Specific Process Knowledge/Thin film deposition/Sputter deposition of oxides and other compounds: Difference between revisions

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=Sputter deposition of oxides and other compounds=
<i> Unless otherwise stated, this page is written by <b>DTU Nanolab internal</b></i>


=<span style="background:#FF2800">THIS PAGE IS UNDER CONSTRUCTION</span>[[image:Under_construction.png|200px]]=
=Sputter deposition of oxides=
 
Some metal oxides are well suited for sputter deposition. Below you can compare the sputter systems available here at Nanolab for depositing them. We often start with a metal target and deposit the material in the presence of oxygen.
 
'''This page is a collective page for sputtering of metal oxides that we do not deposit by any other methods.''' Other metal oxides that may be deposited both by sputtering and other methods are described on their own individual pages (see [[Specific Process Knowledge/Thin film deposition|the thin film main page]]).
 
Metal oxides which may be sputter deposited but cannot be deposited by other methods here at Nanolab include:
<br>
<!-- -->
 
 
<b>BaTiO<sub>3</sub></b> (deposited with the Sputter-System (Lesker), see [http://labmanager.dtu.dk/function.php?module=Processlog&view=editlog&machid=244 process log]) <br/>
<b>Cr<sub>2</sub>O<sub>3</sub></b> (deposited several times with the Sputter-System (Lesker), see [http://labmanager.dtu.dk/function.php?module=Processlog&view=editlog&machid=244 process log]) <br/>
<b>MgO</b> (deposited with the Sputter-System (Lesker), see [http://labmanager.dtu.dk/function.php?module=Processlog&view=editlog&machid=244 process log])
 
*[[Specific_Process_Knowledge/Thin_film_deposition/Deposition of MgO|Deposition of MgO with Sputter System (Lesker)]]
 
<b>NiO</b> (extensively deposited with the Sputter-System (Lesker), see [http://labmanager.dtu.dk/function.php?module=Processlog&view=editlog&machid=244 process log]) <br/>
<b>Ta<sub>2</sub>O<sub>5</sub></b> (deposited several times with the Sputter-System (Lesker), see [http://labmanager.dtu.dk/function.php?module=Processlog&view=editlog&machid=244 process log]) <br/>
<b>VO<sub>x</sub></b> (deposited several times with the Sputter-System (Lesker), see [http://labmanager.dtu.dk/function.php?module=Processlog&view=editlog&machid=244 process log]) <br/>
<b>YSZ</b> (Yttrium stabilized zirconia) <br/>
 
 
You are welcome to contact us with requests for other materials.
 
 
==Comparison of sputter deposition options for metal oxides==
 
 
<br clear="all" />
{|border="1" cellspacing="1" cellpadding="3" style="text-align:left;"
|-
 
|-
|-style="background:silver; color:black"
 
!
! Sputter deposition ([[Specific Process Knowledge/Thin film deposition/Lesker|Sputter-System (Lesker)]])
! Sputter deposition ([[Specific Process Knowledge/Thin film deposition/Cluster-based multi-chamber high vacuum sputtering deposition system|Sputter-system Metal-Oxide (PC1)]])
|-
|-style="background:WhiteSmoke; color:black"
! General description
|
Sputter deposition in chamber with 6 x 2" sputter guns at a slight angle to the substrate.
|
Sputter deposition in chamber with 6 x 3" sputter guns for metal and oxide deposition. Targets at a sligth angle to the substrate.
|-
|-style="background:LightGrey; color:black"
! Pre-clean
|RF Ar clean
|RF Ar clean
|-
|-style="background:WhiteSmoke; color:black"
! Target (source material) size
|2"
|3"
|-
|-style="background:LightGrey; color:black"
! Power supply options
| DC and RF
| DC, RF, Pulsed DC, and HiPIMS
 
|-
|-style="background:WhiteSmoke; color:black"
! Batch size
|
*1x4" wafer or
*1x6" wafer or
*several small samples
|
*up to 10x4" wafers or
*up to 10x6" wafers
*or many smaller samples
 
|-style="background:LightGrey; color:black"
! Pumping time from wafer load
|
Approx. 10 min
|
Approx. 11 min
 
|-style="background:WhiteSmoke; color:black"
! Allowed materials
|
*Almost any - see [http://labmanager.dtu.dk/function.php?module=XcMachineaction&view=edit&MachID=244 cross contamination sheet]
|
*Almost any - see [http://labmanager.dtu.dk/function.php?module=XcMachineaction&view=edit&MachID=441 cross contamination sheet]  
 
|-style="background:LightGrey; color:black"
! Other options
|
Source with high-strength magnet available for magnetic oxides
|
Source with high-strength magnet available for magnetic oxides
 
|-style="background:WhiteSmoke; color:black"
! Comments
| Has been used for many oxides with varying degrees of success. You are welcome to request your material of choice. This is our old workhorse and is a relatively dirty system but works very well for many applications.
| We expect that this system will be used for many oxides. You are welcome to request your material of choice. This is our new system for larger batches and more demanding materials. It is also for normal sputtering needs to complement our old Sputter System (Lesker).
|}

Latest revision as of 13:56, 23 May 2023

Feedback to this page: click here

Unless otherwise stated, this page is written by DTU Nanolab internal

Sputter deposition of oxides

Some metal oxides are well suited for sputter deposition. Below you can compare the sputter systems available here at Nanolab for depositing them. We often start with a metal target and deposit the material in the presence of oxygen.

This page is a collective page for sputtering of metal oxides that we do not deposit by any other methods. Other metal oxides that may be deposited both by sputtering and other methods are described on their own individual pages (see the thin film main page).

Metal oxides which may be sputter deposited but cannot be deposited by other methods here at Nanolab include:


BaTiO3 (deposited with the Sputter-System (Lesker), see process log)
Cr2O3 (deposited several times with the Sputter-System (Lesker), see process log)
MgO (deposited with the Sputter-System (Lesker), see process log)

NiO (extensively deposited with the Sputter-System (Lesker), see process log)
Ta2O5 (deposited several times with the Sputter-System (Lesker), see process log)
VOx (deposited several times with the Sputter-System (Lesker), see process log)
YSZ (Yttrium stabilized zirconia)


You are welcome to contact us with requests for other materials.


Comparison of sputter deposition options for metal oxides


Sputter deposition (Sputter-System (Lesker)) Sputter deposition (Sputter-system Metal-Oxide (PC1))
General description

Sputter deposition in chamber with 6 x 2" sputter guns at a slight angle to the substrate.

Sputter deposition in chamber with 6 x 3" sputter guns for metal and oxide deposition. Targets at a sligth angle to the substrate.

Pre-clean RF Ar clean RF Ar clean
Target (source material) size 2" 3"
Power supply options DC and RF DC, RF, Pulsed DC, and HiPIMS
Batch size
  • 1x4" wafer or
  • 1x6" wafer or
  • several small samples
  • up to 10x4" wafers or
  • up to 10x6" wafers
  • or many smaller samples
Pumping time from wafer load

Approx. 10 min

Approx. 11 min

Allowed materials
Other options

Source with high-strength magnet available for magnetic oxides

Source with high-strength magnet available for magnetic oxides

Comments Has been used for many oxides with varying degrees of success. You are welcome to request your material of choice. This is our old workhorse and is a relatively dirty system but works very well for many applications. We expect that this system will be used for many oxides. You are welcome to request your material of choice. This is our new system for larger batches and more demanding materials. It is also for normal sputtering needs to complement our old Sputter System (Lesker).