Specific Process Knowledge/Characterization/XPS/Processing: Difference between revisions

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= XPS data processing =
<!-- Page reviewed 8/5-2023 jmli -->
<!--Checked for updates on 9/5-2023 - ok/jmli -->
{{Contentbydryetch}}


You will need some kind of dedicated software to analyze and interpret the XPS spectra. The internet has many such software packages among which are:
= XPS Data processing with Avantage =
* Avantage: A software platform developed by Thermofisher for acquisition and processing of XPS spectra on their tools. DTU has an academic license that covers all DTU projects for which Avantage can be freely downloaded and licensed, see below. For other academia and commercial users another solution has been established, see also below.
* CasaXPS: A commercial XPS data analysis platform. DTU has an academic license: Download at http://www.casaxps.com/ . The internet and the CasaXPS homepage has extensive material on using this.


Here we will only use the Avantage for obvious reasons. Installing it on your own PC is strongly adviced as the analysis may be time consuming.
== How to analyze data==
 
== For DTU users: Install Avantage ==
 
To install the last version of Avantage (version 5.9919), please log on to files.dtu.dk [www.files.dtu.dk '''click here'''] (an internal DTU file service that works like Dropbox; log on using your DTU initials and password) to acces the shared link:
* [https://files.dtu.dk/a/Ts4eyAtOHshczh7M/d7a04d3c-3a08-41ae-856b-57d1623f504e?l
* The old link [http://www.surfsciftp.co.uk/avant5/download.php] does not seem to work anymore
 
 
 
Run the install file. At some point a nine digit computer number (for your installation) will be given and you will be prompted for a processing licence. To get a license, write an email to Thermo <b>msd.support.nordic@thermofisher.com</b> requesting a standard processing license. You will also have to inform which system the license has to be used for:
* XPS K-Alpha: Use 'System ID KA1002'.
* XPS Nexsa: Use Serial number NXA9953214.
Usually you will have an answer within a day or two. Use the license to activate Avantage and you are ready to analyze your data.
 
== For non-DTU academia and commercial users ==
Getting a non-DTU license for Avantage is unreasonably expensive so we have made another solution: A virtual PC with Avantage installed that users on a specific list can log on to for the purpose of analysing XPS data. What to do:
# Write to Jonas (jmli@dtu.dk or click [mailto:jmli@dtu.dk?Subject=Request%20for%20access%20to%20nlab-xps-avanta here]) requesting to be added to the list.
# You need a VPN connection to DTU. To get that log on to https://vpn.ait.dtu.dk/ and download and install the Cisco AnyConnect Secure Mobility Client (if not already done).
# Log on with win\''xxxx'' where ''xxxx'' is your DTU initials.
# Using the Windows Remote Desktop Connection, log on to nlab-xps-avanta with the same login.
 
== How to analyze data ==


In this section, all steps (import data, add peaks and backgrounds etc.) of the analysis are described.
In this section, all steps (import data, add peaks and backgrounds etc.) of the analysis are described.
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=== Guidelines on data processing ===
=== Guidelines on data processing ===
Click [[Specific Process Knowledge/Characterization/XPS/Processing/Guidelines|'''HERE''']] to see some general guidelines on data processing in Avantage.
Click [[Specific Process Knowledge/Characterization/XPS/Processing/Guidelines|'''HERE''']] to see some general guidelines on data processing in Avantage.
== Introduction to data analysis with Avantage by Thermofisher ==
In the Youtube video below, the application specialist from Thermorfisher Paul Mack walks you through Avantage...somewhat slowly..
[https://www.youtube.com/watch?v=gVzYThRKjYQ '''Click here ''']


== Examples of data analysis ==
== Examples of data analysis ==
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*[[Specific Process Knowledge/Characterization/XPS/Processing/PeriodicTable]]
*[[Specific Process Knowledge/Characterization/XPS/Processing/PeriodicTable]]
= XPS data analysis with CasaXPS =
CasaXPS has its own [https://www.youtube.com/channel/UCUqLBeW-UAjXC55HbRYOabQ Youtube channel] with more than 250 videos so it would be a complete waste of time to make any instructions here. Instead, this is where you as a CasaXPS user could contribute to this database: In case you found any Youtube video that was particularly good, please notify us and we will post a link.
In order to use CasaXPS, you will need to export the data from Avantage and convert it into the Vamas format. Click [[Specific Process Knowledge/Characterization/XPS/Export2CasaXPS | ''this link'']] to find more information.

Latest revision as of 13:15, 30 October 2023

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Unless otherwise stated, the content of this page was created by the dry etch group at DTU Nanolab

XPS Data processing with Avantage

How to analyze data

In this section, all steps (import data, add peaks and backgrounds etc.) of the analysis are described.

XPS Simplified

The web page XPS Simplified is a ThermoScientific page where you can find a lot of information about the techniques, the hardware, data analysis etc.

XPS Knowledge View

A knowledge database providing specific information on every element is included in the software. It provides very useful information about the XPS characteristics of every detectable element and it may even be a very good idea to consult it before the data is acquired. Click HERE to get information on how to access XPS Knowledge View in Avantage.

Basic instructions

Click HERE to have a complete walk-through of an example. This includes

  • Open data file
  • Open and analyze survey spectrum
  • Analyze high resolution spectra of the individual spectra:
    • Add background
    • Add peaks
    • Quantify
  • Analyze depth profiles

Guidelines on data processing

Click HERE to see some general guidelines on data processing in Avantage.

Introduction to data analysis with Avantage by Thermofisher

In the Youtube video below, the application specialist from Thermorfisher Paul Mack walks you through Avantage...somewhat slowly..

Click here

Examples of data analysis

Periodic table with binding energies of all elements

XPS data analysis with CasaXPS

CasaXPS has its own Youtube channel with more than 250 videos so it would be a complete waste of time to make any instructions here. Instead, this is where you as a CasaXPS user could contribute to this database: In case you found any Youtube video that was particularly good, please notify us and we will post a link.

In order to use CasaXPS, you will need to export the data from Avantage and convert it into the Vamas format. Click this link to find more information.