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'''Feedback to this page''': '''[mailto:labadviser@nanolab.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.nanolab.dtu.dk/index.php/Specific_Process_Knowledge/Characterization click here]''' <br> | |||
==Overview of characteristics and where to measure it== | |||
{| {{table } } | |||
| width="30" align="center" style="writing-mode: vertical-lr; transform: rotate(180deg);background:#f0f0f0;"| | |||
| width="30" align="center" style="writing-mode: vertical-lr; transform: rotate(180deg);background:#f0f0f0;"|[[Specific_Process_Knowledge/Characterization/Optical_microscope| Optical Microscopes]] | |||
| width="30" align="center" style="writing-mode: vertical-lr; transform: rotate(180deg);background:#f0f0f0;"|[[Specific Process Knowledge/Characterization/SEM: Scanning Electron Microscopy|SEM (incl. EDX)]] | |||
| width="30" align="center" style="writing-mode: vertical-lr; transform: rotate(180deg);background:#f0f0f0;"|[[Specific Process Knowledge/Characterization/AFM: Atomic Force Microscopy|AFM]] | |||
| width="30" align="center" style="writing-mode: vertical-lr; transform: rotate(180deg);background:#f0f0f0;"|[[Specific Process Knowledge/Characterization/Topographic measurement#Comparison of Stylus Profilers, Optical Profilers and AFMs at Nanolab|Stylus profilers]] | |||
| width="30" align="center" style="writing-mode: vertical-lr; transform: rotate(180deg);background:#f0f0f0;"|[[Specific_Process_Knowledge/Characterization/Topographic_measurement#Comparison of Stylus Profilers, Optical Profilers and AFMs at Nanolab|Optical profilers]] | |||
| width="30" align="center" style="writing-mode: vertical-lr; transform: rotate(180deg);background:#f0f0f0;"|[[Specific_Process_Knowledge/Characterization/Optical_characterization#Filmtek_4000|Filmtek (reflectometer)]] | |||
| width="30" align="center" style="writing-mode: vertical-lr; transform: rotate(180deg);background:#f0f0f0;"|[[Specific_Process_Knowledge/Characterization/Optical_characterization#Ellipsometer|Ellipsometer]] | |||
| width="30" align="center" style="writing-mode: vertical-lr; transform: rotate(180deg);background:#f0f0f0;"|[[Specific_Process_Knowledge/Characterization/Thickness_Measurer|Thickness stylus]] | |||
| width="30" align="center" style="writing-mode: vertical-lr; transform: rotate(180deg);background:#f0f0f0;"|[[Specific_Process_Knowledge/Characterization/XPS|XPS]] | |||
| width="30" align="center" style="writing-mode: vertical-lr; transform: rotate(180deg);background:#f0f0f0;"|[[Specific_Process_Knowledge/Characterization/PL_mapper|PL mapper]] | |||
| width="30" align="center" style="writing-mode: vertical-lr; transform: rotate(180deg);background:#f0f0f0;"|[[Specific Process Knowledge/Characterization/Four-Point Probe|4-point probe]] | |||
| width="30" align="center" style="writing-mode: vertical-lr; transform: rotate(180deg);background:#f0f0f0;"|[[Specific_Process_Knowledge/Characterization/Probe_station|Probe station]] | |||
| width="30" align="center" style="writing-mode: vertical-lr; transform: rotate(180deg);background:#f0f0f0;"|[[Specific_Process_Knowledge/Characterization/XRD|XRD]] | |||
| width="30" align="center" style="writing-mode: vertical-lr; transform: rotate(180deg);background:#f0f0f0;"|[[Specific_Process_Knowledge/Characterization/Lifetime_scanner_MDPmap|Life time scanner]] | |||
| width="30" align="center" style="writing-mode: vertical-lr; transform: rotate(180deg);background:#f0f0f0;"|[[Specific_Process_Knowledge/Characterization/Drop_Shape_Analyzer|Drop shape analyser]] | |||
