Specific Process Knowledge/Thin film deposition/Physimeca: Difference between revisions
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Physimeca is a system for deposition of metals through electron-beam evaporation. | Physimeca is a system for deposition of metals through electron-beam evaporation. | ||
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[http://www.labmanager.danchip.dtu.dk/function.php?module=Machine&view=view&mach=151 Physimeca in LabManager] | [http://www.labmanager.danchip.dtu.dk/function.php?module=Machine&view=view&mach=151 Physimeca in LabManager] | ||
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==Equipment performance and process related parameters Physimeca== | ==Equipment performance and process related parameters Physimeca== | ||
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'''*''' ''For thicknesses above 2000 Å special permission is required (contact thinfilm@nanolab.dtu.dk).'' | '''*''' ''For thicknesses above 2000 Å special permission is required (contact thinfilm@nanolab.dtu.dk).'' | ||
== | ==Calibration of Physimeca (''experienced users only'')== | ||
As of 16/6/2008, we will use a new system to compensate for "drift" without having to change e.g. 20 gold programs for each refilling. | |||
The power setting during deposition is a fraction of the "auto-emission current" on the genius system. | |||
In order to compensate for drift in the system the auto and max emission current on the genius is adjusted to achieve the rates at the set powers below | |||
This way it should not be necessary to adjust the programs every time, but experienced users will have to occasionally adjust the genius setting. | |||
{| border="2" cellspacing="0" cellpadding="4" | |||
| rowspan=2 |Reference deposition (step) | |||
| rowspan=2 |Material | |||
| rowspan=2 |Pocket | |||
| rowspan=2 |Rate (Å/s) | |||
| rowspan=2 |At power (%) | |||
| colspan="2" align="center"| Example of max emission current (6-2008) | |||
|- | |||
| mA | |||
| ~mA for rate | |||
|- | |||
| Ti100nm-5A-cal | |||
| Ti | |||
| 1 | |||
| 5 | |||
| 70 | |||
| 160 | |||
| 112 | |||
|- | |||
| Pt100nm-5A-cal | |||
| Pt | |||
| 2 | |||
| 5 | |||
| 80 | |||
| 460 | |||
| 368 | |||
|- | |||
| Au100nm-10A-cal | |||
| Au | |||
| 3 | |||
| 10 | |||
| 80 | |||
| 450 | |||
| 360 | |||
|- | |||
| Ni100nm-5A-cal | |||
| Ni | |||
| 4 | |||
| 5 | |||
| 70 | |||
| 250 | |||
| 175 | |||
|- | |||
| Ge100nm-5A-cal | |||
| Ge | |||
| 5 | |||
| 5 | |||
| 70 | |||
| 190 | |||
| 133 | |||
|- | |||
| Cr100nm-5A-cal | |||
| Cr | |||
| 6 | |||
| 5 | |||
| 70 | |||
| 110 | |||
| 77 | |||
|- | |||
| Pd100nm-5A-cal | |||
| Pd | |||
| 6 | |||
| 5 | |||
| 70 | |||
| 160 | |||
| 112 | |||
|- | |||
|} | |||
The tooling factor has been determined to ~110 for 100nm layers (lot, 6-2008). It will of course have a small dependence on material and rate. | |||
You can use the steps above as starting point when making new programs (other thicknesses, rates, tilt etc.) | |||
== Changing Auto and Emission Current (''experienced users only'') == | |||
If the actual power during deposition is significantly different than the target value (e.g. off by a few % you may change the genius values). | |||
Calculate new auto emission current: Inew="good" current during deposition / target power, e.g. 167mA/0.7 = 240mA (new max emission) | |||
# Use genius remote: | |||
# Switch to manual mode. | |||
# Switch to chosen material | |||
# Go to set data and down to auto emission and max emission . | |||
# Change both to the new value and note this in the user log. | |||
# Go to save/load and save values | |||
# Switch back to remote mode on genius. | |||