Jump to content

Specific Process Knowledge/Characterization/Topographic measurement: Difference between revisions

Bghe (talk | contribs)
Reet (talk | contribs)
 
(62 intermediate revisions by 7 users not shown)
Line 1: Line 1:
'''Feedback to this page''': '''[mailto:Characterization@danchip.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.danchip.dtu.dk/index.php?title=Specific_Process_Knowledge/Characterization/Topographic_measurement&action=edit click here]'''
{{cc-nanolab}}


'''Feedback to this page''': '''[mailto:Characterization@nanolab.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.nanolab.dtu.dk/index.php/Specific_Process_Knowledge/Characterization/Topographic_measurement click here]'''
<br>
<br>
=Topographic measurements=
Topographic measurements are measurements of height differences on your sample. If you measure many spots on the sample you can get a topographic image of the surface.


Topographic measurements are measurements were you can measure hight differences on your substrate. If you measure in many spots of the substrate you can get a topographic image of the substrate.
At DTU Nanolab we have eight systems for topographic measurements:
*Stylus profilers (P17, Dektak XTA, Dektak 150 and Dektak 3ST) - ''Profilers for mechanically measuring topography''
*Optical profilers (Optical profiler Sensofar and Optical profiler Filmetrics) - ''3D Profilers for optically measuring topography''
*AFMs (AFM Icon-PT1 and AFM Icon-PT2) - ''AFMs for "mechanically" measuring topography (nano-regime)''
<br>
==High Aspect Ratio Structures==
The fact that the stylus tip of a stylus profiler or an AFM is shaped like a cone with some finite tip angle causes a problem when characterizing high aspect ratio structures. For instance, if a 20 µm wide trench is etched deeper than approximately 18 µm, the tip of the Dektak will not be able to reach the bottom. The optical profiler uses a light beam that is focused through an objective. Therefore it is able to measure higher aspect ratios. The aspect ratio is limited by the possibility for the light to reach the bottom and get back to the detector. On some samples we have been able to measure aspect ratios above 1:10. Otherwise the solution is to cleave the sample along a line that is perpendicular to the trench and then inspect the profile in a [[Specific Process Knowledge/Characterization/SEM: Scanning Electron Microscopy|scanning electron microscope]] or a microscope (for large structures).
<br>
<br>


AT DANCHIP we have four systems for topographic measurement:
==Thin Film Thickness==
*Dektak (there are two systems) - ''Profiler for measuring micro structures''
The profilers can be used to measure the thickness of optically transparent thin films or etched non-transparent thin films. There are also other options for measuring film thickness. All the methods are compared on the [[Specific Process Knowledge/Characterization/Measurement of film thickness and optical constants| "Measurement of Thin Film Thickness and Optical Constants"]] page.
*Optical Profiler (Sensofar) - ''3D Profiler for measuring micro structures''
<br>
*Nanoman - ''AFM for measuring nano structures''
<br>


'''High Aspect ratio structures'''<br/>
=Comparison of Stylus Profilers, Optical Profilers and AFMs at Nanolab=
The fact that the tips of the Dektak profilers and the AFM are shaped like a cone with some tip angle causes a problem when characterizing high aspect ratio structures. For instance, if a 20 µm wide trench is etched deeper than approximately 18 µm, the tip of the Dektak will not be able to reach the bottom. The optical profiler uses a light beam that is focused through an objective. Therefore it is able to measure higher aspect ratios. The aspect ratio is limited by the posibility for the light to reach the bottom and get back to the detector. On some samples we have been able to measure aspect ratios above 1:10. Otherwise the solution is to cleave the sample along a line that is perpendicular to the trench and then inspect the profile in a [[Specific Process Knowledge/Characterization/SEM: Scanning Electron Microscopy|scanning electron microscope]] or a microscope (for large structures).
 
