist is 25 min for 6 wafers load in a boat, recipe 18.

A Descum process in manual mode: O2:70, N2:70, power:150W, time:10 min

Be sure to wait for cooling if the mashine has been used at 1000W right before. At a load at 2 Fused silica wafers resist removed 0.01-01,5um

The other materials have not been tested yet.

The user manual, user APV, and contact information can be found in LabManager

Process Information

• Descum

III-V Plasma Asher

Plasma asher for removing resist on III-V samples: positioned in A-5

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Diener Pico Plasma Asher for III-V materials.

The user manual and contact information can be found in LabManager

Resist Strip

Acetone strip bench in D-3

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This resist strip is only for wafers without metal and SU-8.

There are one Remover 1165 bath for stripping and one IPA bath for rinsing.

Here are the main rules for resist strip use:

• Place the wafers in a wafer holder and put them in the first bath for 10 min, this time is depending how much resist you have on the surface.
• After the strip rinse your wafers in the IPA bath for 2-3 min.
• Rinse your wafers for 4-5 min. in running water after stripping.

The user manual and contact information can be found in LabManager: Resist Strip

Overview of wet bench 06 and 07

	Resist Strip	Lift-off
General description	wet stripping of resist	lift-off process
Chemical solution	NMP Remover 1165	NMP Remover 1165
Process temperature	Up to 60 oC	Up to 60 oC
Batch size	1-25 wafers at a time	1-25 wafer at a time
Size of substrate	4" wafers 6" wafers	4" wafers 6" wafers
Allowed materials	Silicon Silicon Oxide Silicon Nitride Silicon Oxynitride	All metals