Specific Process Knowledge/Characterization/XRD/XRD Powder - Revision history

Eves: /* Anton Paar Heating Stage BTS - 500 */

2026-06-18T12:32:47Z

Anton Paar Heating Stage BTS - 500

← Older revision		Revision as of 14:32, 18 June 2026
Line 133:		Line 133:

	==Anton Paar Heating Stage BTS - 500==		==Anton Paar Heating Stage BTS - 500==

			If required, the ambient stage can be replaced with a heating cell unit, enabling powder samples to be heated up to 500 °C under vacuum or in an inert atmosphere. The gas-flow chemistry can also be modified using a dedicated bubbler connected to the gas lines.


			[[/Anton Paar BTS-500\| Anton Paar BTS-500 heating stage]]

Eves: /* Anton Paar Heating Stage */

2026-06-18T12:28:55Z

Anton Paar Heating Stage

← Older revision		Revision as of 14:28, 18 June 2026
Line 132:		Line 132:


	==Anton Paar Heating Stage==		==Anton Paar Heating Stage BTS - 500==

Eves at 12:27, 18 June 2026

2026-06-18T12:27:48Z

← Older revision		Revision as of 14:27, 18 June 2026
Line 130:		Line 130:

	<br clear="all" />		<br clear="all" />


			==Anton Paar Heating Stage==

Reet: /* The XRD Powder setup */

2025-03-31T13:30:14Z

The XRD Powder setup

← Older revision		Revision as of 15:30, 31 March 2025
Line 10:		Line 10:
	Special capabilities:		Special capabilities:

	* The instrument has a 1D strip detector, which makes data acquisition ~~very efficient,~~ so ~~you can measure your samples relatively quickly~~.		* The instrument has a 1D strip detector, which makes data acquisition quicker.
	* The detector ~~also~~ has a fluorescence suppression option~~, so you can measure~~ samples ~~containing for instance~~ iron ~~with the~~ copper radiation.		* It is possible to load up to 6 samples at a time and program the measurements so the machine loads and measures them automatically one after another.
			* The detector has a fluorescence suppression option for measuring samples with iron and other substances that fluoresce under copper radiation.
	* Sample heating up to 500° C possible in N<sub>2</sub>.		* Sample heating up to 500° C possible in N<sub>2</sub>.
	* Transmission measurements possible.		* Transmission measurements possible.

Reet: /* The XRD Powder setup */

2025-03-31T13:27:02Z

The XRD Powder setup

← Older revision		Revision as of 15:27, 31 March 2025
Line 6:		Line 6:
	=The XRD Powder setup=		=The XRD Powder setup=
	[[Image:machine front with on-off button.JPG\|right\|thumb\|300px\|The XRD Powder located in the basement of building 346 at Nanolab, Room 904.]]		[[Image:machine front with on-off button.JPG\|right\|thumb\|300px\|The XRD Powder located in the basement of building 346 at Nanolab, Room 904.]]
	The "XRD powder" is an Aeris Research edition benchtop X-ray diffractometer from Malvern Panalytical. It is meant for phase analysis of powders, is easy to use~~, and offers the option of making measurements while heating the sample in a N<sub><sub>2</sub></sub> atmosphere~~. The setup allows X-ray diffraction measurements with a Cu source in Bragg-Brentano mode (i.e., Theta-2Theta measurements where the incident and diffraction arms of the goniometer are coupled). We have a very limited selection of optics for this instrument, so there is little that the user can adjust.		The "XRD powder" is an Aeris Research edition benchtop X-ray diffractometer from Malvern Panalytical. It is meant for phase analysis of powders and is easy to use. The setup allows X-ray diffraction measurements with a Cu source in Bragg-Brentano mode (i.e., Theta-2Theta measurements where the incident and diffraction arms of the goniometer are coupled). We have a very limited selection of optics for this instrument, so there is little that the user can adjust.
	The instrument has a 1D strip detector, which makes data acquisition very efficient, so you can measure your samples relatively quickly. The detector also has a fluorescence suppression option, so you can measure samples containing for instance iron with the copper radiation.

	Please contact the equipment responsible if you would like to mount the special sample ~~holder~~ for heating ~~during the measurement~~.		Special capabilities:

			* The instrument has a 1D strip detector, which makes data acquisition very efficient, so you can measure your samples relatively quickly.
			* The detector also has a fluorescence suppression option, so you can measure samples containing for instance iron with the copper radiation.
			* Sample heating up to 500° C possible in N<sub>2</sub>.
			* Transmission measurements possible.

			Please contact the equipment responsible if you would like to mount the special sample holders for heating or transmission measurements.

	'''The user manual(s), user APV(s), technical information, and contact information can be found in LabManager:'''		'''The user manual(s), user APV(s), technical information, and contact information can be found in LabManager:'''

