Specific Process Knowledge/Thin film deposition/Deposition of Tungsten: Difference between revisions

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== Tungsten deposition ==
== Tungsten deposition ==


Tungsten (W) can be deposited by e-beam evaporation. However, it requires very high temperature to evaporate, so it is at the performance limit of the 6 kW power supplies of our systems. This means the deposition rate is rather low. Additionally, the chamber and substrate(s) will get hot during the deposition (despite water cooling), and this means the pressure rises as the chamber is baked out. It is therefore not easy to deposit films much thicker than 50-60 nm. In the Temescal we stopped the deposition every 20 nm to let the pressure drop. Talk to staff when you want to deposit W (write to thinfilm@danchip.dtu.dk). In the chart below you can compare the deposition equipment.
Tungsten (W) can be deposited by e-beam evaporation and sputtering. However, in case of evaporation the precess generates a lot of heat (despite water cooling), and this means the pressure rises as the chamber is baking out. It is therefore not easy to deposit films much thicker than 50-60 nm. In the Temescal we stopped the deposition every 20 nm to let the pressure drop. Also, the rate needs to be low, to avoid overheating. Talk to staff when you want to deposit W (write to thinfilm@danchip.dtu.dk). Sputtering can be used without any sufficient issues. In the chart below you can compare the deposition equipment.




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!   
!   
! E-beam evaporation ([[Specific Process Knowledge/Thin film deposition/Temescal|Temescal]])  
! E-beam evaporation ([[Specific Process Knowledge/Thin film deposition/Temescal|Temescal]])  
! E-beam evaporation ([[Specific Process Knowledge/Thin film deposition/Physimeca|Physimeca]])
! E-beam evaporation ([[Specific Process Knowledge/Thin film deposition/Lesker|Lesker]])
|-  
|-  
|-style="background:WhiteSmoke; color:black"
|-style="background:WhiteSmoke; color:black"
! General description
! General description
| E-beam evaporation of W
| E-beam evaporation of W
| E-beam evaporation of W
| Sputtering of W
|-
|-
|-style="background:Lightgrey; color:black"
|-style="background:Lightgrey; color:black"
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|-style="background:WhiteSmoke; color:black"
|-style="background:WhiteSmoke; color:black"
! Layer thickness
! Layer thickness
|10Å to 600Å*
|10Å to 50nm
|10Å to 500Å*  
|10Å to 600nm*  
|-
|-


|-style="background:Lightgrey; color:black"
|-style="background:Lightgrey; color:black"
! Deposition rate
! Deposition rate
|0.5 Å/s to 2 Å/s
|0.5 Å/s to 1 Å/s
|about 1 Å/s
|about 1 Å/s
|-style="background:WhiteSmoke; color:black"
|-style="background:WhiteSmoke; color:black"
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|
|
*Up to 1x4" wafers
*Up to 1x4" wafers
*Up to 1x6" wafer
*small pieces
*small pieces
|-
|-

Revision as of 14:36, 3 October 2021

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Tungsten deposition

Tungsten (W) can be deposited by e-beam evaporation and sputtering. However, in case of evaporation the precess generates a lot of heat (despite water cooling), and this means the pressure rises as the chamber is baking out. It is therefore not easy to deposit films much thicker than 50-60 nm. In the Temescal we stopped the deposition every 20 nm to let the pressure drop. Also, the rate needs to be low, to avoid overheating. Talk to staff when you want to deposit W (write to thinfilm@danchip.dtu.dk). Sputtering can be used without any sufficient issues. In the chart below you can compare the deposition equipment.


E-beam evaporation (Temescal) E-beam evaporation (Lesker)
General description E-beam evaporation of W Sputtering of W
Pre-clean Ar ion beam None
Layer thickness 10Å to 50nm 10Å to 600nm*
Deposition rate 0.5 Å/s to 1 Å/s about 1 Å/s
Batch size
  • Up to 4x6" wafers
  • Up to 3x8" wafers (ask for holder)
  • small pieces
  • Up to 1x4" wafers
  • Up to 1x6" wafer
  • small pieces
Allowed materials
  • Silicon
  • Silicon oxide
  • Silicon (oxy)nitride
  • Photoresist
  • PMMA
  • Mylar
  • SU-8
  • Metals
  • Silicon
  • Silicon oxide
  • Silicon (oxy)nitride
  • Photoresist
  • PMMA
  • Mylar
Comments Substrate gets hot during deposition

(for a 60 nm film it rose above 123 C)

* For thicknesses above 20 nm talk to staff (write to thinfilm@danchip.dtu.dk), as the heat and subsequent pressure rise means the deposition needs to be carried out in steps.