 
===Comparison of the two profilers and the AFM===
{| border="2" cellspacing="0" cellpadding="4" align="center"
!
![[Specific Process Knowledge/Characterization/Profiler#Dektak_8_stylus_profiler|Dektak 8 stylus profiler]]
![[Specific Process Knowledge/Characterization/Profiler#Dektak XTA_new_stylus_profiler|Dektak XTA_new stylus profiler]]
![[Specific Process Knowledge/Characterization/Profiler#Optical_Profiler_(Sensofar)|Optical Profiler (Sensofar)]]
![[Specific Process Knowledge/Characterization/AFM: Atomic Force Microscopy|Nanoman]]
|- valign="top"
|'''General description'''
|Profiler for measuring micro structures. Can do wafer mapping and stress measurements.
|Profiler for measuring micro structures. Can do wafer mapping and stress measurements.
|3D Profiler for measuring micro structures. Can do wafer mapping.
|AFM for measuring nanostructures and surface roughness
|-valign="top"
|'''Substrate size'''
|up to 8"
|up to 6"
|Up to more than 6"
|6" or less
|-valign="top"
|'''Max. scan range xy'''
|Line scan x: 50µm to 200mm
|Line scan x: 50µm to 55mm in one scan. Maximum scan lenght with stiching 200mm.
|Depending on the objective:
*One view: 127µmX95µm to 1270µmX955µm
*Stitching: In principel a hole 6" wafer (time consuming)
|90 µm square
|-valign="top"
|'''Max. scan range z'''
|50Å to 1mm
|50Å to 1mm
|Depending on the objective and Z resolution:
*94.4µm ->9984µm
|1 µm (can go up to 5 µm under special settings)
|-valign="top"
|'''Resolution xy'''
|down to 0.067 µm
|down to 0.003 µm
|Depending on the objective:
*0.5µm -> 5µm
|Depending on scan size and number of samples per line and number of lines - accuracy better than 2%
|-valign="top"
|'''Resolution z'''
|1Å, 10Å, 40Å or 160Å
|1Å, 10Å, 80Å or 160Å
|Depending on measuring methode:
*PSI down to 0.01 nm
*VSI down to 1 nm
*Confocal (depending on objective): 1nm -> 50nm
|<1Å - accuracy better than 2%
|- valign="top"
|'''Max. scan depth [µm] (as a function of trench width W''')
|1.2*(W[µm]-5µm)
|1.2*(W[µm]-5µm)
|Depending on material and trench width:
*Somewhere between 1:1 and 1:12
|~1:1 with standard cantilever.
|-valign="top"
|'''Tip radius'''
|5 µm 45<sup>o</sup> cone
|5 µm 45<sup>o</sup> cone
|No tip - using light
*Blue monochromatic LED: 460nm
*White broadband LED: 550nm
|<12 nm on standard cantilever
|-valign="top"
|'''Stress measurement'''
|Can be done
|Can be done
|No stress calculation capability
|Cannot be done
|-valign="top"
|'''Surface roughness'''
|Can be done on a line scan
|Can be done on a line scan
|Can be done on a line or an area
|Can be done on a selected surface area
|-
|}


{|border="1" cellspacing="1" cellpadding="3" style="text-align:left;"  
{|border="1" cellspacing="1" cellpadding="3" style="text-align:left;"  
Line 99: Line 30:
|-style="background:silver; color:black"
|-style="background:silver; color:black"
!
!
![[Specific Process Knowledge/Characterization/Profiler#Dektak_8_stylus_profiler|Dektak 8 stylus profiler]]
![[Specific Process Knowledge/Characterization/Tencor P17|Tencor P17 <br>(Stylus Profiler)]]
![[Specific Process Knowledge/Characterization/Profiler#Dektak XTA_new_stylus_profiler|Dektak XTA_new stylus profiler]]
![[Specific Process Knowledge/Characterization/Dektak_XTA|Dektak XTA <br>(Stylus Profiler)]]
![[Specific Process Knowledge/Characterization/Profiler#Optical_Profiler_(Sensofar)|Optical Profiler (Sensofar)]]
![[Specific_Process_Knowledge/Characterization/Dektak_150|Dektak 150 <br>(Stylus Profiler)]]
![[Specific Process Knowledge/Characterization/AFM: Atomic Force Microscopy|Nanoman]]
![[Specific Process Knowledge/Characterization/Dektak_3ST | Dektak_3ST <br>(Stylus Profiler)]]
![[Specific_Process_Knowledge/Characterization/Sensofar_S_Neox|Sensofar S Neox <br>(Optical Profiler)]]
![[Specific Process Knowledge/Characterization/Filmetrics|Filmetrics <br>(Optical Profiler)]]
![[Specific Process Knowledge/Characterization/AFM: Atomic Force Microscopy|AFM Icon 1 and AFM Icon 2 <br>(Atomic Force Microscopy)]]
|-
|-


