LabAdviser/314/Microscopy 314-307/TEM/ETEM: Difference between revisions

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 <!-- <span style="background:#FF2800">THIS PAGE IS UNDER CONSTRUCTION</span>[[image:Under_construction.png|200px]] -->
-'''Feedback to this page''': '''[mailto:labadviser@nanolab.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.nanolab.dtu.dk/index.php?title=LabAdviser/314/TEM/ETEM click here]'''
+'''Feedback to this page''': '''[mailto:labadviser@nanolab.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.nanolab.dtu.dk/index.php?title=LabAdviser/314/Microscopy_314-307/TEM/ETEM click here]'''
+''This section is written by DTU Nanolab internal if nothing else is stated.''
 [[Category:314]]
 [[Category:314-Microscopy]]
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 = FEI Titan 80-300 ETEM =
-The Titan ETEM is a transmission electron microscopy equipped with a field emission electron source, a monochromator and an aberration corrector on the objective lens. This gives the microscope a resolution of about 0.8Å in TEM mode. Other tecniques available on the microscope are scanning transmission electron microscopy (STEM, resolution 1.4 Å) with both high-angle annular dark-field (HAADF) and bright-field (BF) detectors. On the analytical side, the microscope is equipped with Oxford X-Max 80T SDD X-ray detector for Energy Dispersive X-ray (EDX) spectroscopy and Gatan Tridiem 966 imaging filter allowing for electron energy-loss spectroscopy (EELS) and energy-filtered imaging (EFTEM). For imaging, the microscope is equipped with Gatan US1000 cameras before and after the energy filter, as well as a Gatan OneView camera for fast ''in situ'' acquisition (25fps full resolution 4k x 4k, 100fps 2k x 2k, 200fps 1k x 1k).<br />
+The Titan ETEM is a transmission electron microscopy equipped with a field emission electron source (FEI X-FEG), a monochromator and an aberration corrector on the super-twin (S-TWIN) objective lens (CEOS CESCOR). This gives the microscope a resolution of about 0.8 Å in TEM mode. Other tecniques available on the microscope are scanning transmission electron microscopy (STEM, resolution 1.4 Å) with both high-angle annular dark-field (HAADF) and dark-field (DF)/bright-field (BF) detectors. On the analytical side, the microscope is equipped with Oxford X-Max 80T SDD X-ray detector for energy dispersive X-ray (EDS) spectroscopy and Gatan Tridiem 866 imaging filter allowing for electron energy-loss spectroscopy (EELS) and energy-filtered imaging (EF-TEM). For imaging, the microscope is equipped with Gatan US1000 cameras (2048x2048 px) before and after the energy filter, as well as a [[LabAdviser/314/Microscopy 314-307/TEM/ETEM/OneView|Gatan OneView camera]] for fast ''in situ'' acquisition (25fps full resolution 4k x 4k, 100fps 2k x 2k, 200fps 1k x 1k, 300fps 512 x 512).<br />
 The microscope is equipped with a differential pumping system which allows gases to be introduced around the sample to a pressure on the order of 10 mbar (gas specie dependent). Several gases are permanently mounted on the system: Hydrogen, helium, methane carbon monoxide, nitrogen and oxygen. Additional gases and gas mixtures can be added as needed. Please contact Cen staff if you need other gases. [[image:Titan-etem-211113.jpg|400x400px|right|thumb|Schematic of the Titan ETEM differential pumping system.]]<br />
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 == Sample holders ==
-All TEM sample holders available at DTU Nanolab building 314/307 are compatible with the Titan ETEM. The lab has holders for heating (furnace and MEMS-based), cooling, biasing and tomography. For information on the holder see [[LabAdviser/CEN/Sample Holders|HERE]].
+All TEM sample holders available at DTU Nanolab building 314/307 are compatible with the Titan ETEM. The lab has holders for heating (furnace and MEMS-based), cooling, biasing and tomography. For information on the holder see [[LabAdviser/314/Microscopy 314-307/TEM/Sample Holders|HERE]].
 == Who may operate the Titan ETEM ==
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 [http://labmanager.dtu.dk/function.php?module=Machine&view=view&mach=350  Titan ETEM in LabManager]
+= Calibration =
-= Calibration =
+*[[media:ETEM_collection-angles.xlsx‎ |GIF collection angles (20220209)]]
 *Magnification calibration cameras
-*Collection angles GIF
 *Convergence angles STEM
 = Process information =
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 Techniques:
-*[[LabAdviser/314/Technique/EDS|EDS/WDS]]
+*[[LabAdviser/314/Microscopy 314-307/Technique/X-ray_spectroscopy|EDS/WDS]]
-*[[LabAdviser/314/Technique/EELS|EELS]]
+*[[LabAdviser/314/Microscopy 314-307/Technique/EELS|EELS]]
-*[[LabAdviser/314/Technique/EFTEM|EFTEM]]
+*[[LabAdviser/314/Microscopy 314-307/Technique/EFTEM|EFTEM]]
+*[[LabAdviser/314/Microscopy 314-307/Technique/Holo|Holography]]
 Processes:
 *Oxidation/Reduction of metal particles
+<br />
 = Tips and Tricks =
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 Here you can find some help to solve small issues on the microscope. Let us know, if you have other suggestions.
+*[[LabAdviser/314/Microscopy 314-307/TEM/Tips/MagicSwitch|Magic Switch is not working properly]]
-*[[LabAdviser/314/TEM/ETEM/dose-calibration|Set dose calibration for OneView]]
+*[[LabAdviser/314/Microscopy 314-307/TEM/ETEM/OneView|Description OneView camera]]
-*[[LabAdviser/314/TEM/ETEM/GIF-apertures|GIF apertures are not responding]]
+*[[LabAdviser/314/Microscopy 314-307/TEM/Tips/Aztec|Aztec connection problems]]
+*[[LabAdviser/314/Microscopy 314-307/TEM/Tips/GIF-apertures|GIF apertures are not responding]]
+*[[LabAdviser/314/Microscopy 314-307/TEM/Tips/HAADF-detector|HAADF detector doesn't give a signal]]
+*[[LabAdviser/314/Microscopy 314-307/TEM/Tips/No-STEM|No buttons for STEM acquisition]]