Specific Process Knowledge/Characterization/Optical characterization: Difference between revisions
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'''Feedback to this page''': '''[mailto:labadviser@nanolab.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.nanolab.dtu.dk/index.php/Specific_Process_Knowledge/Characterization/Optical_characterization click here]''' | |||
The ellipsometer VASE is a | [[Category: Equipment |Characterization Optical]] | ||
The ellipsometer M2000V is | [[Category: Characterization|Optical]] | ||
==Comparison of the methods== | |||
For comparison of the methods for measuring optical constants and film thickness, see here: [[Specific Process Knowledge/Characterization/Measurement of film thickness and optical constants#Film_thickness_and_optical_constants_of_optical_transparent_films|Film thickness and optical constants of optical transparent films]] | |||
==Ellipsometer VASE and Ellipsometer M-2000V == | |||
''This section is written by Berit Herstrøm @ DTU Nanolab'' | |||
[[image:Ellipsometer_VASE_image.JPG|275x275px|right|thumb|Ellipsometer VASE: positioned in cleanroom A-1, {{photo1}}]] | |||
The ellipsometer VASE is actually a M2000XI-210 ellipsometer from J.A. Woollam Co., Inc.. We call it VASE (Variable Angle Spectroscopic Ellipsometry) because it can do spectroscopic ellipsometry at variable angles. <br/> | |||
The ellipsometer M2000V is an in-situ ellipsometer from J.A. Wollam Co., Inc. This dedicated for being used on the Sputter System Lesker instrument or the ALD2 for in-situ measurements. When it is not on any system it is positioned next to the ALD2. | |||
Ellipsometry is a very sensitive characterization technique which can be used to determine thin film layer thicknesses and/or optical constants. It sends in polarized light on the surface at different angles and measures the change in polarization state of the reflected light. | Ellipsometry is a very sensitive characterization technique which can be used to determine thin film layer thicknesses and/or optical constants. It sends in polarized light on the surface at different angles and measures the change in polarization state of the reflected light. | ||
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Ellipsometry is an indirect measurement so a model has to be fit to the data in order to obtain the film thickness and optical constants. To learn more about ellipsometry you can take a look at the [http://www.jawoollam.com/tutorial_1.html tutorial] provided by the J. A. Woollam Co. | Ellipsometry is an indirect measurement so a model has to be fit to the data in order to obtain the film thickness and optical constants. To learn more about ellipsometry you can take a look at the [http://www.jawoollam.com/tutorial_1.html tutorial] provided by the J. A. Woollam Co. | ||
'''The user | Access to use the CompleteEASE software can be found using Remote Desktop connection to: DTU-8CC0321MFL (you can only log on when you have the user competences in LabManager) or log on to https://remote.dtu.dk. There should be a connection via Citrix to DTU-8CC0321MFL. You will be prompted for user/password. | ||
'''The user manuals, quality control procedure and results and contact information can be found in LabManager:''' | |||
<!-- remember to remove the type of documents that are not present --> | <!-- remember to remove the type of documents that are not present --> | ||
<!-- give the link to the equipment info page in LabManager: --> | <!-- give the link to the equipment info page in LabManager: --> | ||
[http://labmanager | [http://labmanager.dtu.dk/function.php?module=Machine&view=view&mach=316 LabManager page for Ellipsometer VASE] <br/> | ||
[http://labmanager | [http://labmanager.dtu.dk/function.php?module=Machine&view=view&mach=261 LabManager page for Ellipsometer M-2000V] | ||
<br clear="all" /> | <br clear="all" /> | ||
===More details=== | |||
* Before training: | |||
** First go through the Woollam short tutorial: [http://www.jawoollam.com/tutorial_1.html tutorial] | |||
** Second watch our training video: [https://www.youtube.com/watch?v=EC-oyRhKr0A Training Video] | |||
** To get more understanding - short intro from ''Quantum Design - Europe'': [https://qd-europe.com/dk/en/product/short-introduction-ellipsometry/] - ''optional'' | |||
*[[/advanced ellipsometry|Examples of advanced use of the ellipsometer]] | |||
