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==Pyrolysis Recipes==
==Pyrolysis Recipes==
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| 200<sup>o</sup>C
| 200<sup>o</sup>C
|-
|-
| Ramping Rate
| First step Anneal time
| 30 minutes
|-
| First step Ramping Rate
| 2<sup>o</sup>C per minute
| 2<sup>o</sup>C per minute
|-
| Final temperature
| 700<sup>o</sup>C
|-
| Ramping rate to final temperature
| 30<sup>o</sup>C per minute
|-
|-
| Annealing time at final temperature
| Annealing time at final temperature
| 6 hours
| 10 minutes
|-
|-
| Gas
| Gas
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=== Optimized Recipe for the porous structure of pyrolytic carbon ===
=== Optimized Recipe for the porous structure of pyrolytic carbon ===
This recipe is applied for High temperature 3D printing resin in order to obtain the high porous structure of pyrolytic carbon material. The structure is characterized by SEM image.
Recipe: ""
[[File:3_step_pyrolysis.png|400px|]]
{| class="wikitable"
|-
! Parameter
! Value
|-
| Precusor
| High temperature 3D printing resin
|-
| Number of step
| 3
|-
| First step Temperature
| 375<sup>o</sup>C
|-
| First step Anneal time
| 3 hours
|-
| First step Ramping Rate
| 2<sup>o</sup>C per minute
|-
| Second step Temperature
| 425<sup>o</sup>C
|-
| Second step Anneal time
| 30 minutes
|-
| Second step Ramping Rate
| 1<sup>o</sup>C per minute
|-
| Final temperature
| 900<sup>o</sup>C
|-
| Ramping rate to final temperature
| 2<sup>o</sup>C per minute
|-
| Annealing time at final temperature
| 1 hour
|-
| Gas
| 20 sccm N<sub>2</sub>
|}
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