LabAdviser/314/Microscopy 314-307/TEM/T20: Difference between revisions
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'''Feedback to this page''': '''[mailto:labadviser@nanolab.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.nanolab.dtu.dk/index.php?title=LabAdviser/314/Microscopy_314-307/TEM/T20 click here]''' | '''Feedback to this page''': '''[mailto:labadviser@nanolab.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.nanolab.dtu.dk/index.php?title=LabAdviser/314/Microscopy_314-307/TEM/T20 click here]''' | ||
''This section is written by DTU Nanolab internal if nothing else is stated.'' | |||
[[Category:314]] | [[Category:314]] | ||
[[Category:314-Microscopy]] | [[Category:314-Microscopy]] | ||
[[File:IMG_2076.JPG|400x400px|right|thumb|Tecnai T20 in building 314.]] | [[File:IMG_2076.JPG|400x400px|right|thumb|Tecnai T20 in building 314.]] | ||
= FEI Tecnai T20 = | = FEI Tecnai T20 = | ||
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On the analytical side, the microscope is equipped with an Oxford X-Max 80T SDD X-ray detector for Energy Dispersive X-ray (EDS) spectroscopy and a Gatan Tridiem 863 imaging filter allowing for electron energy-loss spectroscopy (EELS) and energy-filtered imaging (EF-TEM). For imaging, the microscope is equipped with TVIPS XF416 CMOS (4096x4096 px) before the the energy filter and a GATAN Ultrascan US1000 (2048x2048 px) after the energy filter.<br /> | On the analytical side, the microscope is equipped with an Oxford X-Max 80T SDD X-ray detector for Energy Dispersive X-ray (EDS) spectroscopy and a Gatan Tridiem 863 imaging filter allowing for electron energy-loss spectroscopy (EELS) and energy-filtered imaging (EF-TEM). For imaging, the microscope is equipped with TVIPS XF416 CMOS (4096x4096 px) before the the energy filter and a GATAN Ultrascan US1000 (2048x2048 px) after the energy filter.<br /> | ||
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== TEM Schematic == | == TEM Schematic == | ||
A general schematic of a transmission electron microscope can be found [[/Schematic|here]] | A general schematic of a transmission electron microscope can be found [[/Schematic|here]] | ||
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== Sample holders == | == Sample holders == | ||
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== Who may operate the Tecnai T20 == | == Who may operate the Tecnai T20 == | ||
Anybody in need of a TEM microscope is welcome to apply for access to our facility by submitting an [ | Anybody in need of a TEM microscope is welcome to apply for access to our facility by submitting an [https://www.nanolab.dtu.dk/use-nanolab/use-of-our-facilities Access Request Form ].Shortly after your ARF has been received you will be contact by the microscopy support team in order to set up a meeting to further discuss your application.<br /> | ||
In order to be authorised to use the Tecnai T20 you must complete the Tecnai training with consists of a theoretical lecture and 3 practical sessions of 4 hours each.<br /> | In order to be authorised to use the Tecnai T20 you must complete the Tecnai training with consists of a theoretical lecture and 3 practical sessions of 4 hours each.<br /> | ||
Due to the similarity of the basic operations on a Tecnai TEM and a Titan TEM, a Tecnai trained user can receive additional training and progress in using a Titan TEM.<br /> | Due to the similarity of the basic operations on a Tecnai TEM and a Titan TEM, a Tecnai trained user can receive additional training and progress in using a Titan TEM.<br /> | ||
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*[[LabAdviser/314/Microscopy 314-307/Technique/EELS|EELS]] | *[[LabAdviser/314/Microscopy 314-307/Technique/EELS|EELS]] | ||
*[[LabAdviser/314/Microscopy 314-307/Technique/EFTEM|EFTEM]] | *[[LabAdviser/314/Microscopy 314-307/Technique/EFTEM|EFTEM]] | ||
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= Tips and Tricks = | = Tips and Tricks = | ||
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Here you can find some help to solve small issues on the microscope. Let us know, if you have other suggestions. | Here you can find some help to solve small issues on the microscope. Let us know, if you have other suggestions. | ||
*[[LabAdviser/314/Microscopy 314-307/TEM/Tips/MagicSwitch|Magic Switch is not working properly]] | |||
*[[LabAdviser/314/Microscopy 314-307/TEM/Tips/TVIPS camera|TVIPS camera]] | |||
*[[LabAdviser/314/Microscopy 314-307/TEM/Tips/Aztec|Aztec connection problems]] | |||
*[[LabAdviser/314/Microscopy 314-307/TEM/Tips/GIF-apertures|GIF apertures are not responding]] | |||
*[[LabAdviser/314/Microscopy 314-307/TEM/Tips/HAADF-detector|HAADF detector doesn't give a signal]] | |||
*[[LabAdviser/314/Microscopy 314-307/TEM/Tips/No-STEM|No buttons for STEM acquisition]] | |||
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= Reference material = | = Reference material = | ||