| width="30" align="center" style="writing-mode: vertical-lr; transform: rotate(180deg);background:#f0f0f0;"|[[Specific_Process_Knowledge/Characterization/Hardness_measurement|Hardness tester]] | |||
| width="30" align="center" style="writing-mode: vertical-lr; transform: rotate(180deg);background:#f0f0f0;"|[[Specific Process Knowledge/Characterization/Particle Scanner Takano|Particle scanner]] | |||
| width="30" align="center" style="writing-mode: vertical-lr; transform: rotate(180deg);background:#f0f0f0;"|IR-camera | |||
| width="30" align="center" style="writing-mode: vertical-lr; transform: rotate(180deg);background:#f0f0f0;"|[[Specific Process Knowledge/Characterization/III-V_ECV-profiler|III-V ECV-profiler]] | |||
| width="30" align="center" style="writing-mode: vertical-lr; transform: rotate(180deg);background:#f0f0f0;"|[[Specific Process Knowledge/Characterization/MicroSpectroPhotometer (Craic 20/30 PV)|Microspectrophotometer (Craic 20/30 PV)]] | |||
|- | |||
|-style="background:#DCDCDC;" align="center" | |||
|align="left"| Breakdown voltage | |||
||||||||||||||||||||||||||||||||||||||| | |||
|- | |||
|-style="background:#C0C0C0;" align="center" | |||
|align="left"| Carrier density/doping profile | |||
|||||||||||||||||||||||||||||||||||||x|| | |||
|- | |||
|-style="background:#DCDCDC;" align="center" | |||
|align="left"| Charge carrier life time||||||||||||||||||||||||||||x|||||||||||| | |||
|- | |||
|-style="background:#C0C0C0;" align="center" | |||
|align="left"| Contact angle hydrophobic/hydrophillic||||||||||||||||||||||||||||||x|||||||||| | |||
|- | |||
|-style="background:#DCDCDC;" align="center" | |||
|align="left"| Crystallinity||||||||||||||||||||||||||x|||||||||||||| | |||
|- | |||
|-style="background:#C0C0C0;" align="center" | |||
|align="left"| Deposition uniformity||||||||||x||x||x|||||||||||||||||||||||||| | |||
|- | |||
|-style="background:#DCDCDC;" align="center" | |||
|align="left"|[[Specific_Process_Knowledge/Characterization/Sample_imaging|Dimensions(in plane)]]||x||x||(x)||(x)||x||||||||||||||||||||||||||||||x | |||
|- | |||
|-style="background:#C0C0C0;" align="center" | |||
|align="left"|[[Specific_Process_Knowledge/Characterization/Topographic_measurement|Dimensions(height)/Topography]]||(x)||(x)||x||x||x|||||||||||||||||||||||||||||| | |||
|- | |||
|-style="background:#DCDCDC;" align="center" | |||
|align="left"| Electrical conductivity||||||||||||||||||||||||x|||||||||||||||| | |||
|- | |||
|-style="background:#C0C0C0;" align="center" | |||
|align="left"| [[Specific_Process_Knowledge/Characterization/Element_analysis|Element analysis]]||||x||||||||||||||x||x <sup>{{fn|4}}</sup>||||||x <sup>{{fn|4}}</sup>|||||||||||||| | |||
|- | |||
|-style="background:#DCDCDC;" align="center" | |||
|align="left"| [[Specific_Process_Knowledge/Characterization/Stress_measurement|Film stress]]||||||||x||||||||||||||||||x <sup>{{fn|7}}</sup>|||||||||||||| | |||
|- | |||
|-style="background:#C0C0C0;" align="center" | |||
|align="left"|[[Specific_Process_Knowledge/Characterization/Sample_imaging|Imaging]]||x||x||x||||x||||||||||||||||||||||||||||||x | |||
|- | |||
|-style="background:#DCDCDC;" align="center" | |||
|align="left"| [[Specific_Process_Knowledge/Characterization/Hardness_measurement|Material Hardness]]||||||||||||||||||||||||||||||||x|||||||| | |||
|- | |||
|-style="background:#C0C0C0;" align="center" | |||
|align="left"| Band gap||||||||||||||x||||x||x|||||||||||||||||||| | |||