Line 108: Line 42:
|-style="background:WhiteSmoke; color:black"
|-style="background:WhiteSmoke; color:black"
!Generel description
!Generel description
|Profiler for measuring micro structures. Can do wafer mapping and stress measurements.
|Profiler for measuring microstructures in cleanroom. Excellent stress measurements. Excellent sequence programs. Plus wafer mapping and roughness measurements.
|Profiler for measuring micro structures. Can do wafer mapping and stress measurements.
|Profiler for measuring microstructures in cleanroom. Quick and easy vertical profiling. Plus wafer mapping, roughness and stress measurements.
|3D Profiler for measuring micro structures. Can do wafer mapping.
|Profiler for measuring microstructures in building 347.
|Profiler for measuring microstructures in building 346 basement.
|3D Profiler for measuring microstructures and surface roughness. Can do wafer mapping. In cleanroom
|3D Profiler for measuring microstructures and surface roughness. Can do wafer mapping. In basement below cleanroom.
|AFM for measuring nanostructures and surface roughness
|AFM for measuring nanostructures and surface roughness
|-
|-
Line 116: Line 53:
|-
|-
|-style="background:LightGrey; color:black"
|-style="background:LightGrey; color:black"
!'''Max. scan range xy'''
!Max. Scan Range xy
|Line scan x: 50µm to 200mm
|Line scan x: 1 µm to 200mm.
|Line scan x: 50µm to 55mm in one scan. Maximum scan lenght with stiching 200mm.
Map scan xy: up to the largest square that can be inscribed in an 8" wafer
|Line scan x: 50 µm to 55 mm in one scan. Maximum scan length with stitching 200mm.
|Line scan x: 50 µm to 55 mm
|Line scan x: 50 µm to 55 mm
|Depending on the objective:
|Depending on the objective:
*One view: 127µmX95µm to 1270µmX955µm
*One view: 127µmX95µm to 1270µmX955µm
*Stitching: In principel a hole 6" wafer (time consuming)
*Stitching: In principle a whole 6" wafer (time consuming)
|Only 10x objective: 2.0 mm x 1.7 mm
|90 µm square
|90 µm square
|-
|-
Line 127: Line 68:
|-
|-
|-style="background:WhiteSmoke; color:black"
|-style="background:WhiteSmoke; color:black"
!'''Max. scan range z'''
!Max. Scan Range z
|1Å, 10Å, 40Å or 160Å
|up to 900 µm
|1Å, 10Å, 80Å or 160Å
|50 Å to 1 mm
|Depending on measuring methode:
|50 Å to 1 mm
*PSI down to 0.01 nm
|100 Å to 130 nm
*VSI down to 1 nm
|Depending on the objective and Z resolution:
*Confocal (depending on objective): 1nm -> 50nm
*94.4 µm ->9984 µm
|<1Å - accuracy better than 2%
|10 mm (piezo range 500 µm)
|1 µm (can go up to 5 µm under special settings)
 
|-
|-
|-style="background:LightGrey; color:black"
|-style="background:LightGrey; color:black"
!'''Resolution xy'''
!Resolution xy
|down to 0.067 µm
|down to 0.025 µm
|down to 0.003 µm
|down to 0.003 µm
|down to 0.003 µm
|down to 0.5 µm
|Depending on the objective:
|Depending on the objective:
*0.5µm -> 5µm
*0.5µm -> 5µm
|Resolving power of the lens: 0.92 µm
|Depending on scan size and number of samples per line and number of lines - accuracy better than 2%
|Depending on scan size and number of samples per line and number of lines - accuracy better than 2%
|-
|-
Line 147: Line 93:
|-
|-
|-style="background:WhiteSmoke; color:black"
|-style="background:WhiteSmoke; color:black"
!'''Max. scan range z'''
!Resolution z
|, 10Å, 40Å or 160Å
|0.01, 0.08 or 0.6 Å depending on range (note resolution below 1 Å is below the noise level)
|, 10Å, 80Å or 160Å
|1 Å, 10 Å, 40 Å or 160 Å depending on range
|1 Å, 10 Å or 20 Å depending on range
|1 Å, 10 Å, 40 Å or 160 Å depending on range
|Depending on measuring methode:
|Depending on measuring methode:
*PSI down to 0.01 nm
*PSI down to 0.01 nm
*VSI down to 1 nm
*VSI down to 1 nm
*Confocal (depending on objective): 1nm -> 50nm
*Confocal (depending on objective): 1nm -> 50nm
|
*Accuracy 0.7%
*Precision 0.1%
|<1Å - accuracy better than 2%
|<1Å - accuracy better than 2%
|-
|-
|-style="background:LightGrey; color:black"
|-style="background:LightGrey; color:black"
!'''Max. scan depth [µm] (as a function of trench width W''')
!Max. Scan Depth [µm] (as a function of trench width W)
|0.866*(W[µm]-2µm)
|1.2*(W[µm]-5µm)
|1.2*(W[µm]-5µm)
|1.2*(W[µm]-5µm)
|1.2*(W[µm]-5µm)
|1.2*(W[µm]-2.5µm)
|Depending on material and trench width:
|Depending on material and trench width:
*Somewhere between 1:1 and 1:12
*Somewhere between 1:1 and 1:12
|Depending on material and trench width.
|~1:1 with standard cantilever.
|~1:1 with standard cantilever.
|-
|-


