Specific Process Knowledge/Characterization/XPS/K-Alpha: Difference between revisions
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<!-- give the link to the equipment info page in LabManager: --> | <!-- give the link to the equipment info page in LabManager: --> | ||
[http://labmanager.dtu.dk/function.php?module=Machine&view=view&mach=276 XPS K-Alpha in LabManager] | [http://labmanager.dtu.dk/function.php?module=Machine&view=view&mach=276 XPS K-Alpha in LabManager] | ||
==Elemental analysis== | |||
The XPS instrument enables elemental analysis, chemical state analysis on the sample surface or deeper down by a depth profiling. A comparison about techniques and instruments used for elemental analysis at DTU Nanolab can be found on the page [[Specific Process Knowledge/Characterization/Element analysis|Element analysis]]. | |||
More about the different possibilities of the XPS instrument is found here: | |||
*[[Specific Process Knowledge/Characterization/XPS/XPS technique|The XPS technique]] | |||
*[[Specific Process Knowledge/Characterization/XPS/XPS elemental composition|Elemental analysis]] | |||
*[[Specific Process Knowledge/Characterization/XPS/XPS Chemical states |Chemical sensitivity]] | |||
*[[Specific Process Knowledge/Characterization/XPS/XPS Depth profiling|Depth profiling]] | |||
*[[/Carbon contamination|Carbon contamination]] | |||
*[[Specific Process Knowledge/Characterization/XPS/ExtDocs | Links to external material ]] | |||
== Getting access to the XPS == | |||
Click [[Specific Process Knowledge/Characterization/XPS/Access | '''HERE''' ]] to see information on how to get access to the XPS. | |||
== Performance of XPS K-Alpha == | |||
{| border="2" cellspacing="0" cellpadding="1" |- | |||
!style="background:silver; color:black;" align="left"|Purpose | |||
|style="background:LightGrey; color:black"|Chemical analysis | |||
|style="background:WhiteSmoke; color:black"| | |||
* [[Specific Process Knowledge/Characterization/XPS/XPS elemental composition|Probing elemental composition]] | |||
* [[Specific Process Knowledge/Characterization/XPS/XPS Chemical states |Chemical state identification]] | |||
* Non destructive technique | |||
* Surface sensitive | |||
* [[Specific Process Knowledge/Characterization/XPS/XPS Depth profiling|Depth profiling]] possible by ion beam etch of sample | |||
|- | |||
!rowspan="5" style="background:silver; color:black" align="left"| Performance | |||
|style="background:LightGrey; color:black"|Spot size | |||
|style="background:WhiteSmoke; color:black"|Can be set between 30µm - 400µm | |||
|- | |||
|style="background:LightGrey; color:black"|Probing depth | |||
|style="background:WhiteSmoke; color:black"|Depending on probed element. Max probe depth lies within 10-200 Å. | |||
|- | |||
|style="background:LightGrey; color:black"|Resolution | |||
|style="background:WhiteSmoke; color:black"|Dependent on probed elements. Concentrations down to about 0,5 atomic % can in some cases be detected. | |||
|- | |||
|style="background:LightGrey; color:black"|Charge compensation | |||
|style="background:WhiteSmoke; color:black"| | |||
Flood gun can be used for charge compensation of non conductive samples | |||
|- | |||
|style="background:LightGrey; color:black"|Finding structures | |||
|style="background:WhiteSmoke; color:black"|Choose measuring spot from camera image (magnified) | |||
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|- | |||
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!rowspan="2" style="background:silver; color:black" align="left"|Depth profiling | |||
|style="background:LightGrey; color:black"|Purpose | |||
|style="background:WhiteSmoke; color:black"|With ion beam etch the top layer of the material can be removed, to do a depth profiling | |||
|- | |||
|style="background:LightGrey; color:black"|Ion beam size | |||
|style="background:WhiteSmoke; color:black"| About 3x1 mm | |||
|- | |||
!rowspan="2" style="background:silver; color:black" align="left"|Substrates | |||
|style="background:LightGrey; color:black"|Substrate size | |||
|style="background:WhiteSmoke; color:black"| | |||
Maximum 60x60 mm | |||
|- | |||
| style="background:LightGrey; color:black"|Substrate thickness | |||
|style="background:WhiteSmoke; color:black"| | |||
Maximum height about 20 mm | |||
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|} | |||