|- | |||
|-style="background:#DCDCDC;" align="center" | |||
|align="left"| Particles||x||x||x||||||||||||||||||||||||||||x||||||x | |||
|- | |||
|-style="background:#C0C0C0;" align="center" | |||
|align="left"| Phase changes|||||||||||||||||||||||||||||||||||||||| | |||
|- | |||
|-style="background:#DCDCDC;" align="center" | |||
|align="left"| Reflectivity||||||||||||x||x||||||x <sup>{{fn|6}}</sup>||||||||||||||||||||x | |||
|- | |||
|-style="background:#C0C0C0;" align="center" | |||
|align="left"| [[Specific_Process_Knowledge/Characterization/Measurement_of_film_thickness_and_optical_constants|Refractive index]]||||||||||||x||x|||||||||||||||||||||||||| | |||
|- | |||
|-style="background:#DCDCDC;" align="center" | |||
|align="left"| Resistivity||||||||||||||||||||||x|||||||||||||||||| | |||
|- | |||
|-style="background:#C0C0C0;" align="center" | |||
|align="left"| Step coverage||x <sup>{{fn|1}}</sup>||x <sup>{{fn|1}}</sup>|||||||||||||||||||||||||||||||||||| | |||
|- | |||
|-style="background:#DCDCDC;" align="center" | |||
|align="left"| Surface roughness||||||x||x||x||||||||||||||||x|||||||||||||| | |||
|- | |||
|-style="background:#C0C0C0;" align="center" | |||
|align="left"| Thermal conductivity|||||||||||||||||||||||||||||||||||||||| | |||
|- | |||
|-style="background:#DCDCDC;" align="center" | |||
|align="left"| [[Specific_Process_Knowledge/Characterization/Measurement_of_film_thickness_and_optical_constants|Thin film thickness]]||x <sup>{{fn|1}}</sup>||x <sup>{{fn|1}}</sup>||x <sup>{{fn|2}}</sup>||x <sup>{{fn|2}}</sup>||x ||x||x||||||x <sup>{{fn|5}}</sup>||x <sup>{{fn|3}}</sup>||||x|||||||||||||| | |||
|- | |||
|-style="background:#C0C0C0;" align="center" | |||
|align="left"| Voids in wafer bonding||x||||||||||||||||||x||||||||||||||||x|||| | |||
|- | |||
|-style="background:#DCDCDC;" align="center" | |||
|align="left"| [[Specific_Process_Knowledge/Characterization/Thickness_Measurer|Wafer thickness]]||x <sup>{{fn|1}}</sup>||x <sup>{{fn|1}}</sup>||||||||||||x|||||||||||||||||||||||| | |||
|- | |||
|-style="background:#C0C0C0;" align="center" | |||
|align="left"| Work function||||||||||||||||||x|||||||||||||||||||||| | |||
|- | |||
|} | |||
<br clear="all"> | |||
<sup>{{fn|1}}</sup> Using the cross section method<br> | |||
<sup>{{fn|2}}</sup> Using the create step method<br> | |||
<sup>{{fn|3}}</sup> With known resistivity<br> | |||
<sup>{{fn|4}}</sup> Composition information for crystalline materials<br> | |||
<sup>{{fn|5}}</sup> Only single layer<br> | |||
<sup>{{fn|6}}</sup> Good for characterization of VCSEL structures and DBR mirrors<br> | |||
<sup>{{fn|7}}</sup> Only for crystalline films<br> | |||
== Choose characterization topic == | |||
*[[Specific Process Knowledge/Characterization/III-V_ECV-profiler|Carrier density (doping) profiler]] | |||
*[[Specific_Process_Knowledge/Characterization/Drop_Shape_Analyzer|Contact angle measurement]] | |||
*[[/Element analysis|Element analysis]] | |||
*[[/Measurement of film thickness and optical constants|Film thickness and optical constants]] | |||
*[[/Hardness measurement|Hardness measurement]] | |||
*[[/PL mapper|Photoluminescence mapping]] | |||
*[[/Four-Point_Probe|Four-Point Probe (Resistivity measurement)]] <!-- [[/Resistivity measurement|Resistivity measurement]] --> | |||
*[[/Sample imaging|Sample imaging]] | |||
*[[/Sample preparation|Sample preparation for inspection]] | |||
*[[Specific Process Knowledge/Characterization/SEM: Scanning Electron Microscopy|Scanning Electron Microscopy]] | |||
