LabAdviser/314/Microscopy 314-307/SEM/AFEG: Difference between revisions
No edit summary |
No edit summary |
||
(16 intermediate revisions by 2 users not shown) | |||
Line 1: | Line 1: | ||
'''Feedback to this page''': '''[mailto:labadviser@nanolab.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.nanolab.dtu.dk/index.php/LabAdviser/314/Microscopy_314-307/SEM/AFEG click here]''' | |||
''This section is written by DTU Nanolab internal if nothing else is stated.'' | |||
[[Category:314]] | |||
[[Category:314-Microscopy]] | |||
__FORCETOC__ | |||
=AFEG 250 Analytical ESEM (FEI Quanta FEG 250) = | =AFEG 250 Analytical ESEM (FEI Quanta FEG 250) = | ||
[[Image:DTU Nanolab AFEG.jpg|300x300px|right|thumb| DTU Nanolab AFEG positioned in B314 R034]] | |||
The AFEG is an FEI Quanta FEG 250(Field Emission Gun) scanning electron microscope with a spatial resolution of 2 nm for the ETD detector in high vacuum at 30 keV. The microscope can operate in high vacuum and low vacuum modes at room temperature. Our AFEG is fitted with EDS and WDS detectors, which allows for analytical measurements in all the operation modes. | The AFEG is an FEI Quanta FEG 250(Field Emission Gun) scanning electron microscope with a spatial resolution of 2 nm for the ETD detector in high vacuum at 30 keV. The microscope can operate in high vacuum and low vacuum modes at room temperature. Our AFEG is fitted with EDS and WDS detectors, which allows for analytical measurements in all the operation modes. | ||
Line 7: | Line 14: | ||
*'''Electron source''' | *'''Electron source''' | ||
Field emission gun | **Field emission gun | ||
*'''Accelerating voltage''' | *'''Accelerating voltage''' | ||
500 V- 30 kV | **500 V- 30 kV | ||
*'''Resolution''' | *'''Resolution''' | ||
2 nm at 30 kV (SE) | **2 nm at 30 kV (SE) | ||
*'''Imaging detectors''' | *'''Imaging detectors''' | ||
Everhart-Thornley (SE/BSE) | **Everhart-Thornley (SE/BSE) | ||
**Solid State BSE | |||
**Large Field (LVD) | |||
**Gaseous SE (GSED) | |||
**Gaseous BSE | |||
**Gaseous Analytical (GAD) | |||
**STEM | |||
**vCD | |||
*'''Imaging modes''' | *'''Imaging modes''' | ||
High and low vacuum | High and low vacuum | ||
*'''Analytical capabilities''' | *'''Analytical capabilities''' | ||
Energy dispersive X-rays (Oxford Instruments 50 mm2 X-Max silicon drift detector, MnKα resolution at 124 eV) | **Energy dispersive X-rays (Oxford Instruments 50 mm2 X-Max silicon drift detector, MnKα resolution at 124 eV) | ||
Wavelength Dispersive Spectrosopy | **Wavelength Dispersive Spectrosopy | ||
==Equipment performance and process related parameters== | ==Equipment performance and process related parameters== | ||
{| border="2" cellspacing="0" cellpadding="0" | {| border="2" cellspacing="0" cellpadding="0" | ||
!colspan="2" border="none" style="background:silver; color:black;" align="center |Equipment | !colspan="2" border="none" style="background:silver; color:black;" align="center |Equipment | ||
|style="background:WhiteSmoke; color:black" align="center"|FEI | |style="background:WhiteSmoke; color:black" align="center"|AFEG FEI Quanta FEG 250 | ||
|- | |- | ||
!style="background:silver; color:black;" align="center" width="60"| Purpose | !style="background:silver; color:black;" align="center" width="60"| Purpose | ||
Line 40: | Line 54: | ||
* 2 nm at 30 keV for Au on C sample with the ETD detector | * 2 nm at 30 keV for Au on C sample with the ETD detector | ||
|- | |- | ||
!style="background:silver; color:black" align="center" valign="center" rowspan=" | !style="background:silver; color:black" align="center" valign="center" rowspan="6"|Instrument specifics | ||
|style="background:LightGrey; color:black"|Detectors | |style="background:LightGrey; color:black"|Detectors | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
Line 69: | Line 83: | ||
|style="background:LightGrey; color:black"|EDS | |style="background:LightGrey; color:black"|EDS | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
* Oxford Instruments | * Oxford Instruments 50 mm<sup>2</sup> X-Max silicon drift detector, MnKα resolution at 124 eV | ||
|- | |- | ||
|style="background:LightGrey; color:black"|Operating pressures | |style="background:LightGrey; color:black"|Operating pressures | ||
Line 75: | Line 89: | ||
* High vacuum (10<sup>-4</sup> Pa), Low vacuum (10 to 200Pa) | * High vacuum (10<sup>-4</sup> Pa), Low vacuum (10 to 200Pa) | ||
|- | |- | ||
!style="background:silver; color:black" align="center" valign="center" rowspan="3"| | !style="background:silver; color:black" align="center" valign="center" rowspan="3"|Samples | ||
|style="background:LightGrey; color:black"|Sample sizes | |style="background:LightGrey; color:black"|Sample sizes | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
Line 82: | Line 96: | ||
| style="background:LightGrey; color:black"|Allowed materials | | style="background:LightGrey; color:black"|Allowed materials | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
* Conductors, Semiconductors,Insulators, Prepared Biological | * Conductors, Semiconductors,Insulators, Prepared Biological ((not pathogents!) | ||
|- | |- | ||
|} | |} | ||
Latest revision as of 09:11, 27 June 2023
Feedback to this page: click here
This section is written by DTU Nanolab internal if nothing else is stated.
AFEG 250 Analytical ESEM (FEI Quanta FEG 250)
The AFEG is an FEI Quanta FEG 250(Field Emission Gun) scanning electron microscope with a spatial resolution of 2 nm for the ETD detector in high vacuum at 30 keV. The microscope can operate in high vacuum and low vacuum modes at room temperature. Our AFEG is fitted with EDS and WDS detectors, which allows for analytical measurements in all the operation modes.
Process information
- Electron source
- Field emission gun
- Accelerating voltage
- 500 V- 30 kV
- Resolution
- 2 nm at 30 kV (SE)
- Imaging detectors
- Everhart-Thornley (SE/BSE)
- Solid State BSE
- Large Field (LVD)
- Gaseous SE (GSED)
- Gaseous BSE
- Gaseous Analytical (GAD)
- STEM
- vCD
- Imaging modes
High and low vacuum
- Analytical capabilities
- Energy dispersive X-rays (Oxford Instruments 50 mm2 X-Max silicon drift detector, MnKα resolution at 124 eV)
- Wavelength Dispersive Spectrosopy
Equipment | AFEG FEI Quanta FEG 250 | |
---|---|---|
Purpose | Vizualization and Microanalysis |
|
Performance | Resolution | The resolution of AFEG depends on the sample and the operation mode! |
| ||
Instrument specifics | Detectors |
|
Electron source |
| |
Stage (room temperature) |
| |
WDS |
| |
EDS |
| |
Operating pressures |
| |
Samples | Sample sizes |
|
Allowed materials |
|