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Specific Process Knowledge/Etch/ASE (Advanced Silicon Etch): Difference between revisions

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In the case of the silicon etching on the ASE, an etch phase with SF<sub>6</sub> and O<sub>2</sub> alternates with a passivation phase with C<sub>4</sub>F<sub>8</sub>.
In the case of the silicon etching on the ASE, an etch phase with SF<sub>6</sub> and O<sub>2</sub> alternates with a passivation phase with C<sub>4</sub>F<sub>8</sub>.


=== The two standard silicon etch recipes ===


Two recipes have been optimized for the ASE. Their specification is on a 10 % etch load wafer with trenches.
==A rough overview of the performance of the RIE´s and some process related parameters==
* '''Shallolr''': The shallow etch process will etch a 2 <math>\mu</math>m opening down to make a 20 <math>\mu</math>m trench.
* '''Deepetch''': The deep etch process will etch a 50 <math>\mu</math>m opening down to make a 300 <math>\mu</math>m trench.
The standardization procedure on the ASE covers these two etches.


== Recipes on the ASE ==
{| border="2" cellspacing="0" cellpadding="10"  
 
=== Shallolr ===
 
The shallolr recipe is designed to etch features (with sizes above 1 <math>\mu</math>m) in silicon down to a depth that ranges from a few microns to some 50 microns. (If you need to etch deeper use Deepetch or more shallow, see Nanoetches.) It is specified to etch a 2 <math>\mu</math>m wide trench down to a depth of 20 <math>\mu</math>m on a wafer that has a global/local etch opening density of 10%.
 
The recipe is given below.
 
{| border="2" cellpadding="2" cellspacing="1"
|+ The shallolr recipe
|-
! colspan="2" align="center"| Common parameters
! colspan="3" align="center"| Multiplexed parameters
|-
! Parameter 
! Setting
! Parameter
! Etch
! Passivation
|-
! Temperature
| 10<sup>o</sup>C
! SF<sub>6</sub> Flow
| 260 sccm
| 0 sccm
|-
! No. of cycles
| 31
! O<sub>2</sub> Flow
| 26 sccm
| 0 sccm
|-
! Process time
| 5:56 mins
! C<sub>4</sub>F<sub>4</sub> Flow
| 0 sccm
| 120 sccm
|-
! APC mode
| manual
! RF coil
| 2800 W
| 1000 W
|-
! APC setting
| 86.8 %
! RF Platen
| 16 W
| 0 W
|-
!
|
! Cycle time
| 6.5 s
| 5 s
|}
 
The process runs for 31 cycles (5:56 mins). The fact that it's Bosch process is clear from the scallops on the sidewalls - one should be able to count 31 of them.
 
<gallery caption="Standardization images of the shallolr recipe" widths="300px" heights="300px" perrow="2">
Image:jmlshal070921 pos1 2mu_09.jpg|The profile of a 2 <math>\mu</math>m trench
image:jmlshal070921 pos1 50mu_08.jpg|The profile of a 50 <math>\mu</math>m trench
</gallery>
 
The process is designed to reach 20 <math>\mu</math>m down in a 2 <math>\mu</math>m trench but as is clear from the image of the corresponding 50 <math>\mu</math>m trench, this one is etched deeper. The reason is the so called Aspect Ratio Dependent Etching or ARDE: See below.
 
=== Deepetch ===
 
The deepetch recipe is designed to etch features (with sizes 2 <math>\mu</math>m) in silicon down to a depth that ranges from some 50 microns to hundreds of microns. (If you need to etch less, use shallow or Nanoetches.) It is specified to etch a 50 <math>\mu</math>m wide trench down to a depth of 300 <math>\mu</math>m on a wafer that has a global/local etch density of 10%.
 
The recipe is given below.
 
