Template:SEM comparison table 314: Difference between revisions

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*X Ray Analysis with EDS
*X Ray Analysis with EDS
*Crystallographic analysis using EBSD and both On and Off axis TKD
*Crystallographic analysis using EBSD and both On and Off axis TKD
* In-situ experiments with Heating and Gas injection
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*Conductive samples in High Vac
*Conductive samples in High Vac
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*Conductive samples in High Vac
*Conductive samples in High Vac
*Charge reduction in Low Vac
*Charge reduction in Low Vac
*X Ray Analysis with EDS and WDS
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*Conductive samples in High Vac
*Conductive samples in High Vac
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** 4.0nm at 30kV (BSE)
** 4.0nm at 30kV (BSE)
** > 12nm at 3kV (SE) -->
** > 12nm at 3kV (SE) -->
|B
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*High Vacuum operation in Mode II:
**1.0 nm at 15 kV (TLD detector and optimum working distance)
**1.8 nm at 1 kV (TLD detector and optimum working distance)
*Low Vacuum operation in Mode II:
**1.5 nm at 10 kV (Helix detector and optimum working distance)
**1.8 nm at 3 kV (Helix detector and optimum working distance)
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* High vacuum  
* High vacuum  
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**3.0 nm at 3 kV (SE)  
**3.0 nm at 3 kV (SE)  
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* Electron Column
* Electron Column Operation in Mode II
**0.8nm @15kV
**0.8nm @15kV
**0.9nm @1kV
**0.9nm @1kV
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* Z 50mm
* Z 50mm
* R 360⁰
* R 360⁰
* T 70⁰ Manua
* T 70⁰ Manual
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* X 150mm Piezo
* X 150mm Piezo

Latest revision as of 08:21, 26 March 2020

Equipment Nova QFEG AFEG Helios
Purpose
  • Conductive samples in High Vac
  • Charge reduction in Low Vac
  • X Ray Analysis with EDS
  • Crystallographic analysis using EBSD and both On and Off axis TKD
  • In-situ experiments with Heating and Gas injection
  • Conductive samples in High Vac
  • Charge reduction in Low Vac
  • Environmental control using Peltier stage
  • Cryogenic sample fixing/stabilization using cryo stage
  • X Ray Analysis with EDS
  • Conductive samples in High Vac
  • Charge reduction in Low Vac
  • X Ray Analysis with EDS and WDS
  • Conductive samples in High Vac
  • Micro and Nano milling/fabrication using various gases and FIB
  • X Ray Analysis with EDS
  • Crystallographic analysis using EBSD and Off Axis TKD
Equipment position Building 314 Room 060 Building 314 Room 011 Building 314 Room 034 Building 314 Room 061
Resolution The resolution of a SEM is strongly dependent on sample type and the operator. Resolution quoted is using sputtered gold on carbon
  • High Vacuum operation in Mode II:
    • 1.0 nm at 15 kV (TLD detector and optimum working distance)
    • 1.8 nm at 1 kV (TLD detector and optimum working distance)
  • Low Vacuum operation in Mode II:
    • 1.5 nm at 10 kV (Helix detector and optimum working distance)
    • 1.8 nm at 3 kV (Helix detector and optimum working distance)
  • High vacuum
    • 0.8 nm at 30 kV (STEM)
    • 1.0 nm at 30 kV (SE)
    • 2.5 nm at 30 kV (BSE) - 3.0 nm at 1 kV (SE)
  • High vacuum with beam deceleration option
    • 3.0 nm at 1 kV (BD mode + BSE)
  • Low vacuum - 1.4 nm at 30 kV (SE)
    • 2.5 nm at 30 kV (BSE)
    • 3.0 nm at 3 kV (SE)
  • Extended vacuum mode (ESEM)
    • 1.4 nm at 30 kV (SE)
  • High vacuum
    • 0.8 nm at 30 kV (STEM)
    • 1.0 nm at 30 kV (SE)
    • 2.5 nm at 30 kV (BSE) - 3.0 nm at 1 kV (SE)
  • High vacuum with beam deceleration option
    • 3.0 nm at 1 kV (BD mode + BSE)
  • Low vacuum - 1.4 nm at 30 kV (SE)
    • 2.5 nm at 30 kV (BSE)
    • 3.0 nm at 3 kV (SE)
  • Electron Column Operation in Mode II
    • 0.8nm @15kV
    • 0.9nm @1kV
  • Ion Column
    • 4.5nm @ 30kV
Detectors
  • ETD/TLD Secondary Electrons
  • BSED Back Scatter Electrons
  • LVD/LFD Low Vac SE
  • Helix Low Vac SE
  • EDS X Ray by energy
  • EBSD Electron Back Scatter Diffraction
  • TKD Transmission Kikuchi Diffraction
  • STEM Scanning Transmission Electron Microscopy
  • GAD Low Vac BSED
  • ETD Secondary Electrons
  • BSED Back Scatter Electrons
  • LVD/LFD Low Vac SE
  • GSED ESEM SE
  • EDS X Ray by energy
  • STEM Scanning Transmission Electron Microscopy
  • ETD Secondary Electrons
  • BSED Back Scatter Electrons
  • LVD/LFD Low Vac SE
  • GSED ESEM SE
  • EDS X Ray by energy
  • STEM Scanning Transmission Electron Microscopy
  • ETD/TLD Secondary Electrons
  • ABS Annular BSED
  • EDS X Ray by energy
  • EBSD Electron Back Scatter Diffraction
  • CDEM Continuos Dinode Electron Multiplier
Stage specifications
  • X 150mm Piezo
  • Y 150mm Piezo
  • Z 10mm
  • R 360⁰ Piezo
  • T 70⁰
  • X 50mm
  • Y 50mm
  • Z 50mm
  • R 360⁰
  • T 70⁰ Manual
  • X 50mm
  • Y 50mm
  • Z 50mm
  • R 360⁰
  • T 70⁰ Manual
  • X 150mm Piezo
  • Y 150mm Piezo
  • Z 10mm
  • R 360⁰ Piezo
  • T 70⁰
Options B C D E
Max sample size Consult with DTU Nanolab staff as weight, dimensions, pumping capacity and technique all play a roll in the sample size