Specific Process Knowledge/Etch/Wet Silicon Oxide Etch (BHF): Difference between revisions
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'''Feedback to this page''': '''[mailto:labadviser@nanolab.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.nanolab.dtu.dk/index.php/Specific_Process_Knowledge/Etch/Wet_Silicon_Oxide_Etch_(BHF) click here]''' | '''Feedback to this page''': '''[mailto:labadviser@nanolab.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.nanolab.dtu.dk/index.php/Specific_Process_Knowledge/Etch/Wet_Silicon_Oxide_Etch_(BHF) click here]''' | ||
'''''Unless anything else is stated, everything on this page, text and pictures are made by DTU Nanolab.''''' | |||
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[[Category: Equipment|Etch Wet Silicon Oxide]] | [[Category: Equipment|Etch Wet Silicon Oxide]] | ||
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'''The user manual for Oxide etch 2: BHF (clean), APV's and contact information can be found in LabManager''' [http://labmanager.dtu.dk/function.php?module=Machine&view=view&mach=378 by clicking here] | '''The user manual for Oxide etch 2: BHF (clean), APV's and contact information can be found in LabManager''' [http://labmanager.dtu.dk/function.php?module=Machine&view=view&mach=378 by clicking here] | ||
'''The user manual for Oxide etch 3: 10% HF, APV's and contact information can be found in LabManager''' [http://labmanager.dtu.dk/function.php?module=Machine&view=view&mach=380 by clicking here] | |||
'''The user manual for various HF baths in RCA and Fume hoods, APV's and contact information can be found in LabManager''' [http://labmanager.dtu.dk/function.php?module=Machine&view=view&mach=64 by clicking here] | '''The user manual for various HF baths in RCA and Fume hoods, APV's and contact information can be found in LabManager''' [http://labmanager.dtu.dk/function.php?module=Machine&view=view&mach=64 by clicking here] | ||
'''<big>Working with HF above 13% is only allowed by Nanolab staff</big>''' | |||
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!colspan="2" border="none" style="background:silver; color:black;" align="center"|Etchant | !colspan="2" border="none" style="background:silver; color:black;" align="center"|Etchant | ||
|style="background:WhiteSmoke; color:black"|<b>[[Specific_Process_Knowledge/Etch/Wet_Silicon_Oxide_Etch_(BHF)#Comparing_different_BHF_baths|BHF]]</b> | |style="background:WhiteSmoke; color:black"|<b>[[Specific_Process_Knowledge/Etch/Wet_Silicon_Oxide_Etch_(BHF)#Comparing_different_BHF_baths|BHF]]</b> | ||
|style="background:WhiteSmoke; color:black"|<b>[[Specific_Process_Knowledge/Etch/Wet_Silicon_Oxide_Etch_(BHF)#Comparing_different_5.25_HF_baths|5% HF]]</b> | |style="background:WhiteSmoke; color:black"|<b>[[Specific_Process_Knowledge/Etch/Wet_Silicon_Oxide_Etch_(BHF)#Comparing_different_5.25_HF_baths|1% HF / 5% HF / 10% HF]]</b> | ||
|style="background:WhiteSmoke; color:black"|<b>[[Specific_Process_Knowledge/Etch/Wet_Silicon_Oxide_Etch_(BHF)#Comparing_different_40.25_HF_baths|40% HF]]</b> | |style="background:WhiteSmoke; color:black"|<b>[[Specific_Process_Knowledge/Etch/Wet_Silicon_Oxide_Etch_(BHF)#Comparing_different_40.25_HF_baths|40% HF]]</b> | ||
|style="background:WhiteSmoke; color:black"|<b>[[Specific_Process_Knowledge/Etch/Wet_Silicon_Oxide_Etch_(BHF)#SiO_etch_bath|BOE 7:1 Etchant VLSI with Surfactant]]</b> | |style="background:WhiteSmoke; color:black"|<b>[[Specific_Process_Knowledge/Etch/Wet_Silicon_Oxide_Etch_(BHF)#SiO_etch_bath|BOE 7:1 Etchant VLSI with Surfactant]]</b> | ||
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*Mainly for removing native oxide | *Mainly for removing native oxide | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
*Mainly for etching deep into borofloat or quartz wafers | *Mainly for etching deep into borofloat or quartz wafers. '''Only Nanolab staff are allowed to work with this HF'''. | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
*Etching of silicon oxide - especially for etching small holes | *Etching of silicon oxide - especially for etching small holes | ||
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|style="background:LightGrey; color:black"|Link to safety APV and SDS (You must be logged in to Kemibrug to view SDSs) | |style="background:LightGrey; color:black"|Link to safety APV and SDS (You must be logged in to Kemibrug to view SDSs) | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
