LabAdviser/314/Microscopy 314-307/FIB/Hydra
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Helios 5 Hydra UX DualBeam
Reading Materials
Technical Notes
Resolution
- Electron beam:
- At optimum WD: 0.7 nm at 1 kV • 1.0 nm at 500 V (ICD)
- At coincident point: 0.6 nm at 15 kV • 1.2 nm at 1 kV
- Xe Ion beam resolution at coincident point:
- <20 nm at 30 kV using preferred statistical method
- <10 nm at 30 kV using selective edge method
Attachments
- PFIB column with unique inductively coupled plasma (ICP) source supporting four ion species with fast switching capability. Ion species available: Xe, Ar, O, N
- MultiChem Gas Injection System (GIS) (for W and Pt both E and I beams. C deposition E beam only. XeF2 and H2O etching Ion beam only. Check this)
- Thermo Scientific EasyLift™ NanoManipulator for precise in situ sample manipulation
- Everhart-Thornley SE detector (ETD)
- In-chamber electron and ion detector (ICE) for secondary ions (SI) and electrons (SE)
- EDS detector
- In-chamber Nav-Cam Sample Navigation Camera
- Integrated plasma cleaner
May have: (need to check)
- Thermo Scientific CryoCleaner Decontamination Device
- WDS
- EBSD
- Retractable low-voltage, high-contrast directional solid-state backscatter electron detector (DBS)
- Elstar Column in-lens SE/BSE detector (TLD-SE, TLD-BSE)
- Elstar Column in-column SE/BSE detector (ICD)*
To find the basic instructions for operating the instrument, the reader is referred to the labmanager manual.
Important Notes
- ALWAYS make sure the EDS (and EBSD relevant?) detectors are RETRACTED when opening and closing the chamber.
- Do NOT adjust the Nitrogen regulator!!! Relevant?
- Always open and close the chamber GENTLY whilst viewing the live CCD image.
- Only home the stage with open door or if in vacuum only with holders that you are 100% sure it is safe to do so.
- Make sure you delete all saved positions before finishing your microscope section.
- When moving between saved positions, BE CAREFUL! If you are unsure move the Z height to the lowest point and lock it so as not to collide with the pole piece.
- Use the logbook
- NEVER work without a valid link between the Z and the FWD
- ONLY INSERT EBSD CAMERA if the sample is at the correct position (in case of a special EBSD holder the stage must be tilted to 16 °). Relevant?
- Always use GLOVES. Only vacuum-ready samples and holders are allowed inside the chamber.
- DO NOT install ANY software on either the microscope or support PC,.
- Transfer your files at the end of each session. We will be deleting files from the support computer without notice.