Reet: /* The XRD Powder setup */

2024-05-13T14:59:39Z

The XRD Powder setup

← Older revision		Revision as of 16:59, 13 May 2024
Line 6:		Line 6:
	=The XRD Powder setup=		=The XRD Powder setup=
	[[Image:machine front with on-off button.JPG\|right\|thumb\|300px\|The XRD Powder located in the basement of building 346 at Nanolab, Room 904.]]		[[Image:machine front with on-off button.JPG\|right\|thumb\|300px\|The XRD Powder located in the basement of building 346 at Nanolab, Room 904.]]
	The "XRD powder" is an Aeris Research edition benchtop X-ray diffractometer from Malvern Panalytical. It is meant for phase analysis of powders, is easy to use, and offers the option of making measurements while heating the sample in a N<sub><sub>2</sub></sub> atmosphere. The setup allows X-ray diffraction measurements in Bragg-Brentano mode (i.e., Theta-2Theta measurements where the incident and diffraction arms of the goniometer are coupled). We have a very limited selection of optics for this instrument, so there is little that the user can adjust.		The "XRD powder" is an Aeris Research edition benchtop X-ray diffractometer from Malvern Panalytical. It is meant for phase analysis of powders, is easy to use, and offers the option of making measurements while heating the sample in a N<sub><sub>2</sub></sub> atmosphere. The setup allows X-ray diffraction measurements with a Cu source in Bragg-Brentano mode (i.e., Theta-2Theta measurements where the incident and diffraction arms of the goniometer are coupled). We have a very limited selection of optics for this instrument, so there is little that the user can adjust.
			The instrument has a 1D strip detector, which makes data acquisition very efficient, so you can measure your samples relatively quickly. The detector also has a fluorescence suppression option, so you can measure samples containing for instance iron with the copper radiation.

	Please contact the equipment responsible if you would like to mount the special sample holder for heating during the measurement.		Please contact the equipment responsible if you would like to mount the special sample holder for heating during the measurement.
Line 17:		Line 18:
	==Process information==		==Process information==

	*Tips for choosing among the scan and hardware parameters ~~you are allowed to change~~: [[/Measurement tips\| XRD Powder measurement tips]]		*Tips for choosing among the scan and hardware parameters including fluorescence suppression: [[/Measurement tips\| XRD Powder measurement tips]]

	*Malvern Panalytical has a large collection of webinars on XRD. You have to register to view them but the amount of email you receive afterwards is modest, so it's worth it in my opinion (Rebecca, July 2022). Some useful webinars include:		*Malvern Panalytical has a large collection of webinars on XRD. You have to register to view them but the amount of email you receive afterwards is modest, so it's worth it in my opinion (Rebecca, July 2022). Some useful webinars include:

Reet: /* Equipment performance and process related parameters */

2023-05-11T11:49:30Z

Equipment performance and process related parameters

← Older revision		Revision as of 13:49, 11 May 2023
Line 34:		Line 34:
	\|-		\|-
	!style="background:silver; color:black;" align="center" width="60"\|Purpose		!style="background:silver; color:black;" align="center" width="60"\|Purpose
	\|style="background:LightGrey; color:black"\| Crystal structure analysis ~~and thin film thickness measurement~~		\|style="background:LightGrey; color:black"\| Crystal structure analysis
	\|style="background:WhiteSmoke; color:black"\|		\|style="background:WhiteSmoke; color:black"\|
	*Phase ID		*Phase ID

Reet: /* Equipment performance and process related parameters */

2023-05-11T11:49:15Z

Equipment performance and process related parameters

← Older revision		Revision as of 13:49, 11 May 2023
Line 71:		Line 71:
	0.4 mm x 12 mm (Line)		0.4 mm x 12 mm (Line)
	\|-		\|-
	!style="background:silver; color:black" align="center" valign="center" rowspan="5"\|Goniometer		!style="background:silver; color:black" align="center" valign="center" rowspan="4"\|Goniometer
	\|style="background:LightGrey; color:black"\|		\|style="background:LightGrey; color:black"\|
	Scanning mode		Scanning mode
Line 92:		Line 92:
	Fixed with rotation		Fixed with rotation
	\|-		\|-
	~~\|style="background:LightGrey; color:black"\|~~
	~~Sample size~~
	~~\|style="background:WhiteSmoke; color:black"\|~~
	~~Powders~~
	\|-
	!style="background:silver; color:black" align="center" valign="center" rowspan="2"\|Optics		!style="background:silver; color:black" align="center" valign="center" rowspan="2"\|Optics
	\|style="background:LightGrey; color:black"\|Incident side		\|style="background:LightGrey; color:black"\|Incident side

Eves at 12:26, 2 February 2023

2023-02-02T12:26:19Z

← Older revision		Revision as of 14:26, 2 February 2023
Line 2:		Line 2:

	<i> Unless otherwise stated, this page is written by <b>DTU Nanolab internal</b><br>		<i> Unless otherwise stated, this page is written by <b>DTU Nanolab internal</b><br>
	All images and photos on this page ~~belonges~~ to <b>DTU Nanolab</b></i>		All images and photos on this page belongs to <b>DTU Nanolab</b></i>

	=The XRD Powder setup=		=The XRD Powder setup=

Eves at 19:58, 1 February 2023

2023-02-01T19:58:55Z

← Older revision		Revision as of 21:58, 1 February 2023
Line 1:		Line 1:
	'''Feedback to this page''': '''[mailto:labadviser@nanolab.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.nanolab.dtu.dk/index.php/Specific_Process_Knowledge/Characterization/XRD/XRD_Powder click here]'''		'''Feedback to this page''': '''[mailto:labadviser@nanolab.dtu.dk?Subject=Feed%20back%20from%20page%20http://labadviser.nanolab.dtu.dk/index.php/Specific_Process_Knowledge/Characterization/XRD/XRD_Powder click here]'''

	<i> Unless otherwise stated, this page is written by <b>DTU Nanolab internal</b></i>		<i> Unless otherwise stated, this page is written by <b>DTU Nanolab internal</b><br>
			All images and photos on this page belonges to <b>DTU Nanolab</b></i>

	=The XRD Powder setup=		=The XRD Powder setup=