*[[/Stress measurement|Stress measurement]] | |||
*[[/Thickness Measurer|Wafer thickness measurement]] | |||
*[[/Topographic measurement|Topographic measurement]] | |||
*[[Specific Process Knowledge/Characterization/XRD|X-ray diffraction]] | |||
<!-- | |||
*[[/Other electrical measurements|Other electrical measurements]] | |||
--> | |||
== Choose equipment == | == Choose equipment == | ||
===[[SEM: Scanning Electron Microscopy]] | ===AFM=== | ||
*[[/AFM: Atomic Force Microscopy|''Atomic Force Microscopy (AFM)'']] | |||
===Electrical measurements=== | |||
*[[/Four-Point Probe|4-Point Probe]] | |||
*[[/Probe station|Probe station]] | |||
*[[/III-V ECV-profiler|III-V ECV-profiler (Electrochemical Capacitance-Voltage carrier density profiler)]] | |||
===Element analysis=== | |||
*[[/SEM Supra 2|SEM with EDX]] | |||
*[[/XPS|XPS tools ]] | |||
===Optical and stylus profilers=== | |||
*[[/Sensofar_S_Neox|Sensofar S Neox (Optical Profiler)]] | |||
*[[/Dektak_XTA|Dektak XTA (Stylus Profiler)]] | |||
*[[/Tencor_P17|Tencor P17 (Stylus Profiler)]] | |||
*[[/Dektak_3ST|Dektak 3ST (Stylus profiler)]] | |||
*[[/Dektak_150|Dektak 150 (Stylus Profiler)]] | |||
===Optical microscopes=== | |||
*[[/Optical microscope|Optical microscopes]] | |||
===Optical characterization=== | |||
*[[/Optical characterization#Ellipsometer|Ellipsometer]] | |||
*[[/Optical characterization#Filmtek_4000|Filmtek 4000]] | |||
*[[/PL mapper|PL mapper - ''Photoluminescence mapper'']] | |||
*[[/Lifetime scanner MDPmap|Lifetime scanner MDPmap]] | |||
===SEMs at DTU Nanolab - building 307/314=== | |||
<!-- *[[LabAdviser/CEN/Quanta 3D FIB/SEM|FIB-SEM FEI QUANTA 200 3D]] --> | |||
*[[LabAdviser/314/Microscopy 314-307/FIB/Helios|Dual Beam FEI Helios Nanolab 600]] | |||
*[[LabAdviser/314/Microscopy 314-307/SEM/Nova|SEM FEI Nova 600 NanoSEM]] | |||
*[[ | |||
LabAdviser/314/Microscopy 314-307/SEM/QFEG|SEM FEI Quanta 200 ESEM FEG]] | |||
<!-- *[[LabAdviser/CEN/Inspect S|SEM Inspect S]] --> | |||
===SEM's in building 346=== | |||
*[[/SEM: Scanning Electron Microscopy |SEM Comparison page]] | |||
*[[/SEM Supra 1|SEM Supra 1]] | |||
*[[/SEM Supra 2|SEM Supra 2]] | |||
*[[/SEM Supra 3|SEM Supra 3]] | |||
*[[/SEM Tabletop 1|SEM Tabletop 1]] | |||
* | ===TEMs at DTU Nanolab - building 307/314=== | ||
* | *[[LabAdviser/314/Microscopy 314-307/TEM/ATEM |Titan ATEM]] | ||
* | *[[LabAdviser/314/Microscopy 314-307/TEM/ETEM |Titan ETEM]] | ||
*[[LabAdviser/314/Microscopy 314-307/TEM/T20 |Tecnai TEM]] | |||
===[[ | ===XRD=== | ||
* | *[[/XRD|General page on XRD]], page describing general info relevant to both our XRD's | ||
*[[/XRD/XRD Powder|XRD Powder]], tabletop XRD for Bregg-Brentano measurements of powders | |||
*[[/XRD/XRD SmartLab|XRD SmartLab]], advanced multipurpose instrument in the cleanroom | |||
*[[/XRD/XRD SmartLab 9kW Rotating Anode|XRD SmartLab 9kW Rotating Anode]] multipurpose system outside the cleanroom | |||
*[[ | ===Various=== | ||
* | *[[/Drop Shape Analyzer|Drop Shape Analyzer]] | ||
*[[/Thickness Measurer|Thickness Measurer]] | |||
*[[/Hardness measurement|Hardness tester]] | |||
*[[/Particle Scanner Takano|Particle Scanner Takano]] | |||
== | ==Decommissioned equipment== | ||
*[[/KLA-Tencor Surfscan 6420|KLA-Tencor Surfscan 6420]] | |||
*[[/X-Ray Diffractometer|Phillips X-Ray Diffractometer (owned by DTU Fotonik)]] | |||
* | |||
Latest revision as of 15:09, 20 June 2025
The content on this page, including all images and pictures, was created by DTU Nanolab staff, unless otherwise stated.