===A rough overview of the performance of the Ellipsometers=== | ===A rough overview of the performance of the Ellipsometers=== | ||
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!colspan="2" border="none" style="background:silver; color:black;" align="center"|Equipment | !colspan="2" border="none" style="background:silver; color:black;" align="center"|Equipment | ||
|style="background:WhiteSmoke; color:black"|<b>Ellipsometer VASE</b> | |style="background:WhiteSmoke; color:black"|<b>Ellipsometer VASE (M2000XI)</b> | ||
|style="background:WhiteSmoke; color:black"|<b>Ellipsometer M-2000V</b> | |style="background:WhiteSmoke; color:black"|<b>Ellipsometer M-2000V</b> | ||
|- | |- | ||
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|- | |- | ||
!style="background:silver; color:black" align="center" valign="center" rowspan="2"|Performance | !style="background:silver; color:black" align="center" valign="center" rowspan="2"|Performance | ||
|style="background:LightGrey; color:black"| | |style="background:LightGrey; color:black"|Films that can be examined | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
* | Any film that is transparent to the light in the given wavelength range | ||
* | e.g.: | ||
*Silicon Oxide | |||
*Silicon nitride | |||
*PolySilicon | |||
*Resists | |||
*Polymers | |||
*Very thin layers of metals | |||
*and many more | |||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
* | Any film that is transparent to the light in the given wavelength range | ||
* | e.g.: | ||
* | *Silicon Oxide | ||
*Silicon nitride | |||
*PolySilicon | |||
*Resists | |||
*Polymers | |||
*Very thin layers of metals | |||
*and many more | |||
|- | |- | ||
|style="background:LightGrey; color:black"| | |style="background:LightGrey; color:black"|Film thickness range | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
* | *~20Å to 2 µm (depending of the material) | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
* | *~20Å to 2 µm (depending of the material) | ||
|- | |- | ||
!style="background:silver; color:black" align="center" valign="center" rowspan=" | !style="background:silver; color:black" align="center" valign="center" rowspan="4"|Process parameter range | ||
|style="background:LightGrey; color:black"|Wavelength range | |style="background:LightGrey; color:black"|Wavelength range | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
*210nm-1690nm | *210nm-1690nm | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
* | *370nm-1000nm | ||
|- | |- | ||
|style="background:LightGrey; color:black"|Incident angle range | |style="background:LightGrey; color:black"|Incident angle range | ||
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*2mm (spot size on sample depends on the angle) | *2mm (spot size on sample depends on the angle) | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
*5mm (spot size on the sample depends on the angle | *5mm (spot size on the sample depends on the angle) | ||
|- | |||
|style="background:LightGrey; color:black"|Mapping facility | |||
|style="background:WhiteSmoke; color:black"| | |||
*Can make wafermaps on up to 150mm wafers | |||
|style="background:WhiteSmoke; color:black"| | |||
*No mapping facility | |||
|- | |- | ||
!style="background:silver; color:black" align="center" valign="center" rowspan="2"|Accessories | !style="background:silver; color:black" align="center" valign="center" rowspan="2"|Accessories | ||
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|} | |} | ||
<br clear="all" /> | |||
==Filmtek 4000== | |||
{{CC-bghe2}} | |||
[[image:Filmtek.JPG|275x275px|right|thumb|FilmTek 4000: positioned in cleanroom A-1, {{photo1}}]] | |||
FilmTek 4000 is a computerized film thickness measurement and material characterization system. This system combines fiber-optic spectrophotometry with advanced material modeling software to provide an affordable and reliable tool for the simultaneous measurement of film thickness, index of refraction, and extinction coefficient | |||
Normal incidence and polarized 70 degree reflection data is collected and used to calculate thickness and index of refraction of the measured film using SCI’s patented Differential Power Spectral Density (DPSD) technique. Absolute reflection data is obtained by comparing sample data to the measured reflection of a known reference sample, typically a silicon wafer with a thermally grown thin oxide (~63 nm) film. | |||