|-
|-
|-style="background:WhiteSmoke; color:black"
|-style="background:WhiteSmoke; color:black"
!'''Tip radius'''
!Standard Tip Radius
|2 µm 60<sup>o</sup> cone
|5 µm 45<sup>o</sup> cone
|5 µm 45<sup>o</sup> cone
|5 µm 45<sup>o</sup> cone
|5 µm 45<sup>o</sup> cone
|2.5 µm 45<sup>o</sup> cone
|No tip - using light
*Blue monochromatic LED: 460nm
*White broadband LED: 550nm
|No tip - using light
|No tip - using light
*Blue monochromatic LED: 460nm
*Blue monochromatic LED: 460nm
Line 177: Line 138:


|-style="background:LightGrey; color:black"
|-style="background:LightGrey; color:black"
!'''Stress measurement'''
!Stress Measurement
|Can be done
|Excellent capability
|Can be done
|Can be done
|
|
|No stress calculation capability
|No stress calculation capability
|Cannot be done
|Cannot be done
|-
|Cannot be done
|


|-
|-
|-style="background:WhiteSmoke; color:black"
|-style="background:WhiteSmoke; color:black"
!'''Surface roughness'''
!Surface Roughness
|Can be done on a line or map (parallel line scans)
|Can be done on a line scan
|Can be done on a line scan
|Can be done on a line scan
|Can be done on a line scan
|Recommend P17 or Dektak XTA
|Can be done on a line or an area
|Can be done on a line or an area
|Can be done on a line or an area
|Can be done on a selected surface area  
|Can be done on a selected surface area  
Line 195: Line 162:
|-
|-
|-style="background:LightGrey; color:black"
|-style="background:LightGrey; color:black"
!Substrate size
!Substrate Size
|
|up to 8"
*<nowiki>#</nowiki> small samples
|up to 6"
*<nowiki>#</nowiki> 50 mm wafers
|up to 6"
*<nowiki>#</nowiki> 100 mm wafers
|up to 4"
*<nowiki>#</nowiki> 150 mm wafers
|Up to more than 6"
|
|100x100 mm
*<nowiki>#</nowiki> small samples
|6" or less
*<nowiki>#</nowiki> 50 mm wafers
*<nowiki>#</nowiki> 100 mm wafers
*<nowiki>#</nowiki> 150 mm wafers
|-
|-


|-
|-
|-style="background:WhiteSmoke; color:black"
|-style="background:WhiteSmoke; color:black"
!'''Allowed materials'''
!Allowed Materials
|
Almost any material that leaves no residuals; please ask responsible group about non-standard materials.
|
Almost any material that leaves no residuals; please ask responsible group about non-standard materials.
|
Almost any material that leaves no residuals; please ask responsible group about non-standard materials.
|
Almost any material that leaves no residuals; please ask responsible group about non-standard materials.
|
Almost any material that leaves no residuals; please ask responsible group about non-standard materials.
|
|
*Allowed material 1
Almost any material that leaves no residuals; please ask responsible group about non-standard materials.
*Allowed material 2
|
|
*Allowed material 1
Almost any material that leaves no residuals; please ask responsible group about non-standard materials.
*Allowed material 2
|-
*Allowed material 3
 
|-
|-
|-style="background:LightGrey; color:black"
!Location
|Cleanroom F-2
|Cleanroom B-1
|Building 347, SupportLab
|Basement, building 346, room 904
|Cleanroom C-1
|Basement, building 346, room 904
|AFM Icon1: Cleanroom C-1
AFM Icon2: Basement, building 346, room 904
|-
|}
|}