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Overview of characteristics and where to measure it
| Optical Microscopes | SEM (incl. EDX) | AFM | Stylus profilers | Optical profilers | Filmtek (reflectometer) | Ellipsometer | Thickness stylus | XPS | PL mapper | 4-point probe | Probe station | XRD | Life time scanner | Drop shape analyser | Hardness tester | Particle scanner | IR-camera | III-V ECV-profiler | Microspectrophotometer (Craic 20/30 PV) | |
| Breakdown voltage | ||||||||||||||||||||
| Carrier density/doping profile | x | |||||||||||||||||||
| Charge carrier life time | x | |||||||||||||||||||
| Contact angle hydrophobic/hydrophillic | x | |||||||||||||||||||
| Crystallinity | x | |||||||||||||||||||
| Deposition uniformity | x | x | x | |||||||||||||||||
| Dimensions(in plane) | x | x | (x) | (x) | x | x | ||||||||||||||
| Dimensions(height)/Topography | (x) | (x) | x | x | x | |||||||||||||||
| Electrical conductivity | x | |||||||||||||||||||
| Element analysis | x | x | x 4 | x 4 | ||||||||||||||||
| Film stress | x | x 7 | ||||||||||||||||||
| Imaging | x | x | x | x | x | |||||||||||||||
| Material Hardness | x | |||||||||||||||||||
| Band gap | x | x | x | |||||||||||||||||
| Particles | x | x | x | x | x | |||||||||||||||
| Phase changes | ||||||||||||||||||||
| Reflectivity | x | x | x 6 | x | ||||||||||||||||
| Refractive index | x | x | ||||||||||||||||||
| Resistivity | x | |||||||||||||||||||
| Step coverage | x 1 | x 1 | ||||||||||||||||||
| Surface roughness | x | x | x | x | ||||||||||||||||
| Thermal conductivity | ||||||||||||||||||||
| Thin film thickness | x 1 | x 1 | x 2 | x 2 | x | x | x | x 5 | x 3 | x | ||||||||||
| Voids in wafer bonding | x | x | x | |||||||||||||||||
| Wafer thickness | x 1 | x 1 | x | |||||||||||||||||
| Work function | x |
1 Using the cross section method
2 Using the create step method
3 With known resistivity
4 Composition information for crystalline materials
5 Only single layer
6 Good for characterization of VCSEL structures and DBR mirrors
7 Only for crystalline films
Choose characterization topic
- Carrier density (doping) profiler
- Contact angle measurement
- Element analysis
- Film thickness and optical constants
- Hardness measurement
- Photoluminescence mapping
- Four-Point Probe (Resistivity measurement)
- Sample imaging
- Sample preparation for inspection
- Scanning Electron Microscopy
- Stress measurement
- Wafer thickness measurement
- Topographic measurement
- X-ray diffraction
Choose equipment
AFM
Electrical measurements
- 4-Point Probe
- Probe station
- III-V ECV-profiler (Electrochemical Capacitance-Voltage carrier density profiler)
Element analysis
Optical and stylus profilers
- Sensofar S Neox (Optical Profiler)
- Dektak XTA (Stylus Profiler)
- Tencor P17 (Stylus Profiler)
- Dektak 3ST (Stylus profiler)
- Dektak 150 (Stylus Profiler)
Optical microscopes
Optical characterization
SEMs at DTU Nanolab - building 307/314
LabAdviser/314/Microscopy 314-307/SEM/QFEG|SEM FEI Quanta 200 ESEM FEG]]
SEM's in building 346
TEMs at DTU Nanolab - building 307/314
XRD
- General page on XRD, page describing general info relevant to both our XRD's
- XRD Powder, tabletop XRD for Bregg-Brentano measurements of powders
- XRD SmartLab, advanced multipurpose instrument in the cleanroom
- XRD SmartLab 9kW Rotating Anode multipurpose system outside the cleanroom