The spectrophotometer scans the sample over a predefined range of wavelengths. The software generates a reflection spectrum based on a previously stored reference scan, and then performs a regression on the unknown parameters to fit the simulated reflection and power spectral density to the observed values. The resulting thin film parameters along with the measured and modeled spectra are then displayed for the user to examine. | |||
'''The user manual, quality control procedure and results, technical information and contact information can be found in LabManager:''' | |||
[http://labmanager.dtu.dk/function.php?module=Machine&view=view&mach=169 FilmTek in LabManager] | |||
<br clear="all" /> | |||
===An overview of the performance of the FilmTek=== | |||
{| border="2" cellspacing="0" cellpadding="10" | {| border="2" cellspacing="0" cellpadding="10" | ||
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*Measurement of (multi layer) film thickness (only one unknown layer) | *Measurement of (multi layer) film thickness (only one unknown layer) | ||
*Optical constants | *Optical constants | ||
*Surface roughness | |||
|- | |- | ||
!style="background:silver; color:black" align="left"|Performance | !style="background:silver; color:black" align="left"|Performance | ||
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*Silicon Oxide | *Silicon Oxide | ||
*Silicon nitride | *Silicon nitride | ||
*PolySilicon | *PolySilicon | ||
*Photoresists | *Photoresists | ||
*SU8 | *SU8 | ||
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|style="background:LightGrey; color:black"|Film thickness range | |style="background:LightGrey; color:black"|Film thickness range | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
* | *<100 Å to 250 µm (depending of the material) | ||
|- | |- | ||
!style="background:silver; color:black" align="left"|Process parameter range | !style="background:silver; color:black" align="left"|Process parameter range | ||
|style="background:LightGrey; color:black"|Wavelength range | |style="background:LightGrey; color:black"|Wavelength range | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
* | *400-1000 nm | ||
|- | |- | ||
!style="background:silver; color:black" align="left"|Substrates | !style="background:silver; color:black" align="left"|Substrates | ||
|style="background:LightGrey; color:black"|Batch size | |style="background:LightGrey; color:black"|Batch size | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
*One sample at a time - all sample larger than | *One sample at a time - all sample larger than 5x5 mm<sup>2</sup>sizes up to 6" | ||
|- | |- | ||
|style="background:silver; color:black"| | |style="background:silver; color:black"| | ||
|style="background:LightGrey; color:black"|Substrate material allowed | | style="background:LightGrey; color:black"|Substrate material allowed | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
*In principle all materials | *In principle all materials | ||
*Only pure silicon, silicon oxides, silicon nitrides and quartz may be in direct contact with the surface of the stage. If you have metals, III-V materials or polymers on the back side of the substrate the please mount your sample on a silicon carrier wafer. | |||
|- | |- | ||
|} | |} | ||
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<br clear="all" /> | <br clear="all" /> | ||
== | <!-- | ||
[[image: | ==Prism Coupler== | ||
[[image:Prism_coupler.jpg|300x300px|right|thumb|Prism coupler: (old image), now positioned cleanroom D-3]] | |||
The Prism coupler is a Metricon model 2010 Prism Coupler. It is an old system from 1991 but the system with a few modifications is still beening manufactured today. It is still a very easy and relaible method of determining thickness and refractive index. | |||
The prism coupler uses an optical waveguide technique to determine the thickness and refractive index of a thin film. To learn more about the theory of measurement please see the homepage of [http://www.metricon.com Metricon] | |||
It is especially good for making fast accurate measurements of dielectric thin films with n<2.02 and a thickness range of 1 µm to about 15 µm. | |||
'''The user manual, quality control procedure and results, technical information and contact information can be found in LabManager:''' | |||
[http://labmanager.danchip.dtu.dk/function.php?module=Machine&view=view&mach=12 Prism Coupler in LabManager] | |||
<br clear="all" /> | <br clear="all" /> | ||
===An overview of the performance of the | |||
