Specific Process Knowledge/Thin film deposition/Physimeca/Physimeca calibration: Difference between revisions

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<i> Unless otherwise stated, this page is written by <b>DTU Nanolab internal</b></i>
 
==<span style="color:Red">This machine has been decommissioned. Al+Ti alloy can be prepared by using the Sputter system (Lesker)</span>==


== Calibration of Physimeca  ==
== Calibration of Physimeca  ==

Latest revision as of 09:45, 6 June 2023

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Unless otherwise stated, this page is written by DTU Nanolab internal

This machine has been decommissioned. Al+Ti alloy can be prepared by using the Sputter system (Lesker)

Calibration of Physimeca

As of 16/6/2008 we will use a new system to compensate for "drift" without having to change e.g. 20 gold programs for each refilling. The power setting during deposition is a fraction of the "auto-emission current" on the genius system. In order to compensate for drift in the system the auto and max emission current on the genius is adjusted to achieve the rates at the set powers below This way it should not be necessary to adjust the programs every time, but experienced users will have to occasionally adjust the genius setting.

Reference deposition (step) Material Pocket Rate (Å/s) At power (%) Example of max emission current (6-2008)
mA ~mA for rate
Ti100nm-5A-cal Ti 1 5 70 160 112
Pt100nm-5A-cal Pt 2 5 80 460 368
Au100nm-10A-cal Au 3 10 80 450 360
Ni100nm-5A-cal Ni 4 5 70 250 175
Ge100nm-5A-cal Ge 5 5 70 190 133
Cr100nm-5A-cal Cr 6 5 70 110 77
Pd100nm-5A-cal Pd 6 5 70 160 112

The tooling factor has been determined to ~110 for 100nm layers (lot, 6-2008). It will of course have a small dependence on material and rate.

You can use the steps above as starting point when making new programs (other thicknesses, rates, tilt etc.)

Changing auto and emission current (experienced users only)

If the actual power during deposition is significantly different than the target value (e.g. off by a few % you may change the genius values).

Calculate new auto emission current: Inew="good" current during deposition / target power, e.g. 167mA/0.7 = 240mA (new max emission)

  1. Use genius remote:
  2. Switch to manual mode.
  3. Switch to chosen material
  4. Go to set data and down to auto emission and max emission .
  5. Change both to the new value and note this in the user log.
  6. Go to save/load and save values
  7. Switch back to remote mode on genius.