Specific Process Knowledge/Lithography/Coaters/SprayCoater: Difference between revisions

Latest revision as of 13:49, 10 May 2023

The contents on this page, including all images and pictures, was created by DTU Nanolab staff unless otherwise stated.

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Spray Coater

The spray coater at DTU Nanolab is located in Cleanroom C-1. The machine is an ExactaCoat from Sono-tek which can be fitted with one of three different nozzles depending on the nature of the spray coating tasks at hand. The three different nozzles (Impact, AccuMist and Vortex) are optimized for different applications such as spray coating of large areas (e.g. entire wafers), smaller areas (e.g. wafer pieces or other small samples) or already structured samples that cannot be coated uniformly by spin coating. All nozzles use an ultrasonic tranducer for atomizing the solution to be spray coated. It is therefore a prerequisite that all components are compatible with this process. This is the case with most substances, although process parameters may need optimization to give satisfactory results.

Practically any sample that will fit inside the spray coater can be processed. Spray patterns are easily programmed either using predefined spray patterns (1D line, 2D rectangles/circles/meanders/spirals) or custom 3D spray patterns.

The spray coating process as well as major features of the three nozzles are described into more detail in the manual which can be found via the Equipment Info page in LabManager under the Documents sections. The manual can also be found by clicking this direct link.

Further information about the spray coater (manual, process log, technical information etc.) can be found in LabManger:

Spray coater in LabManager

Process development

Equipment performance and process related parameters

Equipment		Spray Coater
Purpose		Spraying imprint resists (primarily mr-NIL 6000E and mr-I 8000E) Spraying photoresist (primarily AZ-4562) Spraying of other solutions
Performance	Substrate handling	Can handle almost any sample size and shape (although no automatic handling)
	Permanent media	No permanent media
	Manual dispense option	Two syringe pumps
Process parameter range	Solution viscosity	Should not exceed 20 cP
Process parameter range	Chemical properties	Must be non-toxic Must be compatible with titanium Resistant to ultrasonic sonication
Substrates	Batch size	Any sample(s) size and number that fit inside machine
	Allowed materials	All chemicals to be spray coated must be approved specifically for spray coating Most non-toxic, non-particulate and non-crosslinking material likely to be approved Suspensions challenging due to very low diameter tubing