===An overview of the performance of the Prism Coupler=== | |||
{| border="2" cellspacing="0" cellpadding="10" | {| border="2" cellspacing="0" cellpadding="10" | ||
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!style="background:silver; color:black;" align="left"|Purpose | !style="background:silver; color:black;" align="left"|Purpose | ||
|style="background:LightGrey; color:black"|Film thickness measurements and optical characterization of optically transparent thin films||style="background:WhiteSmoke; color:black"| | |style="background:LightGrey; color:black"|Film thickness measurements and optical characterization of optically transparent thin films||style="background:WhiteSmoke; color:black"| | ||
*Measurement of | *Measurement of film thickness | ||
*Optical constants | *Optical constants | ||
|- | |- | ||
!style="background:silver; color:black" align="left"|Performance | !style="background:silver; color:black" align="left"|Performance | ||
|style="background:LightGrey; color:black"|Thin film materials that can be measured||style="background:WhiteSmoke; color:black"| | |style="background:LightGrey; color:black"|Thin film materials that can be measured||style="background:WhiteSmoke; color:black"| | ||
Film with a refractive index of less than 2.02 and that are transparent to the light in the given wavelength range | |||
ex: | ex: | ||
*Silicon Oxide | *Silicon Oxide | ||
*Silicon nitride | *Silicon nitride | ||
* | *polymers | ||
|- | |- | ||
|style="background:silver; color:black"| | |style="background:silver; color:black"| | ||
|style="background:LightGrey; color:black"|Film thickness range | |style="background:LightGrey; color:black"|Film thickness range | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
* | *~1µm to 15 µm | ||
|- | |||
|style="background:silver; color:black"| | |||
|style="background:LightGrey; color:black"|Film thickness accuracy | |||
|style="background:WhiteSmoke; color:black"| | |||
*±(0.5%+50Å) | |||
|- | |||
|style="background:silver; color:black"| | |||
|style="background:LightGrey; color:black"|Index accuracy | |||
|style="background:WhiteSmoke; color:black"| | |||
*±0.001 | |||
|- | |- | ||
!style="background:silver; color:black" align="left"|Process parameter range | !style="background:silver; color:black" align="left"|Process parameter range | ||
|style="background:LightGrey; color:black"|Wavelength range | |style="background:LightGrey; color:black"|Wavelength range | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
* | Can operate at two different wavelength: | ||
*633 nm | |||
*1550 nm (not working) | |||
|- | |- | ||
!style="background:silver; color:black" align="left"|Substrates | !style="background:silver; color:black" align="left"|Substrates | ||
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|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
*In principle all materials | *In principle all materials | ||
|- | |- | ||
|} | |} | ||
--> | |||
<!-- | |||
==F10-RT reflectometer, transmitance, film thickness measurements == | |||
[[image:F10-RT.JPG|275x275px|right|thumb|F10-RT: positioned in basement project lab]] | |||
F10-RT is a combined reflectance and transmittance measurement system that can also use the reflectance measurements to get the film thickness of transparent thin films. This system combines fiber-optic spectrophotometry with material modeling software to provide an affordable tool for the measurement of reflectance, transmitance and film thickness. | |||
Reflectance and transmittance spectra can be obtained simultaneously. | |||
Normal incidence reflection data is collected and used to calculate thickness and index of refraction of the measured film. Absolute reflection data is obtained by comparing sample data to the measured reflection of a known reference sample. | |||
The spectrophotometer scans the sample over a predefined range of wavelengths. The software generates a reflection spectrum based on a previous measured reference scan, and then performs a regression on the unknown parameters to fit the simulated reflection. The resulting thin film parameters along with the measured and modeled spectra are then displayed for the user to examine. | |||
'''The user manual, quality control procedure and results, technical information and contact information can be found in LabManager:''' | |||
[http://labmanager.dtu.dk/function.php?module=Machine&view=view&mach=466 F10-RT in LabManager] | |||
