Specific Process Knowledge/Characterization/XPS/K-Alpha: Difference between revisions
Appearance
No edit summary |
mNo edit summary |
||
| (10 intermediate revisions by one other user not shown) | |||
| Line 1: | Line 1: | ||
{{cc-nanolab}} | |||
'''Feedback to this page: | '''Feedback to this page: | ||
[mailto:labadviser@nanolab.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.nanolab.dtu.dk/index.php/Specific_Process_Knowledge/Characterization/XPS/K-Alpha click here]''' | [mailto:labadviser@nanolab.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.nanolab.dtu.dk/index.php/Specific_Process_Knowledge/Characterization/XPS/K-Alpha click here]''' | ||
[[Category: Equipment |Characterization chemical]] | [[Category: Equipment |Characterization chemical]] | ||
[[Category: Characterization|Chemical]] | [[Category: Characterization|Chemical]] | ||
<!--Checked for updates on 4/4-2025 - ok/jmli --> | |||
== The XPS K-Alpha == | |||
Name: XPS K-Alpha <br> | |||
Vendor: Thermofisher <br> | |||
The XPS K-Alpha allows you to analyse a broad range of samples with the XPS technique. | |||
'''The user manual(s), user APV(s), technical information and contact information are be found in LabManager:''' | |||
<!-- remember to remove the type of documents that are not present --> | |||
<!-- give the link to the equipment info page in LabManager: --> | |||
[http://labmanager.dtu.dk/function.php?module=Machine&view=view&mach=276 XPS K-Alpha in LabManager] | |||
[[Image:XPS K-Alpha.jpg |thumb|x300px|The K-Alpha has its back turned towards the [[Specific Process Knowledge/Characterization/XPS/Nexsa | XPS Nexsa]] in room 904 in building 346.]] | |||
==Process information== | |||
The XPS instrument enables elemental analysis, chemical state analysis on the sample surface or deeper down by a depth profiling. A comparison about techniques and instruments used for elemental analysis at DTU Nanolab can be found on the page [[Specific Process Knowledge/Characterization/Element analysis|Element analysis]]. | |||
More about the different possibilities of the XPS instrument is found here: | |||
*[[Specific Process Knowledge/Characterization/XPS/XPS technique|The XPS technique]] | |||
*[[Specific Process Knowledge/Characterization/XPS/XPS elemental composition|Elemental analysis]] | |||
*[[Specific Process Knowledge/Characterization/XPS/XPS Chemical states |Chemical sensitivity]] | |||
*[[Specific Process Knowledge/Characterization/XPS/XPS Depth profiling|Depth profiling]] | |||
*[[Specific Process Knowledge/Characterization/XPS/Carbon contamination|Carbon contamination]] | |||
*[[Specific Process Knowledge/Characterization/XPS/ExtDocs | Links to external material ]] | |||
== Getting access to the XPS == | |||
Click [[Specific Process Knowledge/Characterization/XPS/Access | '''HERE''' ]] to see information on how to get access to the XPS. | |||
== Performance of XPS K-Alpha == | |||
{| border="2" cellspacing="0" cellpadding="1" |- | |||
!style="background:silver; color:black;" align="left"|Purpose | |||
|style="background:LightGrey; color:black"|Chemical analysis | |||
|style="background:WhiteSmoke; color:black"| | |||
* [[Specific Process Knowledge/Characterization/XPS/XPS elemental composition|Probing elemental composition]] | |||
* [[Specific Process Knowledge/Characterization/XPS/XPS Chemical states |Chemical state identification]] | |||
* Non destructive technique | |||
* Surface sensitive | |||
* [[Specific Process Knowledge/Characterization/XPS/XPS Depth profiling|Depth profiling]] possible by ion beam etch of sample | |||
|- | |||
!rowspan="5" style="background:silver; color:black" align="left"| Performance | |||
|style="background:LightGrey; color:black"|Spot size | |||
|style="background:WhiteSmoke; color:black"|Can be set between 30µm - 400µm | |||
|- | |||
|style="background:LightGrey; color:black"|Probing depth | |||
|style="background:WhiteSmoke; color:black"|Depending on probed element. Max probe depth lies within 10-200 Å. | |||
|- | |||
|style="background:LightGrey; color:black"|Resolution | |||
|style="background:WhiteSmoke; color:black"|Dependent on probed elements. Concentrations down to about 0,5 atomic % can in some cases be detected. | |||
|- | |||
|style="background:LightGrey; color:black"|Charge compensation | |||
|style="background:WhiteSmoke; color:black"| | |||
Flood gun can be used for charge compensation of non conductive samples | |||
|- | |||
|style="background:LightGrey; color:black"|Finding structures | |||
|style="background:WhiteSmoke; color:black"|Choose measuring spot from camera image (magnified) | |||
|- | |||
|- | |||
|- | |||
!rowspan="2" style="background:silver; color:black" align="left"|Depth profiling | |||
|style="background:LightGrey; color:black"|Purpose | |||
|style="background:WhiteSmoke; color:black"|With ion beam etch the top layer of the material can be removed, to do a depth profiling | |||
|- | |||
|style="background:LightGrey; color:black"|Ion beam size | |||
|style="background:WhiteSmoke; color:black"| About 3x1 mm | |||
= | |- | ||
!rowspan="2" style="background:silver; color:black" align="left"|Substrates | |||
|style="background:LightGrey; color:black"|Substrate size | |||
|style="background:WhiteSmoke; color:black"| | |||
Maximum 60x60 mm | |||
|- | |||
| style="background:LightGrey; color:black"|Substrate thickness | |||
|style="background:WhiteSmoke; color:black"| | |||
Maximum height about 20 mm | |||
|- | |||
|} | |||