Jump to content

Specific Process Knowledge/Thin film deposition/Deposition of NiFe: Difference between revisions

Reet (talk | contribs)
Reet (talk | contribs)
No edit summary
Line 1: Line 1:
'''Feedback to this page''': '''[mailto:labadviser@nanolab.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.nanolab.dtu.dk/index.php/Specific_Process_Knowledge/Thin_film_deposition/Deposition_of_NiFe click here]'''
'''Feedback to this page''': '''[mailto:labadviser@nanolab.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.nanolab.dtu.dk/index.php/Specific_Process_Knowledge/Thin_film_deposition/Deposition_of_NiFe click here]'''


==Deposition of Nickel Iron alloy==
=Deposition of NiFe alloy=
NiFe has been deposited in the [[Specific_Process_Knowledge/Thin_film_deposition/Lesker|Sputter System (Lesker)]] here at Nanolab. Below you will find some results of varying the deposition parameters. You can find more information on the process parameters used by others in the [http://labmanager.dtu.dk/function.php?module=Processlog&view=editlog&machid=244 Process Log] in LabManager.


Nickel Iron alloy, e.g., Invar, has been sputter deposited in the [[Specific_Process_Knowledge/Thin_film_deposition/Lesker|Sputter-system (Lesker)]] here at Nanolab.
==Film quality optimization==
''By Bjarke Thomas Dalslet @Nanotech.dtu.dk''


You will find detailed results of varying the process parameters when sputtering Ni-Fe in the Lesker sputter system [[/Sputtering of NiFe in the Lesker sputter system|here]].
The Lesker CMS 18 sputter system can produce films in a wide range of qualities. The quality of a film depends strongly on the substrate (lattice matching), but also on the energy the sputtered material can utilize for annealing.
 
Strain estimations was done on 30 nm Ni<math>_{81}</math>Fe<math>_{19}</math> thin films using low angle x-ray diffraction, for various substrates. It was found that the strain of the film influenced the resistance (R) and anisotropic magneto resistance (AMR) of the films (this relationship is also documented in literature); A Ta interface layer reduced R and increased AMR on both Si and SiO<math>_2</math> substrates while reducing strain.
 
This study was then done on 30 nm Ni<math>_{81}</math>Fe<math>_{19}</math> thin films deposited on 3 nm Ta on top of a SiO<math>_2</math> substrate, using R and AMR as an indication of strain. As seen in the tables, applying a substrate bias increases AMR and conductance (1/R). An equivalent effect is seen when heating the substrate during deposition. This heating can also be done after deposition without loosing the effect.
 
{| {{table}} border="1" cellspacing="0" cellpadding="8"
| align="center" style="background:#f0f0f0;"|'''Name'''
| align="center" style="background:#f0f0f0;"|'''Substrate bias (W)'''
| align="center" style="background:#f0f0f0;"|'''AMR'''
| align="center" style="background:#f0f0f0;"|'''1/R (S)'''
| align="center" style="background:#f0f0f0;"|'''Crystal strain'''
|-
| 0029 NiFe3_stack_RF20||20||0.02724278||1.308044474||
|-
| 0018_NiFe1_stack_RF||10||0.025850358||0.898311175||
|-
| 0030 NiFe3_stack||0||0.020103598||0.71772052||0.8
|-
|}
 
 
{| {{table}} border="1" cellspacing="0" cellpadding="8"
| align="center" style="background:#f0f0f0;"|'''Name'''
| align="center" style="background:#f0f0f0;"|'''Temperature (C)'''
| align="center" style="background:#f0f0f0;"|'''AMR'''
| align="center" style="background:#f0f0f0;"|'''1/R (S)'''
| align="center" style="background:#f0f0f0;"|'''Crystal strain'''
|-
| 0030 NiFe3_stack||25||0.020103598||0.71772052||0.8
|-
| BDT-NiFe1-blank30||200||0.019319002||1.095770327||
|-
| BTD-NiFe-Blank22||250||0.021768497||1.047668937||
|-
| BTD-NiFe-Blank14||300||0.02983617||1.724137931||
|-
| BTD-NiFe-Blank13||350||0.033944331||1.887504719||
|-
| BTD-NiFe-Blank15||400||0.031176801||1.655903295||0.2
|-
| BTD-NiFe-Blank16||450||0.030843457||||
|-
|
|}
 
==Stress in films deposited at high temperature==
In 2017, Radu Malureanu measured a tensile stress of about 100 MPa on thin films of Invar deposited at 600 °C. Read more about stress in thin films deposited with the Lesker sputter system [http://labadviser.nanolab.dtu.dk/index.php/Specific_Process_Knowledge/Thin_film_deposition/Lesker/Stress_dependence_on_sputter_parameters_in_the_Lesker_sputter_system here].