<br clear="all" /> | <br clear="all" /> | ||
===An overview of the performance of the | ===An overview of the performance of the F10-RT=== | ||
{| border="2" cellspacing="0" cellpadding="10" | {| border="2" cellspacing="0" cellpadding="10" | ||
|- | |- | ||
!style="background:silver; color:black;" align="left"|Purpose | !style="background:silver; color:black;" align="left"|Purpose | ||
|style="background:LightGrey; color:black"| | |style="background:LightGrey; color:black"|Reflectance, transmittance and film thickness measurements optically transparent thin films | ||
|style="background:WhiteSmoke; color:black"|[[:File:Filmetrics Datasheet - F10-RT b3M.pdf |See the datasheet here]] | |||
|- | |- | ||
!style="background:silver; color:black" align="left"|Performance | !style="background:silver; color:black" align="left"|Performance | ||
|style="background:LightGrey; color:black"|Thin film materials that can be measured||style="background:WhiteSmoke; color:black"| | |style="background:LightGrey; color:black"|Thin film materials that can be measured||style="background:WhiteSmoke; color:black"| | ||
Reflectance: any flat surface larger than 6mm <br> | |||
Transmittance: any flat transparent material larger then 6mm <br> | |||
Thin film thickness: Any film that is transparent to the light in the given wavelength range | |||
ex: | ex: | ||
*Silicon Oxide | *Silicon Oxide | ||
*Silicon nitride | *Silicon nitride | ||
*polymers | *PolySilicon | ||
*Photoresists | |||
*SU8 | |||
*Other polymers | |||
*and many more | |||
|- | |- | ||
|style="background:silver; color:black"| | |style="background:silver; color:black"| | ||
|style="background:LightGrey; color:black"|Film thickness range | |style="background:LightGrey; color:black"|Film thickness range | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
* | *15 nm to 70 µm (depending of the material) | ||
*min 100nm (to measure n and k) | |||
|- | |- | ||
|style="background:silver; color:black"| | |style="background:silver; color:black"| | ||
|style="background:LightGrey; color:black"| | |style="background:LightGrey; color:black"|Probe spot size | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
* | *6 mm | ||
|- | |- | ||
|style="background:silver; color:black"| | |style="background:silver; color:black"| | ||
|style="background:LightGrey; color:black"| | |style="background:LightGrey; color:black"|Sample orientation | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
* | *Face down | ||
|- | |- | ||
!style="background:silver; color:black" align="left"|Process parameter range | !style="background:silver; color:black" align="left"|Process parameter range | ||
|style="background:LightGrey; color:black"|Wavelength range | |style="background:LightGrey; color:black"|Wavelength range | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
*380-1050 nm | |||
* | |||
|- | |- | ||
!style="background:silver; color:black" align="left"|Substrates | !style="background:silver; color:black" align="left"|Substrates | ||
|style="background:LightGrey; color:black"|Batch size | |style="background:LightGrey; color:black"|Batch size | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
*One sample at a time - all sample larger than | *One sample at a time - all sample larger than a diameter of 6 mm sizes up to 6" | ||
|- | |- | ||
|style="background:silver; color:black"| | |style="background:silver; color:black"| | ||
| style="background:LightGrey; color:black"|Substrate material allowed | | style="background:LightGrey; color:black"|Substrate material allowed | ||
|style="background:WhiteSmoke; color:black"| | |style="background:WhiteSmoke; color:black"| | ||
*In principle all materials | *In principle all materials as long as they do not leave residuals on the system | ||
|- | |- | ||
|} | |} | ||
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Latest revision as of 10:31, 6 September 2024
Feedback to this page: click here
Comparison of the methods
For comparison of the methods for measuring optical constants and film thickness, see here: Film thickness and optical constants of optical transparent films
Ellipsometer VASE and Ellipsometer M-2000V
This section is written by Berit Herstrøm @ DTU Nanolab
The ellipsometer VASE is actually a M2000XI-210 ellipsometer from J.A. Woollam Co., Inc.. We call it VASE (Variable Angle Spectroscopic Ellipsometry) because it can do spectroscopic ellipsometry at variable angles.