*:[http://labmanager. | *:[http://labmanager.nanolab.dtu.dk/d4Show.php?id=1897&mach=64 see APV here] | ||
*:[https://kemibrug.dk/Kemikalier/Action?id=RCU2MHolYzIlODIlN2UlYzIlODB2JWMyJTgxJTdleiVjMiU4N0RZeiVjMiU4OXYlN2UlYzIlODElYzIlODhESkhKSUxMVGQlYzIlODclN2N2JWMyJTgzJTdlJWMyJTg4diVjMiU4OSU3ZSVjMiU4NCVjMiU4MyVjMiU4OCU1ZVlSSQ==#K see SDS here] | *:[https://kemibrug.dk/Kemikalier/Action?id=RCU2MHolYzIlODIlN2UlYzIlODB2JWMyJTgxJTdleiVjMiU4N0RZeiVjMiU4OXYlN2UlYzIlODElYzIlODhESkhKSUxMVGQlYzIlODclN2N2JWMyJTgzJTdlJWMyJTg4diVjMiU4OSU3ZSVjMiU4NCVjMiU4MyVjMiU4OCU1ZVlSSQ==#K see SDS here] | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
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*Wet thermal oxide:75-80nm/min | *Wet thermal oxide:75-80nm/min | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
*Wet thermal oxide:~25nm/min | *Wet thermal oxide:~6nm/min(1%) / 25nm/min(5%) / 52nm/min(10%) | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
*Boronfloat and quartz: ~3-4 μm/min | *Boronfloat and quartz: ~3-4 μm/min | ||
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*BHF (12%HF with Ammoniumflouride) | *BHF (12%HF with Ammoniumflouride) | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
*5% HF | *1% / 5% HF | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
*40% HF | *40% HF | ||
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<br clear="all" /> | <br clear="all" /> | ||
<gallery caption="Different places to do wet silicon oxide etch" widths=" | <gallery caption="Different places to do wet silicon oxide etch" widths="420px" heights="425px" perrow="5"> image:BHF clean.JPG|BHF in wetbench 04 in D-3 (Oxide etch 2: BHF (clean)). Wet silicon oxide etch bath positioned to the right in the wetbench. This bath can also be used for BHF with wetting agent. | ||
image:KOH_BHF.JPG|BHF in wetbench 01 Si etch in D-3 (Oxide etch 1: BHF. | image:KOH_BHF.JPG|BHF in wetbench 01 Si etch in D-3 (Oxide etch 1: BHF). The BHF bath is positioned in the middle of the bench. This is primarily used to remove oxide before and after a Si etch. | ||
image: | image:BHF clean.JPG|BHF in wetbench 05 in D-3 (Oxide etch 3: 10% HF). Wet silicon oxide etch bath positioned to the right in the wetbench. This bath can also be used for BHF, BHF with wetting agent or 40% HF on request. This bath is also used for cleaning quarts carriers from the PECVD4 system. | ||
image: | image:RCA-HF.jpg|HF baths in RCA bench in B-1. These may only be used together with RCA cleaning and furnace processes. | ||
</gallery> | |||
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<br clear="all" /> | <br clear="all" /> | ||
==Comparing different | ==Comparing different HF baths== | ||
{|border="1" cellspacing="1" cellpadding="3" style="text-align:left;" | {|border="1" cellspacing="1" cellpadding="3" style="text-align:left;" | ||
|- | |- | ||
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|-style="background:silver; color:black" | |-style="background:silver; color:black" | ||
! | ! | ||
! | ! 1% HF in RCA Bench | ||
! | ! 10% HF in D3 wet bench 5 (Oxide etch 3) | ||
! | ! 1% HF Plastic beaker | ||
|- | |- | ||
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!Size of substrate | !Size of substrate | ||
|2"-6" wafers | |2"-6" wafers | ||
|2"- | |2"- 6" wafers or any that fits in a dedicated holder | ||
|2"- 4" wafers or any that fits in a dedicated holder | |2"- 4" wafers or any that fits in a dedicated holder | ||
|- | |- | ||
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<br clear="all" /> | <br clear="all" /> | ||
== | ==40% HF== | ||
{|border="1" cellspacing="1" cellpadding=" | {|border="1" cellspacing="1" cellpadding="2" style="text-align:left;" | ||
|- | |- | ||
|-style="background:silver; color:black" | |-style="background:silver; color:black" | ||
! | ! | ||
! 40% HF | ! 40% HF in Plastic beaker, only done by Nanolab staff | ||
|- | |- | ||
|-style="background:WhiteSmoke; color:black" | |-style="background:WhiteSmoke; color:black" | ||
!Batch size! | !Batch size! | ||
|1 wafer at a time | |1 wafer at a time | ||
|- | |- | ||
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|-style="background:LightGrey; color:black" | |-style="background:LightGrey; color:black" | ||
!Size of substrate | !Size of substrate | ||
|Any that fits to a dedicated holder | |Any that fits to a dedicated holder | ||
|- | |- | ||
|-style="background:WhiteSmoke; color:black" | |-style="background:WhiteSmoke; color:black" | ||
!Allowed materials | !Allowed materials | ||
|All materials | |All materials | ||
|- | |- | ||