{| border="2" cellpadding="2" cellspacing="1"
|+ The deepetch recipe
|-
! colspan="2" align="center"| Common parameters
! colspan="3" align="center"| Multiplexed parameters
|-
|-
! Parameter 
!style="background:silver; color:black;" align="left"|Purpose
! Setting
|style="background:LightGrey; color:black"|Dry etch of ||style="background:WhiteSmoke; color:black"|
! Parameter
*Silicon
! Etch
*Silicon oxide
! Passivation
*Silicon (oxy)nitride
|-
|-
! Temperature
!style="background:silver; color:black" align="left"|Performance
| 20<sup>o</sup>C
|style="background:LightGrey; color:black"|Etch rates||style="background:WhiteSmoke; color:black"|
! SF<sub>6</sub> Flow
*Silicon: ~0.04-0.8 µm/min
| 230 sccm
*Silicon oxide:~0.02-0.15 µm/min
| 0 sccm
*Silicon (oxy)nitride:~0.02-? µm/min
|-
|-
! No. of cycles
|style="background:silver; color:black" |.||style="background:LightGrey; color:black"|Anisotropy||style="background:WhiteSmoke; color:black"|
| 250
*Can vary from isotropic to anisotropic with vertical sidewalls and on to a physical etch were the sidewalls are angled but without etching under the mask.
! O<sub>2</sub> Flow
| 23 sccm
| 0 sccm
|-
|-
! Process time
!style="background:silver; color:black" align="left"|Process parameter range
| 54:10 mins
|style="background:LightGrey; color:black"|Process pressure||style="background:WhiteSmoke; color:black"|
! C<sub>4</sub>F<sub>4</sub> Flow
*~20-200 mTorr
| 0 sccm
| 120 sccm
|-
|-
! APC mode
|style="background:silver; color:black"|.||style="background:LightGrey; color:black"|Gas flows
| manual
|style="background:WhiteSmoke; color:black"|
! RF coil
*SF<math>_6</math>: 0-130 sccm
| 2800 W
*O<math>_2</math>: 0-100 sccm
| 1000 W
*CHF<math>_3</math>: 0-100 sccm
*CF<math>_4</math>: 0-84 sccm
*H<math>_2</math>: ?sccm
*Ar: 0-145 sccm
*N<math>_2</math>: 0-100 sccm
*C<math>_2</math>F<math>_6</math>: 0-24 sccm
|-
|-
! APC setting
!style="background:silver; color:black" align="left"|Substrates
| 87.7 %
|style="background:LightGrey; color:black"|Batch size
! RF Platen
|style="background:WhiteSmoke; color:black"|
| 19 W
*1 4" wafer per run
| 0 W
*1 2" wafer per run
*Or several smaller pieces
|-
|-
!
|style="background:silver; color:black"|.|| style="background:LightGrey; color:black"|Substrate material allowed
|
|style="background:WhiteSmoke; color:black"|
! Cycle time
*Silicon wafers
| 8 s
**with layers of silicon oxide or silicon (oxy)nitride
| 5 s
*Quartz wafers
|-
|style="background:silver; color:black"|.|| style="background:LightGrey; color:black"|Possible masking material
|style="background:WhiteSmoke; color:black"|
*Photoresist/e-beam resist
*Silicon/PolySi
*Silicon oxide or silicon (oxy)nitride
*Aluminium
*Other metals if the coverage is <5% of the wafer area (ONLY PECVD3!)
|-
|}
|}
<gallery caption="Standardization images of the deepetch recipe" widths="300px" heights="300px" perrow="2">
Image:jmldeep071101 pos1 2mu_010.jpg|The profile of a 2 <math>\mu</math>m trench
image:jmldeep071101 pos5 50mu_013.jpg|The profile of a 50 <math>\mu</math>m trench
</gallery>
As is clear from the two images ARDE also plays a role in this case: The 2 <math>\mu</math>m trench (widened to about 5-6 <math>\mu</math>m because of undercut/underetching) is only etched 150 <math>\mu</math>m.
== Standardization procedure on the ASE ==