The ellipsometer M2000V is an in-situ ellipsometer from J.A. Wollam Co., Inc. This dedicated for being used on the Sputter System Lesker instrument or the ALD2 for in-situ measurements. When it is not on any system it is positioned next to the ALD2.
Ellipsometry is a very sensitive characterization technique which can be used to determine thin film layer thicknesses and/or optical constants. It sends in polarized light on the surface at different angles and measures the change in polarization state of the reflected light.
It is especially good for thin films in the thickness range of a few nanometers to a few microns. The layer should be transparent to light in the usable wavelength range for the thickness to be determined. Large roughness (>40nm) and features within the field of view can cause the measurement to fail.
Ellipsometry is an indirect measurement so a model has to be fit to the data in order to obtain the film thickness and optical constants. To learn more about ellipsometry you can take a look at the tutorial provided by the J. A. Woollam Co.
Access to use the CompleteEASE software can be found using Remote Desktop connection to: DTU-8CC0321MFL (you can only log on when you have the user competences in LabManager) or log on to https://remote.dtu.dk. There should be a connection via Citrix to DTU-8CC0321MFL. You will be prompted for user/password.
The user manuals, quality control procedure and results and contact information can be found in LabManager:
LabManager page for Ellipsometer VASE
LabManager page for Ellipsometer M-2000V
More details
- Before training:
- First go through the Woollam short tutorial: tutorial
- Second watch our training video: Training Video
- To get more understanding - short intro from Quantum Design - Europe: [1] - optional
- Examples of advanced use of the ellipsometer
A rough overview of the performance of the Ellipsometers
Equipment | Ellipsometer VASE (M2000XI) | Ellipsometer M-2000V | |
---|---|---|---|
Purpose |
|
| |
Performance | Films that can be examined |
Any film that is transparent to the light in the given wavelength range e.g.:
|
Any film that is transparent to the light in the given wavelength range e.g.:
|
Film thickness range |
|
| |
Process parameter range | Wavelength range |
|
|
Incident angle range |
|
| |
Beam size |
|
| |
Mapping facility |
|
| |
Accessories | Focusing optics |
|
|
Transmission stage |
|
| |
Substrates | Batch size |
|
|
Allowed materials |
|
|
Filmtek 4000
Unless otherwise stated, all content in this section was done by Berit Herstrøm, DTU Nanolab
FilmTek 4000 is a computerized film thickness measurement and material characterization system. This system combines fiber-optic spectrophotometry with advanced material modeling software to provide an affordable and reliable tool for the simultaneous measurement of film thickness, index of refraction, and extinction coefficient
Normal incidence and polarized 70 degree reflection data is collected and used to calculate thickness and index of refraction of the measured film using SCI’s patented Differential Power Spectral Density (DPSD) technique. Absolute reflection data is obtained by comparing sample data to the measured reflection of a known reference sample, typically a silicon wafer with a thermally grown thin oxide (~63 nm) film.
The spectrophotometer scans the sample over a predefined range of wavelengths. The software generates a reflection spectrum based on a previously stored reference scan, and then performs a regression on the unknown parameters to fit the simulated reflection and power spectral density to the observed values. The resulting thin film parameters along with the measured and modeled spectra are then displayed for the user to examine.
The user manual, quality control procedure and results, technical information and contact information can be found in LabManager:
An overview of the performance of the FilmTek
Purpose | Film thickness measurements and optical characterization of optically transparent thin films |
|
---|---|---|
Performance | Thin film materials that can be measured |
Any film that is transparent to the light in the given wavelength range ex:
|
Film thickness range |
| |
Process parameter range | Wavelength range |
|
Substrates | Batch size |
|
Substrate material allowed |
|