Specific Process Knowledge/Thin film deposition/Deposition of Silicon Oxide/Deposition of Silicon Oxide using PECVD: Difference between revisions
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=Recipes on PECVD2 for deposition of silicon oxides= | =Recipes on PECVD2 for deposition of silicon oxides= | ||
See [[Specific Process Knowledge/III-V Process/thin film dep/pecvd2| here]] | See [[Specific Process Knowledge/III-V Process/thin film dep/pecvd2| here]] | ||
==Quality control recipe== | |||
{| border="1" cellspacing="2" cellpadding="2" colspan="3" | |||
|bgcolor="#98FB98" |'''Quality Controle (QC) for PECVD2''' | |||
|- | |||
| | |||
*[http://labmanager.danchip.dtu.dk/d4Show.php?id=1988&mach=17 The QC procedure for PECVD2]<br> | |||
*[http://labmanager.danchip.dtu.dk/function.php?module=Machine&view=view&mach=17 The newest QC data for PECVD2] | |||
{| {{table}} | |||
| align="center" | | |||
{| border="1" cellspacing="1" cellpadding="2" align="center" style="width:300px" | |||
! QC Recipe: | |||
! QCTOXIDE | |||
|- | |||
| SiH<sub>4</sub> flow | |||
|12 sccm | |||
|- | |||
|N<sub>2</sub>O flow | |||
|710 sccm | |||
|- | |||
|N<sub>2</sub> flow | |||
|392 sccm | |||
|- | |||
|Pressure | |||
|550 mTorr | |||
|- | |||
|RF-power | |||
|100 W @380kHz | |||
|- | |||
|Deposition time | |||
|1 min | |||
|} | |||
| align="center" valign="top"| | |||
{| border="2" cellspacing="1" cellpadding="2" align="center" style="width:500px" | |||
!QC limits | |||
!PECVD2 | |||
|- | |||
|Depostion rate of Silicon Oxide | |||
|69nm/min - 119nm/min | |||
|- | |||
|Non-uniformity of the deposition rate (std. deviation of 9 points) | |||
|0 - 2.8 nm | |||
|- | |||
|Refractive index of the Silicon Oxide | |||
|1.41 - 1.53 | |||
|- | |||
|Non-uniformity of the refrative index (std. deviation of 9 points) | |||
|0 - 0.07 | |||
|- | |||
|} | |||
|- | |||
|} | |||
|} | |||
==SiO2 Standard, High Rate== | |||
{| border="1" style="text-align: center; width: 400px; height: 150px;" | |||
! colspan="2" style="text-align: center;" style="background: #efefef;" | SiO2 Standard | |||
|- | |||
!N<math>_2</math>O-flow | |||
|1600 sccm | |||
|- | |||
!SiH<math>_4</math>-flow | |||
|17 sccm | |||
|- | |||
!RF-power (380 kHz) | |||
|380 W | |||
|- | |||
!Process Pressure | |||
|400 mTorr | |||
|- | |||
!Deposition rate | |||
|179 nm/min | |||
|- | |||
!index of refraction | |||
|1.461 | |||
|} | |||
==SiO2 Standard, Low Rate== | |||
{| border="1" style="text-align: center; width: 700px; height: 150px;" | |||
! colspan="2" style="text-align: left;" style="background: #efefef;" | 1STOxide | |||
! colspan="2" style="text-align: left;" style="background: #efefef;" | A test recipe | |||
|- | |||
!N<math>_2</math>-flow | |||
|392 sccm | |||
|392 sccm | |||
|- | |||
!N<math>_2</math>O-flow | |||
|1420 sccm (setting in software is 710 sccm) | |||
|1420 sccm (setting in software is 710 sccm) | |||
|- | |||
!SiH<math>_4</math>-flow | |||
|12 sccm | |||
|12 sccm | |||
|- | |||
!RF-power | |||
|100 W | |||
|150 W | |||
|- | |||
!Process Pressure | |||
|550 mTorr | |||
|700 mTorr | |||
|- | |||
!Deposition rate | |||
|~100 nm/min | |||
|109 ± 2 nm/min [tested: 2014-03-18] | |||
|- | |||
!index of refraction | |||
|1.47 | |||
|1.465 [tested: 2014-03-18] | |||
|- | |||
!Uniformity | |||
|<1 % | |||
|3.2% over the wafer [tested: 2014-03-18] | |||
|} | |||
===Deposition rate as a function of deposition time using 1STOxide:=== | |||
{| border="1" style="text-align: center; width: 400px; height: 150px;" | |||
|- | |||
| | |||
Deposition time [s] | |||
|Oxide thickness [nm] | |||
|Expected naturally grown oxide [nm] | |||
|Deposition rate [nm/min] | |||
|- | |||
|15 | |||
|26.9 | |||
|2 | |||
|99.6 | |||
|- | |||
|30 | |||
|51.9 | |||
|2 | |||
|99.8 | |||
|- | |||
|60 | |||
|102.4 | |||
|2 | |||
|100.4 | |||
|- | |||
|60 | |||
|102.7 | |||
|2 | |||
|100.7 | |||
|- | |||
|120 | |||
|201.1 | |||
|2 | |||
|99.6 | |||
|} | |||
===Thickness uniformity of test wafer using the test recipe=== | |||
[[image:PECVD2 SiO2 Test20 wafer map.jpg|350x350px|left|thumb|Thickness uniformity of test wafer using the test recipe.]] | |||
<br clear="all" /> | |||
==Silicon nitride== | |||
{| border="1" cellspacing="0" cellpadding="7" | |||
|- | |||
|Recipe name | |||
|SiH4 flow [sccm] | |||
|NH3 flow [sccm] | |||
|N2 flow [sccm] | |||
|Pressure [mTorr] | |||
|Power [W] | |||
|Description | |||
|- | |||
|1nitride | |||
|30 | |||
|20 | |||
|1000 | |||
|500 | |||
|80 | |||
| | |||
|- | |||
|} | |||
=Recipes on PECVD3 for deposition of silicon oxides= | =Recipes on PECVD3 for deposition of silicon oxides= | ||