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Specific Process Knowledge/Thin film deposition/Deposition of Silicon Oxide/Deposition of Silicon Oxide using PECVD

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At the moment DANCHIP has 3 PECVDs that can deposite silicon oxide with or without dopants of Boron, Phosphorous or Germanium. PECVD1 and PECVD3 are for silicon based processing. PECVD2 is for III-V processing and is described under III-V processing. Look at the PECVD page to learn more about the PECVDs at DANCHIP. Allthough PECVD1 and PECVD3 are very much alike you cannot count on the a recipe on one system will give exactly the same results on the other system.


Recipes on PECVD1 for deposition of silicon oxides

Recipes

Recipe name SiH4 flow [sccm] N2O flow [sccm] N2 flow [sccm] B2H6 flow [sccm] PH3 flow [sccm] Pressure [mTorr] Power [W] Description
1oxide/1ox_std/standard 17 1600 0 0 0 400 380LF Process control recipe. Developed for waveguides
1PBSG 17 1600 0 135 40 500 800LF Developed for waveguide top cladding by Haiyan Ou @DTU Photonics'.
BGE_PBSG 17 1600 0 240 60 500 800LF Low stress PBSG

Expected results

Recipe name Deposition rate [µm/min] RI Uniformity [%] Comments
1oxide/1ox_std/standard ~0.193 1.46 2 The latest measured values can be seen in the process control sheet in LabManager
1PBSG ~0.3 1.458@633nm

Recipes on PECVD3 for deposition of silicon oxides

Recipes

Recipe name SiH4 flow [sccm] N2O flow [sccm] N2 flow [sccm] B2H6 flow [sccm] PH3 flow [sccm] Pressure [mTorr] Power [W] Description
LFSiO 12 1420 392 0 0 550 60 Uniform silicon oxide
1PBSG 17 1600 0 135 40 500 800LF BPSG glass for waveguide cladding layer

LF=Low Frequency

Expected results

Recipe name Deposition rate [nm/min] RI Uniformity [%]
LFSiO ~75 ~1.48 <1
1PBSG ~228 nm/min . ~17%

Recipes on PECVD3 for deposition of doped oxide

Recipes

Recipe name SiH4 flow [sccm] N2 flow [sccm] GeH4 flow [sccm] (scaled by 100) B2H6 flow [sccm] PH3 flow [sccm] Pressure [mTorr] Power [W] Description
Core-Ge 17 300 300 0 0 400 600 LF Process for germanium doped core layer developed by Haiyan Ou from DTU Photonics

Annnealing: Anneal bond furnace, recipe "core1100"

Top-BPSG 17 0 0 100 40 500 800 LF Process for PBSG top clading layer developed by Haiyan Ou from DTU Photonics

Annnealing/oxidation: Anneal bond furnace, recipe "clad1000"

Expected results

Recipe name Deposition rate [nm/min] Refractive index
Core-Ge ~188 nm/min ~1.46969
Top-BPSG ~248 nm/min ~1.458