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+{{cc-nanolab}}
+'''Feedback to this page''': '''[mailto:CustomerSupport@Nanolab.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.nanolab.dtu.dk/index.php/Specific_Process_Knowledge/Lithography/Coaters/SprayCoater click here]'''
 ==Spray Coater==
-'''Feedback to this page''': '''[mailto:CustomerSupport@danchip.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.danchip.dtu.dk/index.php/Specific_Process_Knowledge/Lithography/Coaters/SprayCoater click here]'''
+[[image:1042_spraycoater_overview.jpg|400x239px|right|thumb|Spray Coater in Cleanroom C-1]]
+The spray coater at DTU Nanolab is located in Cleanroom C-1. The machine is an ExactaCoat from Sono-tek which can be fitted with one of three different nozzles depending on the nature of the spray coating tasks at hand. The three different nozzles (Impact, AccuMist and Vortex) are optimized for different applications such as spray coating of large areas (e.g. entire wafers), smaller areas (e.g. wafer pieces or other small samples) or already structured samples that cannot be coated uniformly by spin coating. All nozzles use an ultrasonic tranducer for atomizing the solution to be spray coated. It is therefore a prerequisite that all components are compatible with this process. This is the case with most substances, although process parameters may need optimization to give satisfactory results.
+Practically any sample that will fit inside the spray coater can be processed. Spray patterns are easily programmed either using predefined spray patterns (1D line, 2D rectangles/circles/meanders/spirals) or custom 3D spray patterns.
-The spray coater at Danchip is located in Cleanroom C-1. The machine is an ExactaCoat from Sono-tek which can be fitted with one of three different nozzles depending on the nature of the spray coating tasks at hand. The three different nozzles (Impact, AccuMist and Vortex) are optimized for different applications such as spray coating of large areas (e.g. entire wafers), smaller areas (e.g. wafer pieces or other smaller samples) or already structured samples that cannot be coated uniformly by spin coating. All nozzles use an ultrasonic tranducer for atomizing the solution to be spray coated. It is therefore a prerequisite that all components are compatible with this process. This is the case with most substances, although process parameters may need optimization to give satisfactory results.
+The spray coating process as well as major features of the three nozzles are described into more detail in the manual which can be found via the Equipment Info page in LabManager under the Documents sections. The manual can also be found by clicking [http://labmanager.dtu.dk/d4Show.php?id=2523&mach=293 this direct link].
-Practically any sample sample that will fit inside the spray coater can be processed. Spray patterns are easily programmed either using pre-defined spray patterns (1D line, 2D rectangles/circles/meanders/spirals or even custom 3D spray patterns).
+'''Further information about the spray coater (manual, process log, technical information etc.) can be found in LabManger''':
-The spray coating process as well as major features of the three nozzles are described into more detail in the manual which can be found via the Equipment Info page in LabManager. It can be found be clicking Equipment -> Info or by using the direct link below. Then follow the 'User Manual' link.
+[http://labmanager.dtu.dk/function.php?module=Machine&view=view&mach=293 Spray coater in LabManager]'''
-'''The user manual(s), quality control procedure(s) and results, user APV(s), technical information and contact information can be found in [http://labmanager.danchip.dtu.dk/function.php?module=Machine&view=view&mach=293 LabManager]'''
+== Process development==
+*[[/AZ4562|Spray coating using AZ4562]]
+*[[/TISpray|Spray coating using TI Spray]]
+==Equipment performance and process related parameters==
-[[image:1042_spraycoater_overview.jpg|400x239px|right|thumb|Spray Coater in Cleanroom 3]]
 {| border="2" cellspacing="0" cellpadding="2"
@@ Line 21: / Line 30: @@
 |style="background:LightGrey; color:black"|
 |style="background:WhiteSmoke; color:black"|
-*Spraying imprint resist
+*Spraying imprint resists  (primarily mr-NIL 6000E and mr-I 8000E)
-*Spraying photoresist
+*Spraying photoresist (primarily AZ-4562)
 *Spraying of other solutions
 |-
@@ Line 28: / Line 37: @@
 |style="background:LightGrey; color:black"|Substrate handling
 |style="background:WhiteSmoke; color:black"|
-* Can handle almost any sample size and shape
+* Can handle almost any sample size and shape (although no automatic handling)
 |-
 |style="background:LightGrey; color:black"|Permanent media
@@ Line 41: / Line 50: @@
 |style="background:LightGrey; color:black"|Solution viscosity
 |style="background:WhiteSmoke; color:black"|
-*Range
+*Should not exceed 20 cP
 |-
 |style="background:LightGrey; color:black"|Chemical properties
 |style="background:WhiteSmoke; color:black"|
 *Must be non-toxic
-*Compatible with titanium
+*Must be compatible with titanium
-*Resistant to ultrasonic atomization
+*Resistant to ultrasonic sonication
 |-
 !style="background:silver; color:black" align="center" valign="center" rowspan="3"|Substrates
 |style="background:LightGrey; color:black"|Batch size
 |style="background:WhiteSmoke; color:black"|
-*Any sample(s) that fit inside machine
+*Any sample(s) size and number that fit inside machine
 |-
 | style="background:LightGrey; color:black"|Allowed materials
 |style="background:WhiteSmoke; color:black"|
-*All chemicals to be spray coated must be approved specifically for spray coating
+*'''All chemicals to be spray coated must be approved specifically for spray coating'''
-*Any non-toxic, non-particulate and non-crosslinking material is likely to be approved
+*Most non-toxic, non-particulate and non-crosslinking material likely to be approved
+*Suspensions challenging due to very low diameter tubing
 |-
 |}