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Specific Process Knowledge/Thermal Process/Dope with Phosphorus: Difference between revisions

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* RCA cleaning of the test wafer (p-type, 1-20 Ωcm) and the dummy wafers
* RCA cleaning of the test wafer (p-type, 1-20 Ωcm) and the dummy wafers
* Phosphorus pre-deposition in the Phosphorus Pre-dep furnace (A4).  
* Phosphorus pre-deposition in the Phosphorus Pre-dep furnace (A4).  
** Recipe: "POCLNEW"
** Recipe: "POCL900"
** Temperature: 900 °C
** Temperature: 900 °C
** Time: 15 min phosphorus pre-dep and 20 min annealing/N<sub>2</sub> post purge
** Time: 15 min phosphorus pre-dep and 20 min annealing/N<sub>2</sub> post purge
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The sheet resistance was 54 Ωsq in the center of the wafer and 45-48 Ωsq in the edge of the wafer. This correspond quite good to the results that previously had been obtained for the furnace as can be seen on this LabAdviser page.
The sheet resistance was 54 Ωsq in the center of the wafer and 45-48 Ωsq in the edge of the wafer. This correspond quite good to the results that previously had been obtained for the furnace as can be seen on this LabAdviser page.


====Notes about the "POCLNEW" recipe====
====Notes about the POCL recipes====


A new recipe called "POCLNEW" was made, after the POCl<sub>3</sub> line was modified. The N<sub>2</sub> high flow (3 SLM) is on all the time through the recipe. There is a 2 min pre-purge with first N2 low (150 sccm) through the POCl3 bubbler, i.e. with the valves v4a and v4b closed, and then with O2 (0.50 SLM), before the pre-deposition time starts. After the pre-deposition, an N2 low post-purge (500 sccm) is done for 2 minutes with v4a and v4b closed.  
A new recipe for POCL doping called was made, after the POCl<sub>3</sub> line was modified. The N<sub>2</sub> high flow (3 SLM) is on all the time through the recipe. There is a 2 min pre-purge with first N2 low (150 sccm) through the POCl3 bubbler, i.e. with the valves v4a and v4b closed, and then with O2 (0.50 SLM), before the pre-deposition time starts. After the pre-deposition, an N2 low post-purge (500 sccm) is done for 2 minutes with v4a and v4b closed.  
    
    
For safety reasons it is important that the POCl<sub>3</sub> is completely removed from the furnace, before it is opened to load or unload wafers.  
For safety reasons it is important that the POCl<sub>3</sub> is completely removed from the furnace, before it is opened to load or unload wafers.